Polysomatism in högbomite: The crystal structures of 10T, 12H, 14T, and 24R polysomes
Clivia Hejny and Thomas Armbruster

Appendix 1: Observed and calculated F-values of högbomite-24R.

h

k

l

F(obs)

s (Fobs)

F(calc)

-1

2

0

262.3417

1.4668

262.1820

0

3

0

191.5251

0.9063

190.5291

-2

4

0

791.5708

6.5069

802.7292

-1

5

0

150.6873

0.8440

147.4857

-3

6

0

146.8710

1.9209

145.7683

0

6

0

415.2779

2.6612

413.8264

-2

7

0

94.0707

0.8276

91.1537

-4

8

0

331.7093

1.5278

329.4506

-1

8

0

97.9746

0.8699

99.4403

-3

9

0

79.1298

1.1850

78.0504

-5

10

0

93.0960

1.3550

94.8863

-1

1

1

47.1612

0.6362

48.7516

0

2

1

9.0097

4.2891

2.2401

-2

3

1

10.4552

2.9046

9.6254

-4

4

1

9.9827

5.5506

10.7855

-1

4

1

19.0330

1.4728

21.8545

-3

5

1

35.3784

1.0123

34.8151

0

5

1

11.6796

4.7809

5.2935

-5

6

1

6.9978

4.7690

5.3664

-2

6

1

14.0391

4.0048

13.9671

-7

7

1

24.9538

3.1010

22.1344

-4

7

1

11.2460

4.1974

3.6173

-1

7

1

7.0342

5.1083

12.2052

-6

8

1

2.7673

6.4061

6.6690

-3

8

1

5.9736

2.8013

 

0

8

1

16.6962

5.8663

13.5207

-8

9

1

6.6865

6.4574

-0.3716

-5

9

1

16.7375

5.1318

14.6919

-2

9

1

2.7022

6.4190

-0.2663

-7

10

1

10.8512

7.5785

-2.4011

-4

10

1

19.9575

4.1400

9.7174

0

1

2

54.2013

0.6367

-54.1969

-2

2

2

17.4924

3.4921

20.7192

-1

3

2

17.9340

1.4028

-16.1085

-3

4

2

31.7440

1.0811

-28.7896

0

4

2

6.6109

5.1716

 

-5

5

2

3.6707

7.0683

-2.2234

-2

5

2

33.9304

1.4008

-33.8751

-4

6

2

4.7034

6.6988

-1.2774

-1

6

2

9.0970

5.7319

-13.7567

-6

7

2

23.8967

2.7774

-24.4369

-3

7

2

13.4280

6.6141

-5.4682

0

7

2

26.3213

3.0559

-27.2475

-8

8

2

20.5421

6.1797

-7.6816

-5

8

2

17.2656

4.7300

-19.6539

-2

8

2

6.2489

7.0774

-4.6181

-7

9

2

4.7328

6.3992

-2.3704

-4

9

2

24.9283

3.1321

-24.7294

-1

9

2

15.2007

6.0791

-9.8024

-6

10

2

7.3848

6.5489

-7.1569

-3

10

2

12.4906

7.0830

-14.6656

0

0

3

3.7941

2.1797

-2.8572

-1

2

3

15.7580

2.3906

-10.8394

-3

3

3

14.8909

4.4018

8.7531

0

3

3

21.1303

4.4983

-19.7904

-2

4

3

2.5701

6.3931

0.2884

-4

5

3

18.5795

2.2167

-18.7957

-1

5

3

9.0351

5.8162

-2.5484

-6

6

3

7.8172

7.2466

3.8971

-3

6

3

13.1326

5.8765

-15.8719

0

6

3

15.9067

6.7960

5.9972

-5

7

3

12.7683

4.7796

10.7566

-2

7

3

12.1445

5.5958

-9.3265

-7

8

3

12.6379

6.4287

-10.9199

-4

8

3

9.8224

7.0837

7.3353

-1

8

3

6.1965

6.4280

-5.2629

-6

9

3

12.8643

5.1314

-5.3483

-3

9

3

11.6901

6.1991

5.3818

-5

10

3

13.6528

7.4702

-10.1042

-1

1

4

22.1839

5.4560

-13.3975

0

2

4

340.1362

1.0177

341.1125

-2

3

4

79.8729

0.7966

79.0159

-4

4

4

268.2338

1.9093

266.0908

-1

4

4

4.4227

5.5084

-1.1756

-3

5

4

39.0897

1.3841

-40.2762

0

5

4

69.1977

1.1582

68.4076

-5

6

4

26.7124

2.4530

24.1649

-2

6

4

204.1686

1.2203

202.3719

-7

7

4

30.6201

2.6351

-31.7023

-4

7

4

47.4444

1.3791

47.9494

-1

7

4

15.7676

4.3960

-16.1938

-6

8

4

145.0898

1.5983

139.0815

-3

8

4

6.1235

7.0436

1.8927

0

8

4

107.6351

3.6047

104.2390

-8

9

4

23.5681

4.2942

25.8998

-5

9

4

17.9833

6.3068

-21.4646

-2

9

4

46.9904

2.8621

48.8878

-7

10

4

5.9737

13.2896

 

-4

10

4

95.9772

1.3276

93.7662

0

1

5

99.9247

0.8481

-98.9888

-2

2

5

50.1719

0.7737

45.9985

-1

3

5

37.6592

0.7533

-37.2997

-3

4

5

43.5066

1.0154

-44.0841

0

4

5

8.0598

7.8531

-1.0696

-5

5

5

23.1913

2.5595

-24.3857

-2

5

5

58.3882

0.9967

-62.4107

-4

6

5

14.0340

3.9005

-14.7349

-1

6

5

15.1456

4.8231

-16.5352

-6

7

5

28.1277

2.2859

-29.4763

-3

7

5

18.9284

3.2902

-18.6416

0

7

5

42.8468

1.9940

-45.5382

-8

8

5

24.0238

4.3310

-23.3390

-5

8

5

11.1180

8.6068

-12.6266

-2

8

5

19.6212

4.1254

-18.9102

-7

9

5

17.7982

4.9666

-16.5671

-4

9

5

32.1562

2.2651

-35.7472

-1

9

5

4.1847

6.4330

-8.6509

-6

10

5

11.5849

6.3703

-22.2411

-3

10

5

5.9736

-2.8470

 

0

0

6

16.0235

1.7355

-5.0044

-1

2

6

4.9858

4.8937

-2.0726

-3

3

6

16.3025

6.5970

-14.3532

0

3

6

1.3849

6.7403

8.5539

-2

4

6

9.1971

6.2476

-5.7707

-4

5

6

5.5591

5.7062

 

-1

5

6

8.4444

5.8787

-6.3509

-6

6

6

8.2589

7.3288

-7.3912

-3

6

6

5.3708

6.2673

1.7664

0

6

6

12.1577

8.5684

-7.5603

-5

7

6

5.9737

-9.5797

 

-2

7

6

8.7517

6.9217

4.1898

-7

8

6

3.2156

6.4271

3.7458

-4

8

6

7.0045

7.1050

-8.1237

-1

8

6

9.2099

7.0510

-0.8806

-6

9

6

12.5458

5.2069

3.0168

-3

9

6

7.4084

8.6045

-5.3172

-5

10

6

7.2109

6.4564

2.9811

-1

1

7

113.2136

0.7326

111.3284

0

2

7

89.6471

1.0196

-81.2069

-2

3

7

32.5479

0.8597

34.2770

-4

4

7

28.0499

2.0541

-28.4300

-1

4

7

63.4601

0.6940

65.6201

-3

5

7

77.8434

0.9632

79.7707

0

5

7

14.0982

6.2435

7.0833

-5

6

7

28.8468

1.6042

29.9365

-2

6

7

6.9759

6.7686

-11.1668

-7

7

7

57.0773

1.8794

59.0060

-4

7

7

5.2536

6.3664

12.1242

-1

7

7

50.8815

1.3557

50.2116

-6

8

7

8.6869

7.3114

-8.8449

-3

8

7

37.5788

1.8178

36.9496

0

8

7

1.7503

7.4584

1.1015

-8

9

7

12.6207

5.5808

16.2859

-5

9

7

49.0854

2.6951

49.5984

-2

9

7

4.9540

6.3946

3.9661

-7

10

7

25.3418

3.4253

22.8875

-4

10

7

6.9982

9.0172

-1.1141

0

1

8

92.7412

2.2484

-90.3934

-2

2

8

34.4754

1.0285

47.4377

-1

3

8

51.7911

1.6258

-49.5470

-3

4

8

71.5248

0.7610

-70.2090

0

4

8

111.0646

1.4371

108.9901

-5

5

8

15.6320

5.7687

-18.2679

-2

5

8

57.7590

0.9565

-56.7712

-4

6

8

100.7082

1.5492

99.8649

-1

6

8

47.7262

1.0763

-46.0968

-6

7

8

44.4557

1.3666

-44.9360

-3

7

8

24.2922

5.1291

-21.9903

0

7

8

29.4747

2.7280

-31.2359

-8

8

8

52.2112

1.9956

54.6335

-5

8

8

49.6219

1.6168

-48.2975

-2

8

8

70.1105

1.2498

67.9159

-7

9

8

3.4153

6.4228

-4.8889

-4

9

8

29.6116

3.1387

-29.2044

-1

9

8

26.2015

3.3138

-24.1107

-6

10

8

47.9242

1.9139

46.9943

-3

10

8

41.6318

2.0782

-36.5670

0

0

9

5.8789

6.5412

-1.1534

-1

2

9

26.8935

0.8231

25.6910

-3

3

9

40.9995

2.2755

-38.2869

0

3

9

78.5796

1.1635

80.1267

-2

4

9

11.1664

4.3295

-3.7562

-4

5

9

50.7365

1.1418

52.0519

-1

5

9

14.3551

3.3084

-13.6348

-6

6

9

12.1222

6.4156

-6.6736

-3

6

9

17.0229

4.7389

19.5254

0

6

9

15.1539

7.2436

-14.8264

-5

7

9

34.8431

2.0685

-33.9944

-2

7

9

49.9724

2.3227

49.3276

-7

8

9

20.4617

4.0200

20.7173

-4

8

9

12.2264

6.2595

-13.4544

-1

8

9

10.8700

8.5778

-4.5211

-6

9

9

29.5118

4.0807

28.2036

-3

9

9

19.8045

6.3241

-20.7436

-5

10

9

5.9736

6.5073

 

-1

1

10

46.4256

0.8855

42.5123

0

2

10

175.4701

0.9350

-163.4884

-2

3

10

28.5567

0.9600

25.9115

-4

4

10

71.9560

1.0657

-74.8643

-1

4

10

20.7496

3.2371

22.0541

-3

5

10

24.5880

2.7442

23.2222

0

5

10

10.9544

8.7785

16.9054

-5

6

10

12.1174

5.3568

13.5606

-2

6

10

45.2608

1.2375

-47.0390

-7

7

10

20.8377

4.3601

16.8806

-4

7

10

14.1129

5.0362

14.0836

-1

7

10

17.6665

5.5868

14.7224

-6

8

10

23.8341

2.9987

-25.7439

-3

8

10

12.4042

6.5784

11.8057

0

8

10

13.5002

9.8926

-21.3729

-8

9

10

10.0809

6.6979

10.1500

-5

9

10

4.2887

6.4470

14.5744

-2

9

10

3.2553

6.4677

12.9469

-7

10

10

5.6941

7.2957

9.1630

-4

10

10

10.5429

6.5336

-17.2391

0

1

11

47.3547

1.2418

-48.1406

-2

2

11

191.4705

1.6194

182.4445

-1

3

11

36.2397

0.7972

-37.2690

-3

4

11

18.8921

2.3408

-20.6185

0

4

11

75.2250

1.1337

76.9210

-5

5

11

28.4588

3.1392

-26.2478

-2

5

11

29.1599

1.5862

-29.9445

-4

6

11

46.1387

1.2462

46.7763

-1

6

11

4.0753

5.7812

-3.6958

-6

7

11

14.9948

5.3773

-6.1951

-3

7

11

14.9283

4.7541

-11.8542

0

7

11

23.6727

3.1918

-18.4633

-8

8

11

19.2501

5.2854

20.6347

-5

8

11

5.9736

7.4878

 

-2

8

11

23.6078

2.7575

23.6979

-7

9

11

10.7590

6.7468

-7.3114

-4

9

11

18.6609

4.9918

-11.3979

-1

9

11

9.5288

7.2118

7.5772

-6

10

11

21.2366

5.3106

15.5019

0

0

12

144.9756

0.9707

141.1686

-1

2

12

361.2104

2.1503

-362.4499

-3

3

12

257.7300

1.0871

-255.5704

0

3

12

335.9925

2.9991

-334.6349

-2

4

12

77.5964

3.4313

76.5328

-4

5

12

236.7579

1.2169

-235.1674

-1

5

12

195.6022

1.0368

-194.0845

-6

6

12

35.0549

2.0135

35.2188

-3

6

12

186.3895

1.5331

-186.5922

0

6

12

45.2572

2.9993

44.5870

-5

7

12

126.0363

1.7020

-124.8032

-2

7

12

176.1946

1.4215

-176.6391

-7

8

12

121.2869

1.5035

-118.1794

-4

8

12

26.1956

4.9644

27.8031

-1

8

12

105.9994

2.5754

-105.2209

-6

9

12

118.7789

2.6937

-117.9031

-3

9

12

91.3464

1.4999

-91.1535

-5

10

12

88.6919

1.4225

-88.2653

-1

1

13

14.3574

3.2827

-19.1561

0

2

13

236.1087

1.0372

-231.8416

-2

3

13

10.1632

3.5299

-9.9749

-4

4

13

113.5809

2.4261

-117.7603

-1

4

13

23.1406

2.4510

-23.5076

-3

5

13

14.3563

4.8706

-11.8792

0

5

13

13.7976

6.5265

2.9154

-5

6

13

22.2949

3.7039

-20.1896

-2

6

13

75.0696

0.9536

-78.6214

-7

7

13

3.5650

7.3674

-4.3475

-4

7

13

9.1216

7.8829

-4.6207

-1

7

13

22.1089

2.3001

-17.8284

-6

8

13

45.3831

1.5721

-44.5020

-3

8

13

25.6418

2.8568

-25.8586

0

8

13

34.5806

2.5815

-36.1878

-8

9

13

2.9028

6.4636

-13.8309

-5

9

13

3.7075

6.4343

-6.6536

-2

9

13

11.2870

5.6841

2.1868

-4

10

13

23.8580

3.6531

-28.9529

0

1

14

43.1523

0.7058

41.4954

-2

2

14

234.1510

0.9335

233.5010

-1

3

14

39.8287

0.7589

37.2739

-3

4

14

28.6444

1.3611

26.9600

0

4

14

115.8661

1.4323

121.8752

-5

5

14

27.3771

2.5215

26.2199

-2

5

14

21.6648

2.0025

19.0243

-4

6

14

83.2152

1.0342

85.2813

-1

6

14

18.5886

3.3502

24.7310

-6

7

14

20.2576

3.1672

19.5081

-3

7

14

26.7382

2.1244

24.4300

0

7

14

15.0843

6.3130

16.5133

-8

8

14

48.6615

1.9862

50.8513

-5

8

14

21.5881

3.2928

21.7181

-2

8

14

55.6865

1.4240

57.8126

-7

9

14

18.6046

6.1386

21.3037

-4

9

14

13.3678

8.2257

17.1249

-1

9

14

22.2837

4.2667

21.3091

-6

10

14

45.0434

1.9709

44.8130

0

0

15

9.5149

7.6521

10.3073

-1

2

15

19.0902

2.8127

-17.1177

-3

3

15

49.7353

1.0345

-52.6973

0

3

15

36.1717

2.1195

35.9107

-2

4

15

13.8635

4.9360

16.6769

-4

5

15

14.4610

3.2799

14.2962

-1

5

15

30.6893

1.8700

-32.8319

-6

6

15

13.4767

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9

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19.5137

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29.6902

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5.7713

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39.6309

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24.1168

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1

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10.0987

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40.9834

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27.6108

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-3

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23.4289

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22.4916

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5.9736

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13.7064

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22.6062

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31.8109

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38.7423

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15.3491

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7.9811

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79.5731

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196.2200

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89.7051

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29

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0

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15.4273

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-1

2

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19.3237

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9.2215

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24.2735

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12.6419

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8

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21.3215

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5.9736

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8

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16.9605

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20.0700

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13.6914

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1

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215.2219

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154.7037

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58.1190

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76.4788

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37.9743

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-5

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0.0007

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118.4543

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3.3174

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13.2153

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279.4219

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147.6674

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60

124.5419

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1

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81.1342

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193.8533

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153.8311

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74.8992

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-3

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58.2155

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-7

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33.6785

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55.1035

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60.6418

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10.6826

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88.2286

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16.2007

3.4929

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-3

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62

11.1392

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68.4270

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-5

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19.4784

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8.9808

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57.1728

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14.3064

6.2012

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-6

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62

6.4494

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10.8900

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132.9962

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63

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63

48.3894

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-6

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63

89.9558

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52.5089

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63

82.0463

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-5

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63

36.9591

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73.6942

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20.1134

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260.1324

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207.5509

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-3

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26.6511

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167.3128

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-4

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18.8725

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11.2009

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3.1111

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0

4

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8.4354

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12.1858

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66

57.4671

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45.7513

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66

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38.1681

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28.8937

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31.4095

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27.5046

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24.7314

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67

20.8914

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67

11.6465

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67

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4

67

12.9774

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67

5.0995

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0.3287

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67

21.1033

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67

8.5673

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17.4302

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1

68

42.4094

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68

89.1146

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68

60.1400

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68

37.2592

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67.9944

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68

59.8792

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68

19.2793

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68

57.9837

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6

68

46.4660

1.7871

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7

68

54.3905

1.7609

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0

69

62.8664

1.9665

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-1

2

69

5.2575

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-3

3

69

2.0249

7.3606

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3

69

20.5876

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69

54.0192

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5

69

8.9933

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5

69

7.5924

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42.0429

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69

9.7056

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44.9375

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-5

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69

15.1212

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7

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9.8782

7.2971

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1

70

33.2780

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2

70

17.4246

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3

70

21.1678

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70

17.9862

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4

70

29.5864

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-3

5

70

35.1207

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5

70

10.3758

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-5

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70

13.6796

7.6183

21.5699

-2

6

70

18.2454

8.2889

14.6884

-4

7

70

5.9737

15.7627

 

0

1

71

12.8155

6.1978

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-2

2

71

69.9727

2.6561

67.1130

-1

3

71

5.5591

-4.9269

 

-3

4

71

10.1238

7.1460

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0

4

71

51.8928

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-5

5

71

14.2611

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71

21.0734

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-4

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71

40.1110

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71

15.8605

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-3

7

71

10.4263

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0

72

13.3648

10.8560

22.0812

-1

2

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10.4845

5.0104

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