Ms.# 8049. Callegari et al. The crystal structure of peprossiite-(Ce)…

Table 5. Observed and calculated structure factors. * mark the reflections considered as not observed during the structure refinement

Crystal Pep1

H K L /FO/ /FC/ H K L /FO/ /FC/ H K L /FO/ /FC/

 

1 0 0 16.3 15.8 6 1 1 11.9 12.1 0 6 2 10.2 10.6

2 0 0 52.4 53.2 7 1 1 4.7 5.0 1 6 2 11.2 11.4

3 0 0 62.5 63.0 8 1 1 5.9 5.7 2 6 2 11.3 11.5

4 0 0 15.1 15.7 9 1 1 4.9 4.2 3 6 2 5.3 4.9

5 0 0 27.5 27.5 0 2 1 42.7 42.6 4 6 2 6.6 6.4

6 0 0 20.2 20.4 2 2 1 22.9 23.4 5 6 2 5.6 5.2

7 0 0 12.5 12.3 3 2 1 17.9 18.2 0 7 2 10.0 10.1

8 0 0 7.9 7.9 4 2 1 18.2 18.4 1 7 2 6.3 6.4

9 0 0 9.8 9.5 5 2 1 9.1 9.2 2 7 2 5.9 5.8

10 0 0 5.6 5.3 6 2 1 7.6 7.6 3 7 2 6.8 6.6

1 1 0 55.0 54.0 7 2 1 8.8 8.5 4 7 2* 2.3 2.2

2 1 0 21.9 21.0 8 2 1* 2.6 1.6 0 8 2 11.2 10.7

3 1 0 12.0 8.7 9 2 1 4.1 4.0 1 8 2 6.6 6.6

4 1 0 28.0 27.9 3 3 1 9.4 9.6 2 8 2 5.1 4.8

5 1 0 8.0 7.8 4 3 1 13.9 14.1 3 8 2 5.7 5.4

6 1 0 3.3 3.8 5 3 1 6.3 6.3 0 9 2* 2.3 2.4

7 1 0 12.4 12.4 6 3 1 5.2 5.2 1 9 2 4.6 4.4

8 1 0 3.1 1.6 7 3 1 4.6 4.4 2 9 2 3.4 3.1

9 1 0* 2.7 1.5 8 3 1* 2.5 2.2 0 10 2 5.5 5.3

2 2 0 44.5 44.6 0 4 1 26.8 27.2 0 0 3 6.4 6.4

2 3 0 24.8 24.9 4 4 1 7.5 7.3 1 0 3 43.8 44.4

3 3 0 26.0 25.6 5 4 1 8.7 8.7 3 0 3 17.1 17.2

4 3 0 8.4 8.8 6 4 1 5.6 5.1 5 0 3 2.2 1.9

5 3 0 10.2 10.3 7 4 1 3.6 3.3 7 0 3 2.5 2.8

6 3 0 10.1 10.0 5 5 1* 2.5 2.0 9 0 3 4.5 4.0

7 3 0 5.7 5.4 6 5 1 3.9 3.5 1 1 3 59.5 58.1

8 3 0 2.6 2.5 0 6 1 8.6 8.8 2 1 3 29.4 28.9

2 4 0 8.2 7.5 0 8 1 4.5 4.1 3 1 3 31.5 31.2

4 4 0 13.4 12.7 0 10 1 2.3 2.1 4 1 3 22.9 23.0

2 5 0 26.0 25.9 0 0 2 40.2 39.8 5 1 3 15.6 15.6

4 5 0 4.8 4.8 0 1 2 54.2 54.3 6 1 3 13.2 13.3

5 5 0 14.6 14.1 1 1 2 31.0 30.8 7 1 3 8.9 8.9

6 5 0* 2.7 2.7 0 2 2 42.9 42.9 8 1 3 7.6 7.0

2 6 0 6.8 5.9 1 2 2 37.7 37.6 9 1 3 4.5 4.4

4 6 0 3.7 2.1 2 2 2 17.6 17.9 0 2 3 6.1 6.7

2 7 0 5.7 5.6 0 3 2 30.4 30.9 2 2 3 25.4 25.3

4 7 0 6.7 6.2 1 3 2 26.9 27.2 3 2 3 8.9 9.2

2 8 0 10.3 9.9 2 3 2 26.8 27.1 4 2 3 17.9 18.0

2 9 0 2.2 2.0 3 3 2 15.2 15.2 5 2 3 5.8 6.0

0 0 1 28.0 28.2 0 4 2 22.7 22.9 6 2 3 8.1 7.8

1 0 1 47.7 47.5 1 4 2 13.8 14.2 7 2 3 4.2 4.2

3 0 1 14.2 14.4 2 4 2 16.2 16.3 8 2 3* 3.0 2.8

5 0 1 13.5 13.7 3 4 2 13.3 13.4 9 2 3 2.8 2.6

7 0 1 10.7 10.9 4 4 2 6.8 6.9 3 3 3 17.6 17.3

9 0 1 5.2 4.8 0 5 2 24.0 24.4 4 3 3 11.1 11.2

1 1 1 25.5 25.5 1 5 2 17.0 17.5 5 3 3 4.8 4.6

2 1 1 32.7 32.8 2 5 2 8.9 9.2 6 3 3 9.3 8.9

3 1 1 27.8 27.6 3 5 2 14.2 14.0 7 3 3* 2.8 2.2

4 1 1 15.4 15.9 4 5 2 7.4 7.2 8 3 3 3.7 2.7

5 1 1 13.7 14.2 5 5 2 6.0 5.8 0 4 3 21.0 21.2

 

 

 

H K L /FO/ /FC/ H K L /FO/ /FC/ H K L /FO/ /FC/

 

4 4 3 13.3 13.0 1 0 5 24.7 24.9 2 4 6 11.8 11.5

5 4 3 6.4 6.3 3 0 5 28.8 29.2 3 4 6 11.4 11.8

6 4 3 6.3 6.0 5 0 5 6.2 6.8 4 4 6 5.9 4.7

7 4 3 4.8 4.6 7 0 5 6.4 6.2 0 5 6 28.4 28.6

5 5 3* 2.0 1.3 9 0 5 7.6 7.5 1 5 6 11.2 11.5

6 5 3 3.7 3.2 1 1 5 49.0 48.8 2 5 6 14.7 14.8

0 6 3 13.5 13.7 2 1 5 19.4 19.3 3 5 6 12.3 12.5

0 8 3* 3.0 2.6 3 1 5 18.2 18.2 4 5 6 6.9 7.0

0 10 3* .7 .6 4 1 5 25.0 25.4 5 5 6 8.4 8.6

0 0 4 29.4 29.6 5 1 5 8.8 9.1 0 6 6 9.3 9.4

0 1 4 48.7 48.8 6 1 5 7.6 8.0 1 6 6 6.8 7.0

1 1 4 28.0 27.0 7 1 5 9.9 10.2 2 6 6 8.6 8.4

0 2 4 36.9 36.8 8 1 5 4.1 3.5 3 6 6 4.0 3.8

1 2 4 34.9 34.8 9 1 5 3.0 2.6 4 6 6 4.5 3.9

2 2 4 17.3 17.3 0 2 5 19.6 19.6 5 6 6 4.1 4.0

0 3 4 29.1 29.3 2 2 5 33.9 34.2 0 7 6 14.0 14.2

1 3 4 25.6 25.4 3 2 5 9.8 10.2 1 7 6 5.4 5.5

2 3 4 23.6 24.1 4 2 5 11.6 12.0 2 7 6 7.6 7.4

3 3 4 16.9 17.0 5 2 5 14.8 15.1 3 7 6 6.8 6.9

0 4 4 19.9 20.1 6 2 5 4.6 4.4 4 7 6* 2.9 2.5

1 4 4 15.4 15.8 7 2 5 4.9 5.1 0 8 6 9.6 9.6

2 4 4 14.4 14.6 8 2 5 5.0 4.9 1 8 6 4.0 3.6

3 4 4 11.5 11.9 3 3 5 18.3 18.7 2 8 6 5.7 5.5

4 4 4 7.8 8.0 4 3 5 8.6 8.9 3 8 6 3.9 3.8

0 5 4 20.9 21.2 5 3 5 2.8 3.2 0 9 6 4.8 4.7

1 5 4 16.0 16.3 6 3 5 9.6 9.7 1 9 6 3.2 2.9

2 5 4 9.3 9.5 7 3 5* 2.7 2.3 0 10 6 5.8 6.2

3 5 4 13.1 13.1 8 3 5* 1.1 1.0 0 0 7 12.7 12.8

4 5 4 6.2 6.3 0 4 5 16.7 17.2 1 0 7 35.0 34.5

5 5 4 6.1 6.0 4 4 5 13.3 13.1 3 0 7 5.8 6.1

0 6 4 11.4 11.9 5 4 5 5.4 5.4 5 0 7 14.3 14.6

1 6 4 10.4 10.5 6 4 5 3.3 3.1 7 0 7 11.1 11.5

2 6 4 10.7 10.8 7 4 5 6.0 5.8 9 0 7* 3.2 3.1

3 6 4 5.8 5.5 5 5 5 5.7 5.7 1 1 7 15.3 14.1

4 6 4 6.3 6.2 6 5 5* 1.8 1.8 2 1 7 27.4 27.2

5 6 4 5.2 5.0 0 6 5 15.5 15.9 3 1 7 24.1 23.8

0 7 4 8.0 8.3 0 8 5* 1.2 1.7 4 1 7 7.5 7.7

1 7 4 7.2 7.3 0 10 5* 2.0 .7 5 1 7 13.0 13.3

2 7 4 4.8 4.8 0 0 6 67.3 67.0 6 1 7 11.5 11.5

3 7 4 6.2 6.1 0 1 6 29.9 29.3 7 1 7* 2.3 1.9

4 7 4* 2.4 2.2 1 1 6 18.4 16.1 8 1 7 5.4 5.6

0 8 4 10.5 10.1 0 2 6 47.8 47.9 9 1 7 4.7 4.3

1 8 4 6.3 6.4 1 2 6 27.0 26.4 0 2 7 33.1 32.9

2 8 4 5.3 5.1 2 2 6 20.8 21.0 2 2 7 12.9 13.3

3 8 4 5.9 5.4 0 3 6 32.8 32.9 3 2 7 17.4 17.7

0 9 4* 2.5 2.2 1 3 6 16.4 15.2 4 2 7 17.0 17.1

1 9 4 4.5 4.3 2 3 6 26.5 26.9 5 2 7 4.7 5.1

2 9 4* 2.5 2.8 3 3 6 12.2 11.9 6 2 7 7.5 7.6

0 10 4 4.9 5.0 0 4 6 19.2 19.7 7 2 7 9.1 8.8

0 0 5 49.0 47.3 1 4 6 12.0 12.2 8 2 7* 1.7 .7

 

 

 

H K L /FO/ /FC/ H K L /FO/ /FC/ H K L /FO/ /FC/

 

3 3 7 4.0 3.2 0 9 8 5.5 5.4 2 4 10 9.6 9.7

4 3 7 13.3 13.7 1 9 8* 2.5 2.4 3 4 10 7.6 7.9

5 3 7 6.7 6.7 0 0 9 2.8 2.5 4 4 10 8.4 8.2

6 3 7* 2.8 2.3 1 0 9 28.9 28.0 0 5 10 12.6 13.0

7 3 7 4.9 4.7 3 0 9 10.5 10.8 1 5 10 11.4 11.3

8 3 7* 2.7 2.4 5 0 9* 1.6 2.1 2 5 10 8.3 8.6

0 4 7 24.0 24.5 7 0 9* 2.9 2.6 3 5 10 9.5 9.4

4 4 7 4.3 3.2 9 0 9* 2.7 2.8 4 5 10 4.1 4.1

5 4 7 8.7 8.9 1 1 9 31.6 30.6 5 5 10 6.2 5.9

6 4 7 5.6 5.1 2 1 9 21.0 20.6 0 6 10 10.9 11.1

7 4 7* 2.1 1.9 3 1 9 22.7 22.2 1 6 10 7.1 7.4

5 5 7* .1 .7 4 1 9 15.7 16.0 2 6 10 7.8 7.8

6 5 7 3.7 3.6 5 1 9 11.9 12.2 3 6 10 6.1 5.9

0 6 7 3.5 3.7 6 1 9 10.6 10.7 4 6 10 4.7 4.5

0 8 7 4.8 4.5 7 1 9 6.2 6.5 0 7 10 4.9 5.0

0 0 8 49.5 48.5 8 1 9 6.1 6.0 1 7 10 7.4 7.4

0 1 8 23.1 22.4 9 1 9 3.8 3.9 2 7 10* 3.3 2.8

1 1 8 32.4 32.2 0 2 9 10.3 10.2 3 7 10 4.4 4.3

0 2 8 24.6 24.4 2 2 9 16.6 16.7 0 8 10 7.3 7.4

1 2 8 19.4 19.4 3 2 9 7.3 7.6 1 8 10 4.9 4.7

2 2 8 24.9 24.9 4 2 9 13.7 13.9 2 8 10 5.3 5.2

0 3 8 34.0 33.8 5 2 9 4.0 4.2 0 9 10* 2.6 2.6

1 3 8 13.8 14.1 6 2 9 6.5 6.6 0 0 11 13.1 13.1

2 3 8 15.9 16.3 7 2 9 3.7 3.9 2 0 11 14.9 15.0

3 3 8 18.7 19.1 8 2 9* 2.0 1.7 4 0 11 13.7 13.9

0 4 8 12.8 13.1 3 3 9 12.6 12.4 6 0 11 7.6 7.6

1 4 8 19.3 19.6 4 3 9 8.7 9.0 8 0 11* 1.9 2.6

2 4 8 8.8 9.2 5 3 9 4.3 4.0 0 1 11 20.8 20.5

3 4 8 7.5 7.8 6 3 9 7.0 6.6 1 1 11 21.2 20.9

4 4 8 10.3 10.8 7 3 9* 2.3 2.1 2 1 11 16.3 16.4

0 5 8 14.9 15.4 0 4 9 15.6 15.9 3 1 11 15.3 15.6

1 5 8 9.7 9.9 4 4 9 10.0 9.7 4 1 11 12.0 12.1

2 5 8 13.9 14.2 5 4 9 5.4 5.5 5 1 11 8.9 9.0

3 5 8 8.6 8.7 6 4 9 5.1 5.2 6 1 11 7.7 7.8

4 5 8 4.3 4.2 5 5 9* 2.1 .7 7 1 11 5.1 5.2

5 5 8 8.4 8.4 6 5 9 3.4 3.0 8 1 11 4.2 3.9

0 6 8 14.6 15.0 0 6 9 9.7 10.0 2 2 11 14.7 14.9

1 6 8 5.9 6.3 0 8 9* 3.0 2.5 3 2 11 9.4 9.7

2 6 8 6.9 6.9 0 0 10 28.5 27.5 4 2 11 10.4 10.6

3 6 8 8.0 8.1 0 1 10 23.4 23.1 5 2 11 6.5 6.7

4 6 8 3.4 3.6 1 1 10 23.7 23.0 6 2 11 4.8 5.0

5 6 8 3.3 3.2 0 2 10 19.4 19.2 7 2 11 4.8 4.6

0 7 8 6.6 6.5 1 2 10 19.8 19.7 8 2 11* 2.3 2.2

1 7 8 9.4 9.6 2 2 10 15.3 15.5 0 3 11 11.7 11.7

2 7 8 3.5 3.5 0 3 10 23.4 23.4 3 3 11 8.9 9.0

3 7 8 4.4 4.1 1 3 10 16.3 16.0 4 3 11 8.0 8.2

4 7 8 4.6 4.5 2 3 10 14.7 14.9 5 3 11 3.9 4.2

0 8 8 6.7 6.8 3 3 10 15.4 15.2 6 3 11 5.1 5.1

1 8 8 4.0 3.6 0 4 10 11.9 12.2 7 3 11 3.0 2.6

2 8 8 7.0 6.9 1 4 10 14.0 14.3 4 4 11 6.8 6.8

 

 

 

H K L /FO/ /FC/ H K L /FO/ /FC/ H K L /FO/ /FC/

 

5 4 11 5.2 5.1 6 1 13 4.1 4.6 3 0 15 2.8 2.8

6 4 11 3.7 3.6 7 1 13 6.2 6.3 5 0 15 2.9 2.9

0 5 11 6.5 7.0 8 1 13* 2.2 2.0 7 0 15* 2.9 2.9

5 5 11* 2.5 2.4 2 2 13 19.5 19.6 1 1 15 12.1 12.0

0 7 11 5.5 5.5 3 2 13 6.8 6.9 2 1 15 13.8 13.6

0 9 11 4.1 3.7 4 2 13 6.9 7.0 3 1 15 15.0 14.6

0 0 12 25.7 25.5 5 2 13 10.9 10.9 4 1 15 6.1 6.4

0 1 12 21.2 20.7 6 2 13* 3.1 2.5 5 1 15 9.0 9.0

1 1 12 5.8 4.0 7 2 13 4.5 4.4 6 1 15 8.3 8.1

0 2 12 29.7 29.5 0 3 13 16.3 16.3 7 1 15* 2.7 2.7

1 2 12 19.4 19.2 3 3 13 10.2 10.3 0 2 15 8.5 8.6

2 2 12 7.6 7.6 4 3 13 5.8 5.8 2 2 15 6.0 6.1

0 3 12 13.5 13.8 5 3 13* 1.4 1.8 3 2 15 6.3 6.5

1 3 12 13.2 12.8 6 3 13 6.3 6.2 4 2 15 10.4 10.2

2 3 12 19.6 19.7 4 4 13 8.4 7.9 5 2 15* 1.7 1.0

3 3 12 4.7 4.2 5 4 13 3.8 4.1 6 2 15 5.5 5.3

0 4 12 15.1 15.2 6 4 13* 2.3 1.8 3 3 15 5.1 4.8

1 4 12 4.1 3.9 0 5 13 6.0 6.0 4 3 15 7.0 7.1

2 4 12 10.1 9.9 5 5 13 4.0 4.1 5 3 15 3.8 3.5

3 4 12 9.8 10.1 0 7 13 5.8 5.6 6 3 15 3.5 3.0

4 4 12* 3.2 1.2 0 0 14 24.7 24.5 0 4 15 11.1 11.4

0 5 12 21.0 21.0 0 1 14 13.1 13.0 4 4 15 4.6 4.5

1 5 12 9.7 10.0 1 1 14 15.7 15.8 5 4 15 4.6 4.6

2 5 12 6.9 7.1 0 2 14 15.4 15.3 0 6 15 3.8 4.1

3 5 12 10.5 10.5 1 2 14 11.6 11.8 0 8 15* 1.9 2.3

4 5 12 6.3 6.2 2 2 14 14.3 14.2 0 0 16 14.0 13.4

5 5 12 4.6 4.7 0 3 14 18.1 18.0 0 1 16 12.4 12.5

0 6 12* 3.0 3.2 1 3 14 8.7 8.9 1 1 16 13.5 13.2

1 6 12 6.6 6.6 2 3 14 10.6 10.8 0 2 16 9.3 9.7

2 6 12 7.6 7.5 3 3 14 10.8 10.8 1 2 16 10.9 11.0

3 6 12* 1.7 .8 0 4 14 9.2 9.1 2 2 16 9.1 9.0

4 6 12 4.3 3.9 1 4 14 11.0 11.1 0 3 16 13.0 13.0

0 7 12 11.7 11.6 2 4 14 6.4 6.6 1 3 16 9.9 9.6

1 7 12* 2.1 1.8 3 4 14 5.8 5.9 2 3 16 8.2 8.4

2 7 12 6.8 6.4 4 4 14 6.4 6.3 3 3 16 10.2 9.9

3 7 12 6.0 6.1 0 5 14 10.5 10.7 0 4 16 6.9 7.1

0 8 12 8.5 8.3 1 5 14 6.4 6.7 1 4 16 9.0 9.1

1 8 12 4.0 3.7 2 5 14 9.1 9.0 2 4 16 6.0 6.0

0 9 12* 1.9 1.8 3 5 14 6.1 6.3 3 4 16 4.7 4.8

0 0 13 23.4 22.9 4 5 14 3.5 3.6 4 4 16 5.9 5.8

2 0 13 12.6 12.8 0 6 14 9.0 8.9 0 5 16 6.8 7.2

4 0 13 10.0 10.2 1 6 14 4.5 4.6 1 5 16 7.3 7.1

6 0 13 9.4 9.7 2 6 14 4.9 5.0 2 5 16 5.5 5.5

8 0 13* 2.2 1.0 3 6 14 5.0 4.8 3 5 16 6.0 6.0

0 1 13 11.8 11.9 0 7 14 5.5 5.5 0 6 16 7.5 7.5

1 1 13 22.4 21.7 1 7 14 5.7 5.7 1 6 16 4.5 4.8

2 1 13 9.8 9.8 2 7 14 3.0 3.2 2 6 16 5.1 5.0

3 1 13 9.0 8.5 0 8 14 5.1 5.1 0 7 16* 3.1 2.8

4 1 13 14.3 14.2 0 0 15 2.2 2.3 1 7 16 5.2 5.3

5 1 13 5.0 4.7 1 0 15 17.0 16.9 0 0 17 3.2 3.5

 

 

 

H K L /FO/ /FC/ H K L /FO/ /FC/ H K L /FO/ /FC/

 

2 0 17 8.5 9.0 4 4 18* 3.8 3.8 1 4 20* 1.9 1.7

4 0 17 8.6 8.9 0 5 18 9.8 9.8 2 4 20 5.5 5.9

6 0 17 3.2 3.1 1 5 18 3.6 3.9 0 5 20 8.3 8.6

0 1 17 12.5 12.5 2 5 18 7.9 8.1 1 5 20 5.1 5.6

1 1 17 8.3 8.4 0 6 18 5.5 6.0 0 0 21* 2.0 3.0

2 1 17 10.5 10.6 1 6 18* 2.4 2.3 2 0 21 3.4 3.3

3 1 17 10.2 10.3 0 0 19 12.5 12.5 4 0 21 4.6 5.1

4 1 17 4.8 5.1 1 0 19 5.9 6.1 0 1 21 7.1 7.0

5 1 17 6.6 6.7 3 0 19 8.7 8.8 1 1 21 9.0 9.2

6 1 17 5.8 5.9 5 0 19 3.8 4.0 2 1 21 5.6 5.6

2 2 17 5.5 5.5 1 1 19 10.8 10.7 3 1 21 6.2 6.4

3 2 17 6.6 6.7 2 1 19 5.4 5.4 4 1 21 5.6 5.9

4 2 17 6.9 7.4 3 1 19 4.9 4.6 2 2 21 5.9 6.2

5 2 17* 2.2 2.2 4 1 19 7.7 7.8 3 2 21* 2.4 2.4

6 2 17 3.7 4.0 5 1 19 2.8 2.8 0 3 21 4.0 4.3

0 3 17 4.3 4.2 0 2 19 7.3 7.5 3 3 21 4.5 4.7

3 3 17 3.7 3.8 2 2 19 10.6 10.6 0 5 21* 1.5 .8

4 3 17 5.9 5.9 3 2 19 4.0 4.3 0 0 22 6.2 6.6

5 3 17 3.8 3.5 4 2 19 4.0 4.1 0 1 22 6.3 6.5

4 4 17 3.2 3.0 5 2 19 6.2 6.4 1 1 22 6.9 7.1

0 5 17 4.4 4.9 3 3 19 5.6 5.6 0 2 22 4.5 4.7

0 7 17 3.6 3.8 4 3 19 3.4 3.7 1 2 22 5.4 5.8

0 0 18 20.5 20.0 0 4 19 5.6 5.8 2 2 22 4.3 4.8

0 1 18 7.4 7.4 0 6 19 5.1 5.4 0 3 22 6.5 6.8

1 1 18 9.3 9.4 0 0 20 6.3 6.5 1 3 22 5.2 5.3

0 2 18 11.8 11.9 0 1 20 9.7 9.9 2 3 22 3.9 4.5

1 2 18 7.1 7.3 1 1 20 2.1 2.1 0 4 22 3.4 3.8

2 2 18 10.2 10.2 0 2 20 11.6 11.7 0 0 23* 1.7 2.5

0 3 18 13.7 13.9 1 2 20 9.0 9.2 1 0 23 5.8 5.9

1 3 18 4.8 4.5 2 2 20* 2.7 2.7 3 0 23 2.6 3.1

2 3 18 8.4 8.6 0 3 20 3.9 4.0 1 1 23 5.2 5.6

3 3 18 7.2 7.3 1 3 20 7.1 7.4 2 1 23 4.6 5.0

0 4 18 5.4 5.8 2 3 20 8.2 8.6 0 2 23 3.3 3.7

1 4 18 7.3 7.5 3 3 20* 1.2 1.8 0 0 24 9.8 10.4

2 4 18 3.7 3.6 0 4 20 7.7 7.8 0 1 24 3.0 3.5

3 4 18 3.9 4.1

 

Crystal Pep2

H K L /FO/ /FC/ H K L /FO/ /FC/ H K L /FO/ /FC/

 

1 0 0 25.5 23.2 1 1 2 39.1 37.0 2 2 4 22.7 23.2

2 0 0 62.8 60.1 2 1 2 44.8 43.6 3 2 4 28.5 28.6

3 0 0 73.2 70.2 3 1 2 33.2 32.5 4 2 4 19.7 20.4

4 0 0 22.4 21.1 4 1 2 19.6 19.7 5 2 4 12.8 13.4

5 0 0 34.7 33.6 5 1 2 22.1 22.2 3 3 4 21.6 21.5

6 0 0 25.6 25.1 6 1 2 15.9 15.9 4 3 4 15.3 16.2

7 0 0 16.7 17.2 2 2 2 24.3 24.5 5 3 4 16.8 16.3

1 1 0 65.6 64.3 3 2 2 32.5 32.2 4 4 4 12.2 13.4

2 1 0 29.3 27.6 4 2 2 21.7 21.9 0 0 5 49.0 50.2

3 1 0 18.5 19.9 5 2 2 13.5 13.3 1 0 5 28.9 31.0

4 1 0 33.7 32.7 3 3 2 20.2 19.8 2 0 5 24.0 24.5

5 1 0 13.2 13.4 4 3 2 18.1 18.0 3 0 5 32.7 33.8

6 1 0 9.7 8.4 5 3 2 17.9 17.8 4 0 5 21.1 21.9

2 2 0 50.7 49.7 4 4 2 11.3 11.5 5 0 5 10.9 11.4

3 2 0 31.6 30.7 0 0 3* 3.3 3.9 6 0 5 19.9 20.0

4 2 0 13.7 12.0 1 0 3 49.2 50.2 1 1 5 52.2 54.1

5 2 0 31.2 31.3 2 0 3 12.5 12.7 2 1 5 24.7 24.8

3 3 0 31.6 32.0 3 0 3 22.6 22.3 3 1 5 23.4 24.0

4 3 0 12.8 13.6 4 0 3 26.6 26.6 4 1 5 29.3 29.8

5 3 0 15.0 15.2 5 0 3 5.4 5.7 5 1 5 12.7 13.7

4 4 0 17.6 16.6 6 0 3 17.5 18.0 6 1 5 11.3 12.0

1 0 1 59.5 55.3 7 0 3 5.5 6.0 2 2 5 37.6 38.3

2 0 1 51.6 48.9 1 1 3 67.5 66.3 3 2 5 14.5 15.1

3 0 1 22.6 20.8 2 1 3 35.4 35.8 4 2 5 15.9 16.2

4 0 1 33.4 32.3 3 1 3 37.7 37.0 5 2 5 18.0 19.0

5 0 1 20.0 19.5 4 1 3 28.4 28.7 3 3 5 22.6 23.4

6 0 1 13.0 13.2 5 1 3 20.2 20.2 4 3 5 12.3 13.0

7 0 1 15.2 15.2 6 1 3 16.8 17.7 0 0 6 69.4 72.1

1 1 1 33.3 34.0 2 2 3 32.3 32.1 1 0 6 32.5 34.1

2 1 1 40.5 38.6 3 2 3 13.7 14.3 2 0 6 50.9 51.4

3 1 1 34.4 34.0 4 2 3 23.2 24.0 3 0 6 37.9 38.4

4 1 1 22.1 20.8 5 2 3 9.7 9.8 4 0 6 23.2 23.9

5 1 1 19.1 19.1 3 3 3 22.9 21.9 5 0 6 31.8 32.8

6 1 1 16.4 16.2 4 3 3 15.7 15.5 6 0 6 12.1 13.6

2 2 1 29.8 28.5 5 3 3 9.0 7.9 1 1 6 23.0 25.4

3 2 1 24.4 23.9 4 4 3 18.0 18.6 2 1 6 30.7 30.9

4 2 1 23.1 22.7 0 0 4 31.1 33.5 3 1 6 20.4 22.2

5 2 1 14.6 14.0 1 0 4 53.4 55.1 4 1 6 16.2 16.6

3 3 1 15.3 15.6 2 0 4 42.2 42.4 5 1 6 14.8 16.0

4 3 1 19.0 18.5 3 0 4 33.0 33.5 6 1 6 9.4 11.0

5 3 1 11.6 11.1 4 0 4 24.9 25.8 2 2 6 25.3 25.6

4 4 1 12.2 10.9 5 0 4 24.4 24.9 3 2 6 31.0 31.1

0 0 2 46.6 49.1 6 0 4 15.5 16.5 4 2 6 15.3 15.3

1 0 2 61.9 61.4 7 0 4 11.0 11.7 5 2 6 18.4 19.0

2 0 2 50.8 49.4 1 1 4 33.4 32.5 3 3 6 16.8 18.1

3 0 2 37.0 36.7 2 1 4 39.9 41.0 4 3 6 15.4 15.8

4 0 2 28.7 28.6 3 1 4 31.0 31.1 0 0 7 18.2 18.7

5 0 2 29.1 29.0 4 1 4 20.5 21.1 1 0 7 37.3 38.8

6 0 2 15.3 15.2 5 1 4 20.1 20.8 2 0 7 36.6 37.2

7 0 2 14.5 14.2 6 1 4 13.7 14.9 3 0 7 11.3 11.8

 

 

 

H K L /FO/ /FC/ H K L /FO/ /FC/ H K L /FO/ /FC/

 

4 0 7 27.5 28.2 2 1 9 24.0 24.9 2 0 12 31.4 30.1

5 0 7 18.6 19.7 3 1 9 25.3 25.3 3 0 12 16.6 16.3

6 0 7 5.3 7.2 4 1 9 18.7 19.9 4 0 12 17.5 17.7

1 1 7 19.2 20.9 5 1 9 14.9 15.2 5 0 12 23.7 22.5

2 1 7 30.7 31.5 2 2 9 19.9 21.3 1 1 12 8.1 9.9

3 1 7 27.7 28.7 3 2 9 11.4 11.9 2 1 12 21.8 21.6

4 1 7 11.2 11.6 4 2 9 17.2 17.9 3 1 12 16.0 16.9

5 1 7 16.2 17.5 3 3 9 15.8 15.6 4 1 12 6.4 6.9

6 1 7 14.7 14.9 4 3 9 11.9 12.1 2 2 12 9.7 10.3

2 2 7 17.1 17.3 0 0 10 29.9 29.9 3 2 12 21.8 21.5

3 2 7 21.8 22.5 1 0 10 26.3 26.5 0 0 13 24.4 24.1

4 2 7 19.8 20.4 2 0 10 22.0 22.8 1 0 13 15.1 15.1

5 2 7 8.9 9.1 3 0 10 25.0 25.6 2 0 13 15.9 15.6

3 3 7 7.1 9.3 4 0 10 15.4 16.2 3 0 13 18.8 18.5

4 3 7 16.3 17.4 5 0 10 15.0 15.4 4 0 13 12.7 12.6

0 0 8 51.6 53.1 1 1 10 26.4 25.9 1 1 13 23.5 23.5

1 0 8 25.8 26.4 2 1 10 23.3 23.5 2 1 13 13.6 12.8

2 0 8 28.3 29.2 3 1 10 19.8 19.5 3 1 13 11.9 12.6

3 0 8 37.0 37.4 4 1 10 16.8 17.8 4 1 13 16.2 15.9

4 0 8 17.1 17.4 5 1 10 14.3 14.3 2 2 13 22.1 20.5

5 0 8 18.5 19.6 2 2 10 18.6 19.4 3 2 13 10.0 10.2

6 0 8 17.8 18.2 3 2 10 16.7 17.8 0 0 14 27.9 26.4

1 1 8 33.8 35.2 4 2 10 13.1 14.1 1 0 14 14.7 14.9

2 1 8 22.8 23.7 3 3 10 17.3 17.8 2 0 14 18.4 17.4

3 1 8 17.2 18.0 0 0 11 17.4 16.5 3 0 14 21.1 20.0

4 1 8 22.5 23.0 1 0 11 23.4 23.4 4 0 14 10.6 11.3

5 1 8 13.2 13.5 2 0 11 17.5 17.5 1 1 14 17.8 17.7

2 2 8 28.0 28.8 3 0 11 14.8 15.4 2 1 14 13.8 13.8

3 2 8 19.7 20.4 4 0 11 15.9 16.7 3 1 14 10.8 11.0

4 2 8 12.1 13.2 5 0 11 8.9 9.7 2 2 14 17.7 16.4

5 2 8 17.4 17.8 1 1 11 24.7 25.0 0 0 15 6.4 4.2

3 3 8 21.9 22.3 2 1 11 19.0 19.4 1 0 15 18.9 18.0

4 3 8 10.7 11.5 3 1 11 18.0 18.8 2 0 15 11.2 12.0

0 0 9 6.9 8.2 4 1 11 15.2 15.6 3 0 15* 2.7 6.1

1 0 9 31.1 31.4 2 2 11 17.9 18.3 1 1 15 14.4 13.2

2 0 9 15.1 15.6 3 2 11 12.4 12.6 2 1 15 15.7 15.4

3 0 9 15.1 15.0 4 2 11 13.6 13.6 0 0 16 16.7 15.2

4 0 9 18.8 19.7 3 3 11 11.2 12.4 1 0 16 14.7 13.7

5 0 9 5.0 6.0 0 0 12 27.3 26.0 2 0 16 12.4 11.7

6 0 9 12.9 13.4 1 0 12 23.6 23.4 1 1 16 16.1 14.4

1 1 9 33.2 33.4