data_NH4-NAT_publ _pd_block_id 2010-12-15T23:07|NH4-NAT|NH4-NAT| _audit_creation_method "from EXP file using GSAS2CIF" _audit_creation_date 2010-12-15T23:07 _audit_author_name NH4-NAT _audit_update_record ; 2010-12-15T23:07 Initial CIF as created by GSAS2CIF ; #============================================================================= # this information describes the project, paper etc. for the CIF # # Acta Cryst. Section C papers and editorial correspondence is generated # # from the information in this section # # # # (from) CIF submission form for Rietveld refinements (Acta Cryst. C) # # Version 14 December 1998 # #============================================================================= # 1. SUBMISSION DETAILS _publ_contact_author_name ? # Name of author for correspondence _publ_contact_author_address # Address of author for correspondence ; ? ; _publ_contact_author_email ? _publ_contact_author_fax ? _publ_contact_author_phone ? _publ_contact_letter ; ? ; _publ_requested_journal ? _publ_requested_coeditor_name ? _publ_requested_category ? # Acta C: one of CI/CM/CO/FI/FM/FO #============================================================================== # 2. PROCESSING SUMMARY (IUCr Office Use Only) _journal_data_validation_number ? _journal_date_recd_electronic ? _journal_date_to_coeditor ? _journal_date_from_coeditor ? _journal_date_accepted ? _journal_date_printers_first ? _journal_date_printers_final ? _journal_date_proofs_out ? _journal_date_proofs_in ? _journal_coeditor_name ? _journal_coeditor_code ? _journal_coeditor_notes ; ? ; _journal_techeditor_code ? _journal_techeditor_notes ; ? ; _journal_coden_ASTM ? _journal_name_full ? _journal_year ? _journal_volume ? _journal_issue ? _journal_page_first ? _journal_page_last ? _journal_paper_category ? _journal_suppl_publ_number ? _journal_suppl_publ_pages ? #============================================================================== # 3. TITLE AND AUTHOR LIST _publ_section_title ; ? ; _publ_section_title_footnote ; ? ; # The loop structure below should contain the names and addresses of all # authors, in the required order of publication. Repeat as necessary. loop_ _publ_author_name _publ_author_footnote _publ_author_address ? #<--'Last name, first name' ; ? ; ; ? ; #============================================================================== # 4. TEXT _publ_section_synopsis ; ? ; _publ_section_abstract ; ? ; _publ_section_comment ; ? ; _publ_section_exptl_prep # Details of the preparation of the sample(s) # should be given here. ; ? ; _publ_section_exptl_refinement ; ? ; _publ_section_references ; ? ; _publ_section_figure_captions ; ? ; _publ_section_acknowledgements ; ? ; #============================================================================= # 5. OVERALL REFINEMENT & COMPUTING DETAILS _refine_special_details ; ? ; _pd_proc_ls_special_details ; ? ; # The following items are used to identify the programs used. _computing_molecular_graphics ? _computing_publication_material ? _refine_ls_weighting_scheme ? _refine_ls_weighting_details ? _refine_ls_hydrogen_treatment ? _refine_ls_extinction_method ? _refine_ls_extinction_coef ? _refine_ls_number_constraints ? _refine_ls_restrained_S_all ? _refine_ls_restrained_S_obs ? #============================================================================== # 6. SAMPLE PREPARATION DATA # (In the unusual case where multiple samples are used in a single # Rietveld study, this information should be moved into the phase # blocks) # The following three fields describe the preparation of the material. # The cooling rate is in K/min. The pressure at which the sample was # prepared is in kPa. The temperature of preparation is in K. _pd_prep_cool_rate ? _pd_prep_pressure ? _pd_prep_temperature ? _pd_char_colour ? # use ICDD colour descriptions _refine_ls_shift/su_max 10.06 _refine_ls_shift/su_mean 1.51 _computing_structure_refinement GSAS _refine_ls_number_parameters 45 _refine_ls_goodness_of_fit_all 3.74 _refine_ls_number_restraints 28 _refine_ls_matrix_type full #============================================================================== # 7. CHEMICAL, STRUCTURAL AND CRYSTAL DATA _pd_char_particle_morphology ? _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_formula_moiety ? _chemical_formula_structural ? _chemical_formula_analytical ? _chemical_melting_point ? _chemical_compound_source ? # for minerals and # natural products _symmetry_space_group_name_Hall ? _exptl_crystal_F_000 ? _exptl_crystal_density_diffrn ? _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _cell_measurement_temperature ? _cell_special_details ; ? ; _geom_special_details ? # The following item identifies the program(s) used (if appropriate). _computing_structure_solution ? #============================================================================== # 8. Phase information from GSAS _pd_phase_name NH4-NAT _cell_length_a 19.84234(15) _cell_length_b 20.06522(15) _cell_length_c 6.51942(5) _cell_angle_alpha 90.0 _cell_angle_beta 90.0 _cell_angle_gamma 90.0 _cell_volume 2595.65(4) _symmetry_cell_setting orthorhombic _symmetry_space_group_name_H-M "F d d 2" loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz 1 +x,+y,+z 2 -x+1/4,+y+1/4,+z+1/4 3 +x+1/4,-y+1/4,+z+1/4 4 -x,-y+1/2,+z+1/2 101 +x,+y+1/2,+z+1/2 102 -x+1/4,+y+3/4,+z+3/4 103 +x+1/4,-y+3/4,+z+3/4 104 -x,-y,+z 201 +x+1/2,+y,+z+1/2 202 -x+3/4,+y+1/4,+z+3/4 203 +x+3/4,-y+1/4,+z+3/4 204 -x+1/2,-y+1/2,+z 301 +x+1/2,+y+1/2,+z 302 -x+3/4,+y+3/4,+z+1/4 303 +x+3/4,-y+3/4,+z+1/4 304 -x+1/2,-y,+z+1/2 # ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_occupancy _atom_site_thermal_displace_type _atom_site_U_iso_or_equiv _atom_site_symmetry_multiplicity Si Si1 0.0 0.0 -0.0177(10) 1.0 Uiso 0.0154(4) 8 Si Si2 0.17335(10) 0.18978(11) 0.6015(8) 1.0 Uiso 0.0154(4) 16 Al Al 0.05926(11) 0.07292(10) 0.5952(8) 1.0 Uiso 0.0154(4) 16 O O1 0.04726(19) 0.04706(20) 0.8475(9) 1.0 Uiso 0.0158(7) 16 O O2 0.11078(16) 0.14124(17) 0.5845(13) 1.0 Uiso 0.0158(7) 16 O O3 0.09610(15) 0.00861(18) 0.4572(9) 1.0 Uiso 0.0158(7) 16 O O4 0.22994(16) 0.15604(16) 0.7453(10) 1.0 Uiso 0.0158(7) 16 O O5 0.20355(21) 0.20319(20) 0.3732(8) 1.0 Uiso 0.0158(7) 16 N N1A 0.1701(8) 0.0815(11) 0.0872(27) 0.73(6) Uiso 0.0251(24) 16 N N1B 0.1550(23) 0.1047(34) 0.111(8) 0.27(6) Uiso 0.0251(24) 16 O OW1A 0.2371(6) 0.0038(14) 0.5741(28) 0.447(34) Uiso 0.0224(24) 16 O OW1B 0.2452(7) 0.0347(15) 0.5438(29) 0.432(32) Uiso 0.0224(24) 16 # If you change Z, be sure to change all 3 of the following _chemical_formula_sum "Al2 N2.00 O11.76 Si3" _chemical_formula_weight 354.33 _cell_formula_units_Z 8 # MOLECULAR GEOMETRY loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_publ_flag Si1 O1 1.5947(21) . 1_554 N Si1 O1 1.5947(21) . 104_554 N Si1 O3 3.640(6) . 1_555 N Si1 O3 3.640(6) . 104_555 N Si1 O5 1.6046(22) . 102_544 N Si1 O5 1.6046(22) . 203_454 N Si2 O2 1.5818(26) . 1_555 N Si2 O3 1.5909(27) . 2_555 N Si2 O3 3.646(4) . 3_555 N Si2 O4 1.6116(27) . 1_555 N Si2 O5 1.6272(29) . 1_555 N Si2 O5 3.577(4) . 204_555 N Si2 OW1B 3.444(24) . 1_555 N Al O1 1.7416(29) . 1_555 N Al O1 3.601(4) . 104_555 N Al O2 1.7115(26) . 1_555 N Al O3 1.7345(27) . 1_555 N Al O3 3.604(4) . 104_555 N Al O4 3.499(4) . 102_544 N Al O4 1.7549(26) . 203_454 N Al O5 3.761(5) . 203_454 N Al OW1B 3.693(23) . 203_454 N O1 Si1 1.5947(21) . 1_556 N O1 Al 1.7416(29) . 1_555 N O1 Al 3.601(4) . 104_555 N O1 O1 2.662(7) . 104_555 N O1 O2 2.846(5) . 1_555 N O1 O3 2.830(6) . 1_555 N O1 O3 4.163(6) . 1_556 N O1 O3 3.977(6) . 104_555 N O1 O4 4.286(5) . 1_555 N O1 O4 3.684(6) . 102_544 N O1 O4 2.819(5) . 203_454 N O1 O5 2.6033(32) . 102_545 N O1 O5 2.5858(32) . 203_455 N O1 N1A 2.977(12) . 1_556 N O1 N1B 2.98(4) . 1_556 N O1 OW1A 4.256(14) . 1_555 N O1 OW1A 4.207(30) . 2_555 N O2 Si2 1.5818(26) . 1_555 N O2 Al 1.7115(26) . 1_555 N O2 O1 2.846(5) . 1_555 N O2 O3 2.803(5) . 1_555 N O2 O3 2.630(4) . 2_555 N O2 O4 2.603(4) . 1_555 N O2 O4 2.825(4) . 203_454 N O2 O5 2.614(5) . 1_555 N O2 OW1A 3.727(20) . 1_555 N O2 OW1A 3.364(22) . 2_555 N O2 OW1A 3.652(21) . 203_454 N O2 OW1B 3.429(16) . 1_555 N O2 OW1B 3.816(25) . 2_555 N O2 OW1B 3.326(18) . 203_454 N O3 Si1 3.640(6) . 1_555 N O3 Si2 1.5909(27) . 102_544 N O3 Si2 3.646(4) . 203_454 N O3 Al 1.7345(27) . 1_555 N O3 Al 3.604(4) . 104_555 N O3 O1 4.163(6) . 1_554 N O3 O1 2.830(6) . 1_555 N O3 O1 3.977(6) . 104_555 N O3 O2 2.803(5) . 1_555 N O3 O2 2.630(4) . 102_544 N O3 O3 3.829(6) . 104_555 N O3 O4 2.564(5) . 102_544 N O3 O4 2.882(4) . 203_454 N O3 O5 2.636(5) . 102_544 N O3 O5 3.651(6) . 203_454 N O3 N1A 3.180(15) . 1_555 N O3 N1B 3.19(5) . 1_555 N O3 OW1A 2.901(12) . 1_555 N O3 OW1A 4.154(13) . 304_554 N O3 OW1B 3.057(16) . 1_555 N O3 OW1B 4.235(15) . 304_554 N O4 Si2 1.6116(27) . 1_555 N O4 Al 3.499(4) . 2_555 N O4 Al 1.7549(26) . 3_555 N O4 O1 4.286(5) . 1_555 N O4 O1 3.684(6) . 2_555 N O4 O1 2.819(5) . 3_555 N O4 O2 2.603(4) . 1_555 N O4 O2 2.825(4) . 3_555 N O4 O3 2.564(5) . 2_555 N O4 O3 2.882(4) . 3_555 N O4 O4 3.854(6) . 204_555 N O4 O5 2.656(6) . 1_555 N O4 O5 4.234(6) . 1_556 N O4 O5 3.950(6) . 204_555 N O4 N1A 2.936(14) . 1_556 N O4 N1B 2.99(5) . 1_556 N O4 OW1A 3.255(26) . 1_555 N O4 OW1A 3.913(22) . 304_555 N O4 OW1B 2.783(22) . 1_555 N O4 OW1B 4.322(23) . 304_555 N O5 Si1 1.6046(22) . 2_555 N O5 Si2 1.6272(29) . 1_555 N O5 Si2 3.577(4) . 204_555 N O5 Al 3.761(5) . 3_555 N O5 O1 2.6033(32) . 2_554 N O5 O1 2.5858(32) . 3_554 N O5 O2 2.614(5) . 1_555 N O5 O3 2.636(5) . 2_555 N O5 O3 3.651(6) . 3_555 N O5 O4 4.234(6) . 1_554 N O5 O4 2.656(6) . 1_555 N O5 O4 3.950(6) . 204_555 N O5 O5 2.632(7) . 204_555 N O5 N1A 3.143(21) . 1_555 N O5 N1B 2.79(6) . 1_555 N O5 OW1A 4.262(29) . 1_555 N O5 OW1B 3.654(30) . 1_555 N O5 OW1B 4.174(15) . 203_454 N N1A O1 2.977(12) . 1_554 N N1A O3 3.180(15) . 1_555 N N1A O4 2.936(14) . 1_554 N N1A O5 3.143(21) . 1_555 N N1A N1B 0.57(6) . 1_555 N N1A OW1A 2.516(32) . 304_554 N N1A OW1B 2.887(34) . 304_554 N N1B O1 2.98(4) . 1_554 N N1B O3 3.19(5) . 1_555 N N1B O4 2.99(5) . 1_554 N N1B O5 2.79(6) . 1_555 N N1B N1A 0.57(6) . 1_555 N N1B OW1A 3.06(8) . 304_554 N OW1A O1 4.256(14) . 1_555 N OW1A O1 4.207(30) . 102_544 N OW1A O2 3.727(20) . 1_555 N OW1A O2 3.652(21) . 3_555 N OW1A O2 3.364(22) . 102_544 N OW1A O3 2.901(12) . 1_555 N OW1A O3 4.154(13) . 304_555 N OW1A O4 3.255(26) . 1_555 N OW1A O4 3.913(22) . 304_554 N OW1A O5 4.262(29) . 1_555 N OW1A N1A 2.516(32) . 304_555 N OW1A N1B 3.06(8) . 304_555 N OW1A OW1A 3.303(4) . 304_554 N OW1A OW1A 3.303(4) . 304_555 N OW1A OW1B 0.669(18) . 1_555 N OW1A OW1B 3.560(31) . 304_554 N OW1A OW1B 3.177(28) . 304_555 N OW1B Si2 3.444(24) . 1_555 N OW1B Al 3.693(23) . 3_555 N OW1B O2 3.429(16) . 1_555 N OW1B O2 3.326(18) . 3_555 N OW1B O2 3.816(25) . 102_544 N OW1B O3 3.057(16) . 1_555 N OW1B O3 4.235(15) . 304_555 N OW1B O4 2.783(22) . 1_555 N OW1B O4 4.322(23) . 304_554 N OW1B O5 3.654(30) . 1_555 N OW1B O5 4.174(15) . 3_555 N OW1B N1A 2.887(34) . 304_555 N OW1B OW1A 0.669(18) . 1_555 N OW1B OW1A 3.177(28) . 304_554 N OW1B OW1A 3.560(31) . 304_555 N OW1B OW1B 3.549(23) . 304_554 N OW1B OW1B 3.549(23) . 304_555 N loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Si1 O1 113.1(4) 1_554 . 104_543 N O1 Si1 O5 108.92(14) 1_554 . 102_544 N O1 Si1 O5 107.85(14) 1_554 . 203_454 N O1 Si1 O5 107.85(14) 104_543 . 102_544 N O1 Si1 O5 108.92(14) 104_543 . 203_454 N O5 Si1 O5 110.2(4) 102_544 . 203_454 N O2 Si2 O3 111.99(22) 1_555 . 2_555 N O2 Si2 O4 109.20(25) 1_555 . 1_555 N O2 Si2 O5 109.08(30) 1_555 . 1_555 N O3 Si2 O4 106.37(27) 2_555 . 1_555 N O3 Si2 O5 110.00(27) 2_555 . 1_555 N O4 Si2 O5 110.17(29) 1_555 . 1_555 N O1 Al O2 111.01(28) 1_555 . 1_555 N O1 Al O3 109.02(28) 1_555 . 1_555 N O1 Al O4 107.44(23) 1_555 . 203_454 N O2 Al O3 108.86(26) 1_555 . 1_555 N O2 Al O4 109.15(21) 1_555 . 203_454 N O3 Al O4 111.37(24) 1_555 . 203_454 N Si1 O1 Al 141.02(33) 1_556 . 1_555 N Si2 O2 Al 163.57(32) 1_555 . 1_555 N Si2 O3 Al 140.19(24) 102_544 . 1_555 N Si2 O4 Al 137.70(24) 1_555 . 3_555 N Si1 O5 Si2 146.3(4) 2_555 . 1_555 N # Powder diffraction data for histogram 1 #============================================================================== # 9. INSTRUMENT CHARACTERIZATION _exptl_special_details ; ? ; # if regions of the data are excluded, the reason(s) are supplied here: _pd_proc_info_excluded_regions ; ? ; # The following item is used to identify the equipment used to record # the powder pattern when the diffractogram was measured at a laboratory # other than the authors' home institution, e.g. when neutron or synchrotron # radiation is used. _pd_instr_location ; ? ; _pd_calibration_special_details # description of the method used # to calibrate the instrument ; ? ; _diffrn_ambient_temperature ? _diffrn_source ? _diffrn_source_target ? _diffrn_source_type ? _diffrn_measurement_device_type ? _diffrn_detector ? _diffrn_detector_type ? # make or model of detector _pd_meas_scan_method ? # options are 'step', 'cont', # 'tof', 'fixed' or # 'disp' (= dispersive) _pd_meas_special_details ; ? ; # The following two items identify the program(s) used (if appropriate). _computing_data_collection ? _computing_data_reduction ? # Describe any processing performed on the data, prior to refinement. # For example: a manual Lp correction or a precomputed absorption correction _pd_proc_info_data_reduction ? # The following item is used for angular dispersive measurements only. _diffrn_radiation_monochromator ? # The following items are used to define the size of the instrument. # Not all distances are appropriate for all instrument types. _pd_instr_dist_src/mono ? _pd_instr_dist_mono/spec ? _pd_instr_dist_src/spec ? _pd_instr_dist_spec/anal ? _pd_instr_dist_anal/detc ? _pd_instr_dist_spec/detc ? # 10. Specimen size and mounting information # The next three fields give the specimen dimensions in mm. The equatorial # plane contains the incident and diffracted beam. _pd_spec_size_axial ? # perpendicular to # equatorial plane _pd_spec_size_equat ? # parallel to # scattering vector # in transmission _pd_spec_size_thick ? # parallel to # scattering vector # in reflection _pd_spec_mounting # This field should be # used to give details of the # container. ; ? ; _pd_spec_mount_mode ? # options are 'reflection' # or 'transmission' _pd_spec_shape ? # options are 'cylinder' # 'flat_sheet' or 'irregular' loop_ _atom_type_symbol _atom_type_number_in_cell _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source Si 24.0 0.000 0.000 6.29150 2.43860 3.03530 32.3337 1.98910 0.67850 1.54100 81.6937 1.14070 International_Tables_Vol_C Al 16.0 0.000 0.000 6.42020 3.03870 1.90020 0.74260 1.59360 31.5472 1.96460 85.0886 1.11510 International_Tables_Vol_C O 94.053 0.000 0.000 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700 32.9089 0.25080 International_Tables_Vol_C N 16.0 0.000 0.000 12.2126 0.00570 3.13220 9.89330 2.01250 28.9975 1.16630 0.58260 -11.529 International_Tables_Vol_C _diffrn_radiation_probe x-ray _diffrn_radiation_polarisn_ratio 0.95 _diffrn_radiation_wavelength 1.549 _diffrn_radiation_type ? _pd_proc_ls_prof_R_factor 0.0898 _pd_proc_ls_prof_wR_factor 0.1197 _pd_proc_ls_prof_wR_expected 0.0323 _refine_ls_R_Fsqd_factor 0.14029 _pd_proc_ls_background_function ; GSAS Background function number 2 with 3 terms. Cosine Fourier series 1: 1.00000 2: 0.00000 3: 0.00000 ; _exptl_absorpt_process_details ; GSAS Absorption/surface roughness correction: function number 0 No correction is applied. ; _exptl_absorpt_correction_T_min 1.00000 _exptl_absorpt_correction_T_max 1.00000 # Extinction correction _gsas_exptl_extinct_corr_T_min 1.00000 _gsas_exptl_extinct_corr_T_max 1.00000 _pd_proc_ls_pref_orient_corr ; March-Dollase AXIS 1 Ratio= 1.29127 h= 0.000 k= 0.000 l= 1.000 Prefered orientation correction range: Min= 0.46286, Max= 1.46986 ; _pd_proc_ls_profile_function ; CW Profile function number 3 with 19 terms Pseudovoigt profile coefficients as parameterized in P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83. Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994). J. Appl. Cryst.,27,892-900. #1(GU) = 4.211 #2(GV) = 1.547 #3(GW) = -0.074 #4(GP) = 0.000 #5(LX) = 2.298 #6(LY) = 10.951 #7(S/L) = 0.0047 #8(H/L) = 0.0188 #9(trns) = 0.00 #10(shft)= 0.0000 #11(stec)= 0.00 #12(ptec)= 0.00 #13(sfec)= 0.00 #14(L11) = 0.000 #15(L22) = 0.000 #16(L33) = 0.000 #17(L12) = 0.000 #18(L13) = 0.000 #19(L23) = 0.000 Peak tails are ignored where the intensity is below 0.0010 times the peak Aniso. broadening axis 0.0 0.0 1.0 ; _pd_proc_ls_peak_cutoff 0.00100 _pd_proc_info_datetime 2010-12-15T23:07:29 _pd_calc_method "Rietveld Refinement" #---- raw/calc data loop ----- _pd_meas_2theta_range_min 7.0 _pd_meas_2theta_range_max 127.995 _pd_meas_2theta_range_inc 0.005 _pd_proc_2theta_range_min 6.98746 _pd_proc_2theta_range_max 127.98246 _pd_proc_2theta_range_inc 0.005 loop_ _pd_meas_counts_total _pd_proc_ls_weight _pd_proc_intensity_bkg_calc _pd_calc_intensity_total 2590.0 0.0 1.00000 . 2392.0 0.0 1.00000 . 2570.0 0.0 1.00000 . 2477.0 0.0 1.00000 . 2326.0 0.0 1.00000 . 2502.0 0.0 1.00000 . 2337.0 0.0 1.00000 . 2367.0 0.0 1.00000 . 2444.0 0.0 1.00000 . 2466.0 0.0 1.00000 . 2502.0 0.0 1.00000 . 2490.0 0.0 1.00000 . 2316.0 0.0 1.00000 . 2439.0 0.0 1.00000 . 2381.0 0.0 1.00000 . 2536.0 0.0 1.00000 . 2411.0 0.0 1.00000 . 2402.0 0.0 1.00000 . 2413.0 0.0 1.00000 . 2390.0 0.0 1.00000 . 2268.0 0.0 1.00000 . 2413.0 0.0 1.00000 . 2341.0 0.0 1.00000 . 2293.0 0.0 1.00000 . 2388.0 0.0 1.00000 . 2347.0 0.0 1.00000 . 2417.0 0.0 1.00000 . 2562.0 0.0 1.00000 . 2267.0 0.0 1.00000 . 2289.0 0.0 1.00000 . 2257.0 0.0 1.00000 . 2376.0 0.0 1.00000 . 2326.0 0.0 1.00000 . 2360.0 0.0 1.00000 . 2232.0 0.0 1.00000 . 2247.0 0.0 1.00000 . 2329.0 0.0 1.00000 . 2272.0 0.0 1.00000 . 2318.0 0.0 1.00000 . 2327.0 0.0 1.00000 . 2232.0 0.0 1.00000 . 2224.0 0.0 1.00000 . 2360.0 0.0 1.00000 . 2253.0 0.0 1.00000 . 2285.0 0.0 1.00000 . 2310.0 0.0 1.00000 . 2319.0 0.0 1.00000 . 2236.0 0.0 1.00000 . 2145.0 0.0 1.00000 . 2135.0 0.0 1.00000 . 2267.0 0.0 1.00000 . 2156.0 0.0 1.00000 . 2197.0 0.0 1.00000 . 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0.000594 1175.83447 644.51440 1722.0 0.000581 1183.50952 545.33405 1630.0 0.000613 1191.18176 470.14175 1650.0 0.000606 1198.85681 412.66907 1513.0 0.000661 1206.52893 368.34607 1426.0 0.000701 1214.20105 333.94269 1503.0 0.000665 1221.87622 307.21814 1374.0 0.000728 1229.54834 286.63071 1428.0 0.000700 1237.22339 271.12448 1416.0 0.000706 1244.89551 259.98557 1477.0 0.000677 1259.88269 252.75221 1408.0 0.000710 1285.82471 249.16331 1447.0 0.000691 1311.77673 249.13394 1544.0 0.000648 1337.71875 252.75313 1577.0 0.000634 1363.66077 260.30273 1534.0 0.000652 1389.61267 272.30078 1628.0 0.000614 1415.55469 289.57349 1747.0 0.000572 1441.50659 313.35944 1824.0 0.000548 1467.44861 345.44403 1759.0 0.000569 1493.40051 388.31421 1943.0 0.000515 1519.34253 445.31091 2044.0 0.000489 1545.29443 520.72681 2014.0 0.000497 1571.23645 619.70087 2348.0 0.000426 1597.17847 747.49561 2365.0 0.000423 1623.13037 907.23004 2530.0 0.000395 1649.07239 1094.99280 2839.0 0.000352 1675.02429 1294.29749 2922.0 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101.52608 2495.0 0.000401 2438.12402 93.99224 2562.0 0.000390 2477.13696 87.31562 2731.0 0.000366 2516.16479 81.36903 2659.0 0.000376 2555.17773 76.04806 2720.0 0.000368 2594.20532 71.26634 2777.0 0.000360 2633.21826 66.95198 2738.0 0.000365 2672.24609 63.04473 2957.0 0.0003382 2711.25903 59.49382 2901.0 0.0003447 2750.28662 56.25618 2867.0 0.0003488 2780.94775 53.29513 2834.0 0.000353 2778.18506 50.57924 2816.0 0.000355 2775.42139 48.08148 2847.0 0.000351 2772.65869 45.77845 2823.0 0.000354 2769.89502 43.64989 2835.0 0.000353 2767.13232 41.67810 2750.0 0.000364 2764.36865 39.84762 2807.0 0.000356 2761.60596 38.14486 2797.0 0.000358 2758.84229 36.55785 2743.0 0.000365 2713.44312 35.07603 2764.0 0.000362 2657.38989 33.69001 2563.0 0.000390 2601.31519 32.39145 2672.0 0.000374 2545.26196 31.17292 2539.0 0.000394 2489.18726 30.02777 2527.0 0.000396 2433.13379 28.95003 2563.0 0.000390 2377.05933 27.93436 2339.0 0.000428 2321.00586 26.97592 2400.0 0.000417 2264.95264 26.07035 2351.0 0.000425 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281.40231 1080.76355 1594.0 0.000627 281.49023 1225.84326 1758.0 0.000569 281.57822 1401.47839 1908.0 0.000524 281.66620 1613.87976 2087.0 0.000479 281.75412 1869.67529 2349.0 0.000426 281.84210 2175.38452 2607.0 0.000384 281.93008 2536.39746 2992.0 0.0003342 282.01807 2955.04810 3145.0 0.0003180 282.10599 3427.18213 3490.0 0.0002865 282.19397 3936.72534 3709.0 0.0002696 282.28195 4448.93408 4027.0 0.0002483 282.36987 4906.16016 4126.0 0.0002424 282.45786 5234.04834 4244.0 0.0002356 282.54584 5364.58496 4305.0 0.0002323 282.63382 5268.09326 4214.0 0.0002373 282.72174 4969.93457 3949.0 0.0002532 282.80972 4536.21387 3582.0 0.0002792 282.89771 4042.03467 3325.0 0.0003008 282.98563 3547.08984 2949.0 0.0003391 283.07361 3088.17603 2661.0 0.000376 283.16159 2682.89160 2417.0 0.000414 283.24957 2336.38892 2087.0 0.000479 283.33749 2046.98523 2004.0 0.000499 283.42548 1809.76343 1705.0 0.000587 283.51346 1618.61572 1654.0 0.000605 283.60144 1467.34424 1596.0 0.000627 283.68936 1350.24744 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1843.97705 1946.0 0.000514 286.15237 1650.44946 1832.0 0.000546 286.24036 1492.32324 1681.0 0.000595 286.32834 1367.52234 1593.0 0.000628 286.41632 1272.46021 1524.0 0.000656 286.50424 1203.78455 1516.0 0.000660 286.59222 1158.68201 1486.0 0.000673 286.68021 1135.06445 1410.0 0.000709 286.76813 1131.68884 1542.0 0.000649 286.85611 1148.23999 1488.0 0.000672 286.94409 1185.38708 1659.0 0.000603 287.03207 1244.82019 1693.0 0.000591 287.12000 1329.26074 1890.0 0.000529 287.20798 1442.43738 1994.0 0.000502 287.29596 1589.00525 2168.0 0.000461 287.38388 1774.37854 2424.0 0.000413 287.47186 2004.41541 2653.0 0.000377 287.55984 2284.83594 2872.0 0.0003482 287.64783 2620.14185 3107.0 0.0003219 287.73572 3011.61572 3636.0 0.0002750 287.82373 3453.84326 4047.0 0.0002471 287.91171 3929.35376 4288.0 0.0002332 287.99969 4402.30469 4591.0 0.0002178 288.08759 4815.28027 4904.0 0.0002039 288.17560 5096.82275 4920.0 0.0002033 288.26358 5184.75928 4837.0 0.0002067 288.35147 5055.89209 4574.0 0.0002186 288.43945 4738.93896 4153.0 0.0002408 288.52744 4298.56543 3762.0 0.0002658 288.61545 3805.35718 3344.0 0.0002990 288.70334 3314.18457 2996.0 0.0003338 288.79132 2858.31372 2680.0 0.000373 288.87930 2453.29907 2363.0 0.000423 288.96722 2103.31519 2198.0 0.000455 289.05521 1806.29468 1891.0 0.000529 289.14319 1557.19739 1769.0 0.000565 289.23117 1349.85925 1673.0 0.000598 289.31909 1177.97705 1425.0 0.000702 289.40707 1035.62085 1319.0 0.000758 289.49506 917.48877 1239.0 0.000807 289.58298 819.01337 1108.0 0.000903 289.67096 736.37695 1026.0 0.000975 289.75894 666.46619 909.0 0.001100 289.84692 606.79236 887.0 0.001127 289.93484 555.39447 852.0 0.001174 290.02283 510.74091 766.0 0.001305 290.11081 471.63818 763.0 0.001311 290.19879 437.15381 705.0 0.001418 290.28671 406.55322 711.0 0.001406 290.37469 379.25113 677.0 0.001477 290.46268 354.77527 610.0 0.001639 290.55060 332.73926 561.0 0.001783 290.63858 312.82339 583.0 0.001715 290.72656 294.76007 587.0 0.001704 290.81454 278.32346 541.0 0.001848 290.90247 263.32147 523.0 0.001912 290.99045 249.58958 531.0 0.001883 291.07843 236.98648 479.0 0.002088 291.16635 225.38989 461.0 0.002169 291.25433 214.69370 476.0 0.002101 291.34232 204.80550 465.0 0.002151 291.43030 195.64442 427.0 0.002342 291.51822 187.13957 456.0 0.002193 291.60620 179.22847 464.0 0.002155 291.69418 171.85603 407.0 0.002457 291.78210 164.97343 448.0 0.002232 291.87009 158.53728 433.0 0.002309 291.95807 152.50899 387.0 0.002584 292.04605 146.85403 383.0 0.002611 292.13397 141.54158 428.0 0.002336 292.22195 136.54391 397.0 0.002519 292.30994 131.83612 383.0 0.002611 292.39792 127.39574 421.0 0.002375 292.48584 123.20247 394.0 0.002538 292.57382 119.23798 356.0 0.002809 292.66180 115.48559 381.0 0.002625 292.74973 111.93018 395.0 0.002532 292.83771 108.55794 377.0 0.002653 292.92569 105.35632 387.0 0.002584 293.01367 102.31384 381.0 0.002625 293.10159 99.41998 383.0 0.002611 293.18958 96.66512 399.0 0.002506 293.27756 94.04041 320.0 0.003125 293.36548 91.53772 338.0 0.002959 293.45346 90.01653 339.0 0.002950 293.54144 87.74374 358.0 0.002793 293.62943 85.57233 357.0 0.002801 293.71735 83.49641 334.0 0.002994 293.80533 81.51055 349.0 0.002865 293.89331 79.60966 363.0 0.002755 293.98123 77.78911 369.0 0.002710 294.06921 76.04454 359.0 0.002786 294.15720 74.37189 384.0 0.002604 294.24518 72.76743 370.0 0.002703 294.33310 70.44730 322.0 0.003106 294.42108 68.97579 384.0 0.002604 294.50906 67.56256 400.0 0.002500 294.59705 66.20477 301.0 0.003322 294.68497 64.89974 317.0 0.003155 294.77295 63.64501 344.0 0.002907 294.86093 62.43824 307.0 0.003257 294.94885 61.27726 331.0 0.003021 295.03683 60.16002 326.0 0.003067 295.12482 59.08461 340.0 0.002941 295.21280 58.04924 300.0 0.003333 295.30072 57.05220 363.0 0.002755 295.38870 56.09193 317.0 0.003155 295.47668 55.16693 353.0 0.002833 295.56461 54.27579 316.0 0.003165 295.65259 53.41722 344.0 0.002907 295.74057 52.58996 330.0 0.003030 295.82855 49.93595 346.0 0.002890 295.91644 49.18421 322.0 0.003106 296.00446 48.46028 348.0 0.002874 296.09244 47.76320 326.0 0.003067 296.18033 47.09206 321.0 0.003115 296.26831 46.44600 335.0 0.002985 296.35632 45.82423 331.0 0.003021 296.44431 45.22600 341.0 0.002933 296.53220 44.65059 351.0 0.002849 296.62018 44.09734 344.0 0.002907 296.70816 43.56563 304.0 0.003289 296.79617 43.05490 339.0 0.002950 296.88406 42.56457 307.0 0.003257 296.97205 42.09417 350.0 0.002857 297.06003 41.64322 349.0 0.002865 297.14795 41.21127 335.0 0.002985 297.23593 40.79792 293.0 0.003413 297.32391 40.40283 333.0 0.003003 297.41190 40.02563 327.0 0.003058 297.49982 39.66601 328.0 0.003049 297.58780 39.32371 306.0 0.003268 297.67578 38.99847 332.0 0.003012 297.76370 38.69006 317.0 0.003155 297.85168 38.39830 327.0 0.003058 297.93967 38.12300 339.0 0.002950 298.00049 37.86406 314.0 0.003185 297.95313 37.62133 348.0 0.002874 297.90570 37.39475 347.0 0.002882 297.85831 37.18426 313.0 0.003195 297.81094 36.98983 315.0 0.003175 297.76352 36.81147 320.0 0.003125 297.71613 36.64920 314.0 0.003185 297.66870 36.50309 333.0 0.003003 297.62134 36.37323 314.0 0.003185 297.57391 36.25975 347.0 0.002882 297.52652 36.16280 342.0 0.002924 297.47910 36.08257 367.0 0.002725 297.43173 36.01929 340.0 0.002941 297.38431 35.97322 338.0 0.002959 297.33691 35.94468 313.0 0.003195 297.28952 35.93399 331.0 0.003021 297.24213 35.94154 298.0 0.003356 297.19470 35.96778 326.0 0.003067 297.14731 36.01319 338.0 0.002959 297.09991 36.07829 282.0 0.00355 297.05252 36.16368 348.0 0.002874 297.00510 36.27000 334.0 0.002994 296.95773 36.39797 318.0 0.003145 296.91031 36.54838 355.0 0.002817 296.86292 36.72208 344.0 0.002907 296.81549 36.91999 328.0 0.003049 296.76813 37.14316 338.0 0.002959 296.72073 37.39269 321.0 0.003115 296.67331 37.66981 313.0 0.003195 296.62595 37.97584 339.0 0.002950 296.57852 38.31224 305.0 0.003279 296.53113 38.68061 335.0 0.002985 296.48370 39.08266 347.0 0.002882 296.43634 39.52030 341.0 0.002933 296.38892 39.99559 330.0 0.003030 296.34152 40.51081 333.0 0.003003 296.29410 41.06844 348.0 0.002874 296.24673 41.67119 326.0 0.003067 296.19931 42.32206 349.0 0.002865 296.15192 43.02432 349.0 0.002865 296.10452 43.78158 351.0 0.002849 296.05713 44.59782 317.0 0.003155 296.00970 45.47743 327.0 0.003058 295.96231 46.42524 358.0 0.002793 295.91492 47.44662 310.0 0.003226 295.86752 48.54753 377.0 0.002653 295.82010 49.73453 308.0 0.003247 295.77274 51.01500 358.0 0.002793 295.72531 52.39711 357.0 0.002801 295.67792 53.89001 344.0 0.002907 295.63049 51.67322 350.0 0.002857 295.58313 53.45335 366.0 0.002732 295.53574 55.37851 386.0 0.002591 295.48831 57.46331 364.0 0.002747 295.44095 59.72425 401.0 0.002494 295.39352 62.18007 341.0 0.002933 295.34613 64.85207 377.0 0.002653 295.29871 67.76456 365.0 0.002740 295.25134 70.94539 375.0 0.002667 295.20392 74.42651 378.0 0.002646 295.15652 78.24481 373.0 0.002681 295.10910 82.44296 411.0 0.002433 295.06174 87.07062 384.0 0.002604 295.01431 92.18586 433.0 0.002309 294.96692 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1476.57227 1422.0 0.000703 293.59232 1356.60706 1376.0 0.000727 293.54492 1212.87488 1251.0 0.000799 293.49753 1063.70020 1241.0 0.000806 293.45010 921.41943 1092.0 0.000916 293.40274 792.62970 999.0 0.001001 293.35535 679.86584 925.0 0.001081 293.30792 583.26532 895.0 0.001117 293.26050 501.69397 726.0 0.001377 293.21313 433.49167 771.0 0.001297 293.16574 376.82208 659.0 0.001517 293.11832 329.88559 632.0 0.001582 293.07095 291.02628 578.0 0.001730 293.02353 258.78372 594.0 0.001684 292.97614 231.91156 470.0 0.002128 292.92871 209.37466 534.0 0.001873 292.88135 190.33231 493.0 0.002028 292.83392 174.11369 494.0 0.002024 292.78653 160.19023 475.0 0.002105 292.73911 148.14838 451.0 0.002217 292.69174 137.66496 427.0 0.002342 292.64432 128.48648 416.0 0.002404 292.59692 120.41252 351.0 0.002849 292.54953 109.53210 410.0 0.002439 292.50214 103.25001 406.0 0.002463 292.45471 97.67599 426.0 0.002347 292.40732 92.72227 427.0 0.002342 292.35995 88.31554 377.0 0.002653 292.31253 84.39422 388.0 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290.89053 94.86289 435.0 0.002299 290.84314 100.25619 447.0 0.002237 290.79575 106.42520 456.0 0.002193 290.74832 113.50582 490.0 0.002041 290.70096 121.66989 460.0 0.002174 290.65353 131.13623 534.0 0.001873 290.60614 142.18454 528.0 0.001894 290.55872 155.17201 540.0 0.001852 290.51135 170.55156 588.0 0.001701 290.46393 188.89069 597.0 0.001675 290.41653 210.88831 644.0 0.001553 290.36911 237.38672 673.0 0.001486 290.32175 269.37454 659.0 0.001517 290.27432 307.97610 762.0 0.001312 290.22693 354.41931 836.0 0.001196 290.17957 409.96909 885.0 0.001130 290.13214 475.80063 950.0 0.001053 290.08472 552.76111 978.0 0.001022 290.03732 640.93921 1137.0 0.000880 289.98996 738.93561 1165.0 0.000858 289.94254 842.79053 1260.0 0.000794 289.89514 944.80029 1369.0 0.000730 289.84775 1033.06396 1437.0 0.000696 289.80035 1093.18030 1422.0 0.000703 289.75293 1112.87585 1456.0 0.000687 289.70554 1087.64758 1373.0 0.000728 289.65814 1023.16296 1245.0 0.000803 289.61075 932.26709 1215.0 0.000823 289.56332 829.25061 1061.0 0.000943 289.51596 725.54175 1050.0 0.000952 289.46854 628.34247 937.0 0.001067 289.42114 541.23779 863.0 0.001159 289.37372 465.39691 828.0 0.001208 289.32635 400.60721 792.0 0.001263 289.27893 345.96320 741.0 0.001350 289.23154 300.26852 703.0 0.001422 289.18411 262.25668 647.0 0.001546 289.13675 230.70876 623.0 0.001605 289.08932 204.51482 533.0 0.001876 289.04193 182.70273 533.0 0.001876 288.99457 164.44690 548.0 0.001825 288.94714 149.06404 501.0 0.001996 288.89972 136.00035 487.0 0.002053 288.85233 124.81435 488.0 0.002049 288.80496 115.15794 452.0 0.002212 288.75754 106.75831 426.0 0.002347 288.71014 99.40158 449.0 0.002227 288.66275 92.91936 461.0 0.002169 288.61536 87.17780 424.0 0.002358 288.56793 82.06937 456.0 0.002193 288.52054 77.50655 385.0 0.002597 288.47314 73.41726 466.0 0.002146 288.42575 69.74143 401.0 0.002494 288.37833 66.42857 446.0 0.002242 288.33096 63.43586 445.0 0.002247 288.28354 60.72677 399.0 0.002506 288.23615 58.26998 400.0 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247.89215 8.52491 268.0 0.00373 247.91669 8.47877 322.0 0.003106 247.94121 8.43520 280.0 0.00357 247.96574 8.39417 255.0 0.00392 247.99028 8.35563 295.0 0.003390 248.01480 8.31952 332.0 0.003012 248.03934 8.28581 240.0 0.00417 248.06387 8.25447 267.0 0.00375 248.08841 8.22545 293.0 0.003413 248.11293 8.19874 333.0 0.003003 248.13747 8.17428 272.0 0.00368 248.16200 8.15207 289.0 0.003460 248.18652 8.13208 275.0 0.00364 248.21106 8.11428 286.0 0.003497 248.23560 8.09867 294.0 0.003401 248.26013 8.08523 274.0 0.00365 248.28465 8.07395 292.0 0.003425 248.30919 8.06481 275.0 0.00364 248.33372 8.05782 279.0 0.00358 248.35826 8.05297 272.0 0.00368 248.38277 8.05027 276.0 0.00362 248.40730 8.04971 303.0 0.003300 248.43184 8.05130 264.0 0.00379 248.45636 8.05507 286.0 0.003497 248.48090 8.06100 277.0 0.00361 248.50543 8.06914 261.0 0.00383 248.52997 8.07949 298.0 0.003356 248.55449 8.09208 264.0 0.00379 248.57903 8.10693 297.0 0.003367 248.60356 8.12409 293.0 0.003413 248.62808 8.38745 308.0 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552.36652 846.0 0.001182 241.58803 571.71759 889.0 0.001125 241.53748 579.00928 792.0 0.001263 241.48689 572.27545 829.0 0.001206 241.43631 552.44910 827.0 0.001209 241.38573 520.51361 764.0 0.001309 241.33517 480.90506 717.0 0.001395 241.28459 437.54135 676.0 0.001479 241.23401 393.69348 616.0 0.001623 241.18346 351.65439 539.0 0.001855 241.13287 312.78818 554.0 0.001805 241.08229 277.74786 500.0 0.002000 241.03169 246.71097 456.0 0.002193 240.98116 219.56725 462.0 0.002165 240.93056 196.04787 410.0 0.002439 240.87997 175.80772 428.0 0.002336 240.82939 158.47459 411.0 0.002433 240.77884 143.67900 411.0 0.002433 240.72826 131.07124 382.0 0.002618 240.67767 120.33123 404.0 0.002475 240.62712 111.17341 354.0 0.002825 240.57654 103.34850 321.0 0.003115 240.52596 96.64294 357.0 0.002801 240.47536 90.87666 353.0 0.002833 240.42482 85.89985 344.0 0.002907 240.37424 81.58922 341.0 0.002933 240.32364 77.84403 379.0 0.002639 240.27310 74.58246 363.0 0.002755 240.22250 71.73804 321.0 0.003115 240.17192 69.25674 322.0 0.003106 240.12134 67.09450 317.0 0.003155 240.07079 65.21518 316.0 0.003165 240.02020 63.58895 342.0 0.002924 239.96962 62.19106 331.0 0.003021 239.91907 61.00083 336.0 0.002976 239.86848 60.00095 303.0 0.003300 239.81790 59.17688 337.0 0.002967 239.76730 58.51643 284.0 0.00352 239.71677 58.00941 323.0 0.003096 239.66618 57.64738 324.0 0.003086 239.61559 57.42342 364.0 0.002747 239.56500 57.33199 286.0 0.003497 239.51445 57.36874 307.0 0.003257 239.46387 57.53052 303.0 0.003300 239.41328 57.81518 312.0 0.003205 239.36273 58.22158 320.0 0.003125 239.31215 58.74954 297.0 0.003367 239.26157 59.39981 319.0 0.003135 239.21098 60.17406 346.0 0.002890 239.16043 61.07489 299.0 0.003344 239.10985 62.10582 291.0 0.003436 239.05925 63.27137 325.0 0.003077 239.00871 64.57711 321.0 0.003115 238.95813 66.02966 311.0 0.003215 238.90753 67.63686 319.0 0.003135 238.85695 69.40779 318.0 0.003145 238.80640 71.35294 302.0 0.003311 238.75581 73.48440 344.0 0.002907 238.70523 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323.78738 494.0 0.002024 190.44122 300.38150 522.0 0.001916 190.45404 280.07239 498.0 0.002008 190.46687 262.65463 487.0 0.002053 190.47971 247.92645 472.0 0.002119 190.49254 235.69656 479.0 0.002088 190.50536 225.78795 462.0 0.002165 190.51819 218.03969 458.0 0.002183 190.53102 212.30676 462.0 0.002165 190.54384 208.45775 503.0 0.001988 190.55667 206.37061 462.0 0.002165 190.56950 205.92534 515.0 0.001942 190.58234 206.99365 467.0 0.002141 190.59515 209.42477 509.0 0.001965 190.60799 213.02675 528.0 0.001894 190.62082 217.54495 570.0 0.001754 190.63364 222.63982 550.0 0.001818 190.64647 227.87157 564.0 0.001773 190.65930 232.70036 575.0 0.001739 190.67213 236.51538 581.0 0.001721 190.68495 238.69846 531.0 0.001883 190.69778 238.71902 527.0 0.001898 190.71062 236.23479 521.0 0.001919 190.72345 231.16498 509.0 0.001965 190.73627 223.70364 453.0 0.002208 190.74910 214.26813 429.0 0.002331 190.76193 203.40378 427.0 0.002342 190.77475 191.68181 443.0 0.002257 190.78758 179.61949 387.0 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212.76280 552.97284 821.0 0.001218 212.82458 594.03497 922.0 0.001085 212.88647 636.93237 999.0 0.001001 212.94826 680.66431 1008.0 0.000992 213.01006 723.84772 1067.0 0.000937 213.07193 764.70990 1115.0 0.000897 213.13371 801.15765 1157.0 0.000864 213.19551 830.95251 1169.0 0.000855 213.25739 851.99152 1163.0 0.000860 213.31918 862.64856 1153.0 0.000867 213.38097 862.08459 1173.0 0.000853 213.44284 849.99866 1064.0 0.000940 213.50464 828.30597 1044.0 0.000958 213.56651 798.35956 967.0 0.001034 213.62831 762.33240 970.0 0.001031 213.69009 722.45496 905.0 0.001105 213.75197 680.75940 872.0 0.001147 213.81377 638.93213 834.0 0.001199 213.87555 598.26544 691.0 0.001447 213.93744 559.68158 733.0 0.001364 213.99922 523.78900 657.0 0.001522 214.06100 490.95325 658.0 0.001520 214.12289 461.36179 659.0 0.001517 214.18468 435.07877 630.0 0.001587 214.24646 412.08798 605.0 0.001653 214.30835 392.32385 612.0 0.001634 214.37013 375.69489 577.0 0.001733 214.43202 362.09906 570.0 0.001754 214.49380 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0.001550 216.28659 566.79547 596.0 0.001678 216.34848 537.43378 595.0 0.001681 216.41026 508.54843 559.0 0.001789 216.47206 480.93463 562.0 0.001779 216.53394 455.14349 523.0 0.001912 216.59572 431.52866 496.0 0.002016 216.65761 410.29376 490.0 0.002041 216.71939 391.53583 465.0 0.002151 216.78119 375.27979 429.0 0.002331 216.84306 361.50470 489.0 0.002045 216.90486 350.16306 477.0 0.002096 216.96664 341.73148 457.0 0.002188 217.02852 335.07544 492.0 0.002033 217.09032 330.66867 501.0 0.001996 217.15210 328.45856 474.0 0.002110 217.21399 328.40280 542.0 0.001845 217.27577 330.47110 517.0 0.001934 217.33755 334.64539 507.0 0.001972 217.39944 340.91898 563.0 0.001776 217.46123 349.29465 578.0 0.001730 217.52312 359.78113 551.0 0.001815 217.58490 372.38730 543.0 0.001842 217.64668 387.11456 637.0 0.001570 217.70857 403.94507 660.0 0.001515 217.77036 422.82629 744.0 0.001344 217.83214 443.65012 688.0 0.001453 217.89403 466.22839 760.0 0.001316 217.95581 490.26529 762.0 0.001312 218.01761 515.33185 832.0 0.001202 218.07948 540.85266 918.0 0.001089 218.14127 566.11639 933.0 0.001072 218.20316 590.32458 965.0 0.001036 218.26494 612.68268 1025.0 0.000976 218.32674 632.53430 1015.0 0.000985 218.38861 649.50000 1065.0 0.000939 218.45039 663.59027 1017.0 0.000983 218.51219 675.24615 1064.0 0.000940 218.57407 685.29712 1066.0 0.000938 218.63586 694.84845 1063.0 0.000941 218.69765 705.14124 1087.0 0.000920 218.75952 717.42426 1134.0 0.000882 218.82132 732.86224 1032.0 0.000969 218.88310 752.48767 1103.0 0.000907 218.94499 777.18744 1084.0 0.000923 219.00677 808.32178 1134.0 0.000882 219.06865 845.28802 1178.0 0.000849 219.13045 889.19879 1204.0 0.000831 219.19223 940.43579 1233.0 0.000811 219.25412 999.24323 1336.0 0.000749 219.31590 1065.68994 1361.0 0.000735 219.37769 1139.61475 1388.0 0.000720 219.43958 1220.54724 1425.0 0.000702 219.50136 1307.61292 1560.0 0.000641 219.56314 1399.43103 1565.0 0.000639 219.62503 1494.01855 1520.0 0.000658 219.68681 1588.73364 1619.0 0.000618 219.74870 1680.29504 1856.0 0.000539 219.81049 1764.91614 1802.0 0.000555 219.87227 1838.58679 1855.0 0.000539 219.93416 1897.48193 1890.0 0.000529 219.99594 1938.43921 1877.0 0.000533 220.05774 1959.37903 1868.0 0.000535 220.11961 1959.56372 1999.0 0.000500 220.18140 1939.62830 2002.0 0.000500 220.24319 1901.40686 1984.0 0.000504 220.30507 1847.61719 2103.0 0.000476 220.36687 1781.48315 2021.0 0.000495 220.42865 1706.35132 1842.0 0.000543 220.49052 1625.34778 1748.0 0.000572 220.55232 1541.12415 1650.0 0.000606 220.61420 1455.72180 1659.0 0.000603 220.67599 1370.56604 1473.0 0.000679 220.73778 1286.57288 1387.0 0.000721 220.79965 1204.31836 1298.0 0.000770 220.86145 1124.21143 1272.0 0.000786 220.92323 1046.62537 1239.0 0.000807 220.98512 971.96069 1169.0 0.000855 221.04691 900.64337 1132.0 0.000883 221.10869 833.08405 964.0 0.001037 221.17058 769.62537 924.0 0.001082 221.23236 710.50293 869.0 0.001151 221.29425 655.82709 838.0 0.001193 221.35603 605.58582 770.0 0.001299 221.41782 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253.08601 55.06378 279.0 0.00358 252.53613 54.59636 269.0 0.00372 251.98541 54.20347 272.0 0.00368 251.43553 53.88569 263.0 0.00380 250.88565 53.00186 248.0 0.00403 250.33493 52.84143 230.0 0.00435 249.78505 52.76099 264.0 0.00379 249.23517 52.76326 240.0 0.00417 248.68445 52.85141 232.0 0.00431 248.13457 53.02916 257.0 0.00389 247.58467 53.21338 287.0 0.003484 247.03395 53.58361 269.0 0.00372 246.48407 54.05708 231.0 0.00433 245.93335 54.63905 275.0 0.00364 245.38347 55.33496 256.0 0.00391 244.83359 56.15041 282.0 0.00355 244.28287 57.09092 288.0 0.003472 243.73299 58.16178 289.0 0.003460 243.18311 59.36773 270.0 0.00370 242.63239 60.71267 266.0 0.00376 242.08250 62.19906 245.0 0.00408 241.53262 63.82737 297.0 0.003367 240.98190 65.59521 293.0 0.003413 240.43202 67.49635 305.0 0.003279 239.88130 69.51950 262.0 0.00382 239.33142 71.64713 270.0 0.00370 238.78154 73.85423 316.0 0.003165 238.23082 76.10754 306.0 0.003268 237.68094 78.36538 313.0 0.003195 237.13106 80.57890 326.0 0.003067 236.58032 82.69460 329.0 0.003040 236.03044 84.65893 325.0 0.003077 235.48056 86.42420 328.0 0.003049 234.92984 87.95530 337.0 0.002967 234.37996 89.23557 312.0 0.003205 233.83008 90.27111 312.0 0.003205 233.27936 91.09145 281.0 0.00356 232.72948 91.84165 313.0 0.003195 232.17876 92.40081 317.0 0.003155 231.62888 92.93954 281.0 0.00356 231.07899 93.53816 308.0 0.003247 230.52827 94.27510 328.0 0.003049 229.97839 95.22346 308.0 0.003247 229.42851 96.44885 316.0 0.003165 228.87779 98.00899 267.0 0.00375 228.32791 99.95387 293.0 0.003413 227.77803 102.32654 282.0 0.00355 227.22731 105.16390 311.0 0.003215 226.67743 108.49718 281.0 0.00356 226.12671 112.35210 301.0 0.003322 225.57681 116.74853 345.0 0.002899 225.02693 121.69936 323.0 0.003096 224.47621 127.20873 314.0 0.003185 223.92633 133.26958 333.0 0.003003 223.37645 139.86014 339.0 0.002950 222.82573 146.94026 324.0 0.003086 222.27585 154.44698 342.0 0.002924 221.72597 162.29065 363.0 0.002755 221.17525 170.35252 366.0 0.002732 220.62537 178.48439 352.0 0.002841 220.07549 186.51274 406.0 0.002463 219.52477 194.24748 399.0 0.002506 218.97488 201.49614 413.0 0.002421 218.42416 208.08133 382.0 0.002618 217.87428 213.85927 422.0 0.002370 217.32440 218.73407 442.0 0.002262 216.77368 222.66438 416.0 0.002404 216.22380 225.65923 439.0 0.002278 215.67392 227.76421 426.0 0.002347 215.12320 229.04187 480.0 0.002083 214.57332 229.55081 501.0 0.001996 214.02342 229.33028 462.0 0.002165 213.47270 228.39307 430.0 0.002326 212.92282 226.72913 460.0 0.002174 212.37210 224.31776 477.0 0.002096 211.82222 221.32509 408.0 0.002451 211.27234 217.40019 429.0 0.002331 210.72162 212.76622 412.0 0.002427 210.17174 207.50420 430.0 0.002326 209.62186 201.72569 420.0 0.002381 209.07114 195.55997 380.0 0.002632 208.52126 189.13724 419.0 0.002387 207.97137 182.57359 403.0 0.002481 207.42065 175.96002 342.0 0.002924 206.87077 169.35780 373.0 0.002681 206.32089 162.79929 404.0 0.002475 205.77017 156.29425 370.0 0.002703 205.22029 149.83937 365.0 0.002740 204.66957 143.42822 357.0 0.002801 204.11969 137.06026 390.0 0.002564 203.56981 131.40376 335.0 0.002985 203.01907 125.17044 348.0 0.002874 202.46919 119.04984 339.0 0.002950 201.91931 113.08372 288.0 0.003472 201.36859 107.31520 311.0 0.003215 200.81871 101.78431 313.0 0.003195 200.26883 96.52442 293.0 0.003413 199.71811 91.56049 308.0 0.003247 199.16823 86.90865 292.0 0.003425 198.61751 82.57678 319.0 0.003135 198.06763 78.56581 273.0 0.00366 197.51775 74.87093 253.0 0.00395 196.96703 71.48335 276.0 0.00362 196.41714 68.39120 242.0 0.00413 195.86726 65.58077 266.0 0.00376 195.31654 63.03730 244.0 0.00410 194.76666 60.74545 290.0 0.003448 194.21678 58.68974 251.0 0.00398 193.66606 56.85471 234.0 0.00427 193.11618 55.46216 240.0 0.00417 192.56630 54.02351 244.0 0.00410 192.01558 52.75932 239.0 0.00418 191.46568 51.65364 242.0 0.00413 190.91496 50.68970 239.0 0.00418 190.36508 49.84961 250.0 0.00400 189.81520 49.11399 277.0 0.00361 189.26448 48.46192 250.0 0.00400 188.71460 47.87096 255.0 0.00392 188.16472 47.31773 246.0 0.00407 187.61400 46.77882 235.0 0.00426 187.06412 46.23232 241.0 0.00415 186.51424 45.65931 203.0 0.00493 185.96352 45.04573 229.0 0.00437 185.41364 44.38351 202.0 0.00495 184.86292 43.67108 238.0 0.00420 184.31303 42.91309 227.0 0.00441 183.76315 42.11912 234.0 0.00427 183.21243 41.30213 260.0 0.00385 182.66255 40.47659 250.0 0.00400 182.11267 39.65690 206.0 0.00485 181.56195 38.85626 234.0 0.00427 181.01207 38.08591 263.0 0.00380 180.46217 37.35489 231.0 0.00433 179.91145 36.67007 250.0 0.00400 179.36157 36.03637 217.0 0.00461 178.81169 35.45710 204.0 0.00490 178.26097 34.93426 237.0 0.00422 177.71109 34.46893 221.0 0.00452 177.16037 34.06150 242.0 0.00413 176.61049 33.71189 199.0 0.00503 176.06061 33.41979 231.0 0.00433 175.50989 33.18475 239.0 0.00418 174.96001 33.00632 211.0 0.00474 175.12231 32.88414 220.0 0.00455 175.28488 32.81801 217.0 0.00461 175.44719 32.80799 235.0 0.00426 175.60951 32.85441 223.0 0.00448 175.77206 32.95796 230.0 0.00435 175.93437 32.86586 228.0 0.00439 176.09694 32.71085 221.0 0.00452 176.25925 32.99697 249.0 0.00402 176.42157 33.34760 259.0 0.00386 176.58412 33.76606 220.0 0.00455 176.74644 34.25637 237.0 0.00422 176.90875 34.82341 248.0 0.00403 177.07130 35.47287 251.0 0.00398 177.23363 36.21138 221.0 0.00452 177.39594 37.04662 247.0 0.00405 177.55850 37.98732 232.0 0.00431 177.72081 39.04340 222.0 0.00450 177.88312 40.22593 225.0 0.00444 178.04568 41.54729 252.0 0.00397 178.20799 43.02107 250.0 0.00400 178.37056 44.66218 228.0 0.00439 178.53287 46.48676 254.0 0.00394 178.69518 48.51218 259.0 0.00386 178.85774 50.75688 270.0 0.00370 179.02005 53.26243 283.0 0.00353 179.18237 56.00498 255.0 0.00392 179.34492 59.02733 269.0 0.00372 179.50725 62.35051 263.0 0.00380 179.66956 65.99527 288.0 0.003472 179.83212 69.98152 235.0 0.00426 179.99443 74.32758 246.0 0.00407 180.15698 79.04891 292.0 0.003425 180.31931 84.15687 261.0 0.00383 180.48161 89.65665 298.0 0.003356 180.64418 95.54491 282.0 0.00355 180.80649 101.80637 282.0 0.00355 180.96880 108.41006 257.0 0.00389 181.13136 115.30456 333.0 0.003003 181.29367 122.41290 297.0 0.003367 181.45599 129.62759 292.0 0.003425 181.61855 136.80644 280.0 0.00357 181.78085 143.77109 330.0 0.003030 181.94318 150.30922 348.0 0.002874 182.10573 156.54726 320.0 0.003125 182.26805 161.50958 382.0 0.002618 182.43060 165.32101 351.0 0.002849 182.59293 167.78014 351.0 0.002849 182.75523 168.74675 353.0 0.002833 182.91779 168.16145 356.0 0.002809 183.08011 165.97244 305.0 0.003279 183.24242 162.45850 346.0 0.002890 183.40498 157.72104 324.0 0.003086 183.56729 151.98862 340.0 0.002941 183.72960 145.50882 288.0 0.003472 183.89217 138.42010 298.0 0.003356 184.05447 131.15445 287.0 0.003484 184.21704 123.79660 330.0 0.003030 184.37935 116.50057 309.0 0.003236 184.54166 109.38490 279.0 0.00358 184.70422 102.53597 269.0 0.00372 184.86653 96.01294 264.0 0.00379 185.02885 89.89021 330.0 0.003030 185.19141 84.11304 256.0 0.00391 185.35373 78.72540 276.0 0.00362 185.51604 73.72437 251.0 0.00398 185.67859 69.10027 267.0 0.00375 185.84091 64.77428 241.0 0.00415 186.00322 60.85742 280.0 0.00357 186.16579 57.26545 268.0 0.00373 186.32809 53.97755 268.0 0.00373 186.49066 50.97245 258.0 0.00388 186.65297 48.22890 228.0 0.00439 186.81528 45.72614 239.0 0.00418 186.97784 43.44403 215.0 0.00465 187.14015 41.36338 256.0 0.00391 187.23294 39.46602 219.0 0.00457 187.04738 37.73493 234.0 0.00427 186.86209 36.22221 249.0 0.00402 186.67679 34.77769 247.0 0.00405 186.49123 33.45564 254.0 0.00394 186.30594 32.24384 235.0 0.00426 186.12036 31.13125 264.0 0.00379 185.93507 30.10793 239.0 0.00418 185.74979 29.16496 241.0 0.00415 185.56421 28.85217 229.0 0.00437 185.37892 28.04930 242.0 0.00413 185.19363 27.30543 214.0 0.00467 185.00806 26.61497 223.0 0.00448 184.82277 25.97298 195.0 0.00513 184.63748 25.37509 219.0 0.00457 184.45190 24.81742 209.0 0.00478 184.26662 24.29655 209.0 0.00478 184.08133 23.80945 242.0 0.00413 183.89575 23.35341 221.0 0.00452 183.71046 22.92604 198.0 0.00505 183.52490 22.52519 225.0 0.00444 183.33961 22.14894 214.0 0.00467 183.15431 21.79556 238.0 0.00420 182.96875 21.46351 225.0 0.00444 182.78346 21.15137 245.0 0.00408 182.59818 20.85790 251.0 0.00398 182.41260 20.58191 221.0 0.00452 182.22731 20.43985 224.0 0.00446 182.04202 20.19659 205.0 0.00488 181.85645 19.96795 216.0 0.00463 181.67116 19.75312 191.0 0.00524 181.48558 19.55135 205.0 0.00488 181.30029 19.36197 184.0 0.00543 181.11501 19.18437 191.0 0.00524 180.92943 19.01796 200.0 0.00500 180.74414 18.86222 228.0 0.00439 180.55885 18.71666 202.0 0.00495 180.37328 18.58085 234.0 0.00427 180.18799 18.45437 243.0 0.00412 180.00270 18.33684 218.0 0.00459 179.81714 18.22792 195.0 0.00513 179.63184 18.12731 218.0 0.00459 179.44655 18.03471 200.0 0.00500 179.26099 17.79208 219.0 0.00457 179.07570 17.71543 237.0 0.00422 178.89012 17.64608 194.0 0.00515 178.70483 17.57645 229.0 0.00437 178.51955 17.52121 209.0 0.00478 178.33397 17.47277 191.0 0.00524 178.14868 16.90394 181.0 0.00552 177.96339 16.87111 207.0 0.00483 177.77782 16.84478 201.0 0.00498 177.59253 16.83190 221.0 0.00452 177.40724 16.81853 225.0 0.00444 177.22166 16.81159 215.0 0.00465 177.03638 16.81114 207.0 0.00483 176.85080 16.81724 214.0 0.00467 176.66551 16.82997 205.0 0.00488 176.48022 16.99526 194.0 0.00515 176.29466 17.02231 211.0 0.00474 176.10936 17.05648 215.0 0.00465 175.92407 17.09800 225.0 0.00444 175.73851 17.14714 209.0 0.00478 175.55322 17.20420 218.0 0.00459 175.36792 17.26954 207.0 0.00483 175.18236 17.34354 201.0 0.00498 174.99707 17.42663 217.0 0.00461 174.96001 17.51929 214.0 0.00467 174.96001 17.62201 231.0 0.00433 174.96001 17.73533 240.0 0.00417 174.96001 17.85981 214.0 0.00467 174.96001 17.99603 214.0 0.00467 174.96001 18.14459 204.0 0.00490 174.96001 18.30608 201.0 . . . 209.0 . . . 205.0 . . . 221.0 . . . 249.0 . . . 219.0 . . . 211.0 . . . 194.0 . . . 215.0 . . . 207.0 . . . 226.0 . . . 177.0 . . . 214.0 . . . 211.0 . . . 209.0 . 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308.0 . . . 310.0 . . . 320.0 . . . 312.0 . . . 307.0 . . . 283.0 . . . 324.0 . . . 299.0 . . . 322.0 . . . 348.0 . . . 341.0 . . . 362.0 . . . 346.0 . . . 358.0 . . . 364.0 . . . 408.0 . . . 370.0 . . . 428.0 . . . 421.0 . . . 405.0 . . . 485.0 . . . 480.0 . . . 505.0 . . . 536.0 . . . 546.0 . . . 567.0 . . . 662.0 . . . 646.0 . . . 634.0 . . . 649.0 . . . 644.0 . . . 756.0 . . . 683.0 . . . 690.0 . . . 668.0 . . . 640.0 . . . 643.0 . . . 565.0 . . . 581.0 . . . 561.0 . . . 470.0 . . . 443.0 . . . 475.0 . . . 410.0 . . . 483.0 . . . 439.0 . . . 401.0 . . . 384.0 . . . 360.0 . . . 355.0 . . . 402.0 . . . 363.0 . . . 327.0 . . . 313.0 . . . 342.0 . . . 324.0 . . . 357.0 . . . 290.0 . . . 306.0 . . . 314.0 . . . 280.0 . . . 275.0 . . . 316.0 . . . 264.0 . . . 272.0 . . . 280.0 . . . 282.0 . . . 273.0 . . . 270.0 . . . 260.0 . . . 299.0 . . . 297.0 . . . 270.0 . . . 282.0 . . . 274.0 . . . 239.0 . . . 268.0 . . . 277.0 . . . 270.0 . . . 267.0 . . . 285.0 . . . 303.0 . . . 252.0 . . . 265.0 . . . 273.0 . . . 303.0 . . . 269.0 . . . 306.0 . . . 273.0 . . . 296.0 . . . 305.0 . . . 317.0 . . . 325.0 . . . 314.0 . . . 318.0 . . . 341.0 . . . 352.0 . . . 316.0 . . . 370.0 . . . 386.0 . . . 422.0 . . . 371.0 . . . 391.0 . . . 387.0 . . . 400.0 . . . 412.0 . . . 429.0 . . . 368.0 . . . 389.0 . . . 354.0 . . . 347.0 . . . 356.0 . . . 389.0 . . . 405.0 . . . 325.0 . . . 438.0 . . . 383.0 . . . 403.0 . . . 390.0 . . . 404.0 . . . 391.0 . . . 410.0 . . . 389.0 . . . 395.0 . . . 440.0 . . . 468.0 . . . 482.0 . . . 476.0 . . . 474.0 . . . 502.0 . . . 545.0 . . . 518.0 . . . 557.0 . . . 591.0 . . . 606.0 . . . 556.0 . . . 628.0 . . . 724.0 . . . 655.0 . . . 772.0 . . . 731.0 . . . 742.0 . . . 726.0 . . . 766.0 . . . 769.0 . . . 801.0 . . . 788.0 . . . 739.0 . . . 764.0 . . . 796.0 . . . 773.0 . . . 776.0 . . . 742.0 . . . 773.0 . . . 774.0 . . . 854.0 . . . 820.0 . . . 762.0 . . . 839.0 . . . 761.0 . . . 803.0 . . . 856.0 . . . 812.0 . . . 746.0 . . . 796.0 . . . 828.0 . . . 781.0 . . . 758.0 . . . 769.0 . . . 737.0 . . . 769.0 . . . 719.0 . . . 719.0 . . . 662.0 . . . 700.0 . . . 664.0 . . . 667.0 . . . 650.0 . . . 593.0 . . . 615.0 . . . 573.0 . . . 539.0 . . . 514.0 . . . 500.0 . . . 536.0 . . . 464.0 . . . 479.0 . . . 455.0 . . . 424.0 . . . 424.0 . . . 383.0 . . . 397.0 . . . 363.0 . . . 353.0 . . . 378.0 . . . 323.0 . . . 380.0 . . . 357.0 . . . 335.0 . . . 313.0 . . . 333.0 . . . 329.0 . . . 331.0 . . . 330.0 . . . 270.0 . . . 300.0 . . . 279.0 . . . 282.0 . . . 289.0 . . . 302.0 . . . 282.0 . . . 289.0 . . . 318.0 . . . 303.0 . . . 312.0 . . . 298.0 . . . 337.0 . . . 336.0 . . . 349.0 . . . 321.0 . . . 309.0 . . . 376.0 . . . 363.0 . . . 329.0 . . . 334.0 . . . 374.0 . . . 332.0 . . . 356.0 . . . 379.0 . . . 376.0 . . . 451.0 . . . 396.0 . . . 446.0 . . . 452.0 . . . 456.0 . . . 481.0 . . . 486.0 . . . 535.0 . . . 558.0 . . . 578.0 . . . 609.0 . . . 637.0 . . . 669.0 . . . 780.0 . . . 737.0 . . . 784.0 . . . 758.0 . . . 867.0 . . . 807.0 . . . 825.0 . . . 813.0 . . . 860.0 . . . 837.0 . . . 828.0 . . . 779.0 . . . 738.0 . . . 783.0 . . . 741.0 . . . 731.0 . . . 737.0 . . . 707.0 . . . 746.0 . . . 732.0 . . . 691.0 . . . 667.0 . . . 703.0 . . . 654.0 . . . 665.0 . . . 682.0 . . . 666.0 . . . 634.0 . . . 624.0 . . . 580.0 . . . 622.0 . . . 677.0 . . . 601.0 . . . 665.0 . . . 624.0 . . . 618.0 . . . 712.0 . . . 701.0 . . . 707.0 . . . 766.0 . . . 774.0 . . . 796.0 . . . 870.0 . . . 803.0 . . . 779.0 . . . 854.0 . . . 796.0 . . . 850.0 . . . 877.0 . . . 856.0 . . . 902.0 . . . 895.0 . . . 811.0 . . . 834.0 . . . 853.0 . . . 805.0 . . . 811.0 . . . 762.0 . . . 780.0 . . . 797.0 . . . 807.0 . . . 743.0 . . . 722.0 . . . 786.0 . . . 728.0 . . . 735.0 . . . 700.0 . . . 694.0 . . . 751.0 . . . 651.0 . . . 663.0 . . . 598.0 . . . 636.0 . . . 583.0 . . . 593.0 . . . 580.0 . . . 523.0 . . . 548.0 . . . 514.0 . . . 435.0 . . . 518.0 . . . 470.0 . . . 473.0 . . . 451.0 . . . 462.0 . . . 444.0 . . . 453.0 . . . 480.0 . . . 423.0 . . . 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206.0 . . . 226.0 . . . 199.0 . . . 199.0 . . . 208.0 . . . 215.0 . . . 208.0 . . . 207.0 . . . 206.0 . . . 227.0 . . . 220.0 . . . 195.0 . . . 208.0 . . . 215.0 . . . 215.0 . . . 197.0 . . . 183.0 . . . 226.0 . . . 223.0 . . . 221.0 . . . 225.0 . . . 192.0 . . . 210.0 . . . 197.0 . . . 224.0 . . . 210.0 . . . 203.0 . . . 247.0 . . . 233.0 . . . 206.0 . . . 212.0 . . . 217.0 . . . 235.0 . . . 212.0 . . . 222.0 . . . 221.0 . . . 231.0 . . . 229.0 . . . 223.0 . . . 243.0 . . . 229.0 . . . 234.0 . . . 224.0 . . . 218.0 . . . 210.0 . . . 220.0 . . . 207.0 . . . 240.0 . . . 206.0 . . . 232.0 . . . 234.0 . . . 212.0 . . . 212.0 . . . 241.0 . . . 236.0 . . . 276.0 . . . 251.0 . . . 244.0 . . . 222.0 . . . 226.0 . . . 256.0 . . . 219.0 . . . 217.0 . . . 232.0 . . . 267.0 . . . 254.0 . . . 223.0 . . . 198.0 . . . 221.0 . . . 225.0 . . . 219.0 . . . 220.0 . . . 263.0 . . . 251.0 . . . 230.0 . . . 217.0 . . . 256.0 . . . 241.0 . . . 223.0 . . . 247.0 . . . 224.0 . . . 225.0 . . . 225.0 . . . 199.0 . . . 205.0 . . . 231.0 . . . 226.0 . . . 225.0 . . . 214.0 . . . 216.0 . . . 233.0 . . . 230.0 . . . 233.0 . . . 235.0 . . . 190.0 . . . 242.0 . . . 237.0 . . . 204.0 . . . 235.0 . . . 232.0 . . . 212.0 . . . 219.0 . . . 233.0 . . . 206.0 . . . 229.0 . . . 214.0 . . . 231.0 . . . 222.0 . . . 201.0 . . . 204.0 . . . 168.0 . . . 209.0 . . . 234.0 . . . 208.0 . . . 233.0 . . . 213.0 . . . 237.0 . . . 206.0 . . . 247.0 . . . 246.0 . . . 202.0 . . . 192.0 . . . 208.0 . . . 220.0 . . . 245.0 . . . 229.0 . . . 235.0 . . . 202.0 . . . 177.0 . . . 215.0 . . . 232.0 . . . 209.0 . . . 219.0 . . . 206.0 . . . 212.0 . . . 203.0 . . . 222.0 . . . 225.0 . . . 228.0 . . . 224.0 . . . 242.0 . . . 226.0 . . . 229.0 . . . 222.0 . . . 214.0 . . . 246.0 . . . 203.0 . . . 207.0 . . . 223.0 . . . 226.0 . . . 249.0 . . . 236.0 . . . 247.0 . . . 248.0 . . . 241.0 . . . 247.0 . . . 225.0 . . . 257.0 . . . 254.0 . . . 262.0 . . . 244.0 . . . 254.0 . . . 223.0 . . . 269.0 . . . 207.0 . . . 247.0 . . . 235.0 . . . 243.0 . . . 235.0 . . . 255.0 . . . 235.0 . . . 261.0 . . . 236.0 . . . 241.0 . . . 248.0 . . . 216.0 . . . 258.0 . . . 238.0 . . . 253.0 . . . 270.0 . . . 242.0 . . . 239.0 . . . 236.0 . . . 263.0 . . . 253.0 . . . 286.0 . . . 262.0 . . . 241.0 . . . 260.0 . . . 269.0 . . . 243.0 . . . 272.0 . . . 257.0 . . . 235.0 . . . 258.0 . . . 269.0 . . . 248.0 . . . 223.0 . . . 240.0 . . . 262.0 . . . 243.0 . . . 222.0 . . . 214.0 . . . 249.0 . . . 234.0 . . . 195.0 . . . 240.0 . . . 234.0 . . . 246.0 . . . 208.0 . . . 223.0 . . . 208.0 . . . 206.0 . . . 207.0 . . . 231.0 . . . 209.0 . . . 233.0 . . . 244.0 . . . 217.0 . . . 257.0 . . . 211.0 . . . 212.0 . . . 232.0 . . . 201.0 . . . 221.0 . . . 201.0 . . . 209.0 . . . 213.0 . . . 186.0 . . . 252.0 . . . 199.0 . . . 192.0 . . . 227.0 . . . 214.0 . . . 196.0 . . . 199.0 . . . 214.0 . . . 243.0 . . . 202.0 . . . 239.0 . . . 194.0 . . . 209.0 . . . 222.0 . . . 225.0 . . . 201.0 . . . 237.0 . . . 164.0 . . . 218.0 . . . 234.0 . . . 201.0 . . . 242.0 . . . 238.0 . . . 218.0 . . . 201.0 . . . 238.0 . . . 239.0 . . . 195.0 . . . 237.0 . . . 244.0 . . . 236.0 . . . 239.0 . . . 229.0 . . . 200.0 . . . 207.0 . . . 228.0 . . . 228.0 . . . 227.0 . . . 228.0 . . . 241.0 . . . 226.0 . . . 244.0 . . . 265.0 . . . 262.0 . . . 250.0 . . . 234.0 . . . 254.0 . . . 248.0 . . . 266.0 . . . 219.0 . . . 267.0 . . . 258.0 . . . 245.0 . . . 269.0 . . . 263.0 . . . 265.0 . . . 258.0 . . . 278.0 . . . 260.0 . . . 240.0 . . . 260.0 . . . 288.0 . . . 249.0 . . . 242.0 . . . 265.0 . . . 238.0 . . . 253.0 . . . 249.0 . . . 245.0 . . . 233.0 . . . 249.0 . . . 271.0 . . . 244.0 . . . 245.0 . . . 233.0 . . . 273.0 . . . 252.0 . . . 243.0 . . . 240.0 . . . 254.0 . . . 234.0 . . . 235.0 . . . 248.0 . . . 241.0 . . . 245.0 . . . 222.0 . . . 229.0 . . . 240.0 . . . 234.0 . . . 243.0 . . . 221.0 . . . 251.0 . . . 206.0 . . . 197.0 . . . 247.0 . . . 243.0 . . . 203.0 . . . 238.0 . . . 226.0 . . . 201.0 . . . 197.0 . . . 204.0 . . . 208.0 . . . 227.0 . . . 193.0 . . . 234.0 . . . 186.0 . . . 218.0 . . . 217.0 . . . 219.0 . . . 196.0 . . . 213.0 . . . 217.0 . . . 210.0 . . . 202.0 . . . 212.0 . . . 227.0 . . . 217.0 . . . 204.0 . . . 225.0 . . . 241.0 . . . 220.0 . . . 206.0 . . . 232.0 . . . 210.0 . . . 240.0 . . . 212.0 . . . 203.0 . . . 244.0 . . . 232.0 . . . 218.0 . . . 235.0 . . . 226.0 . . . 239.0 . . . 232.0 . . . 231.0 . . . 239.0 . . . 223.0 . . . 209.0 . . . 241.0 . . . 229.0 . . . 237.0 . . . 267.0 . . . 224.0 . . . 241.0 . . . 208.0 . . . 221.0 . . . 229.0 . . . 221.0 . . . 238.0 . . . 247.0 . . . 252.0 . . . 264.0 . . . 241.0 . . . 249.0 . . . 239.0 . . . 257.0 . . . 258.0 . . . 235.0 . . . 275.0 . . . 267.0 . . . 264.0 . . . 250.0 . . . 273.0 . . . 275.0 . . . 275.0 . . . 259.0 . . . 258.0 . . . 266.0 . . . 261.0 . . . 248.0 . . . 271.0 . . . 257.0 . . . 231.0 . . . 281.0 . . . 263.0 . . . 263.0 . . . 270.0 . . . 268.0 . . . 252.0 . . . 214.0 . . . 288.0 . . . 240.0 . . . 276.0 . . . 270.0 . . . 248.0 . . . 264.0 . . . 287.0 . . . 226.0 . . . 254.0 . . . 230.0 . . . 265.0 . . . 262.0 . . . 245.0 . . . 229.0 . . . 257.0 . . . 236.0 . . . 210.0 . . . 240.0 . . . 242.0 . . . 252.0 . . . 275.0 . . . 260.0 . . . 240.0 . . . 212.0 . . . 220.0 . . . 231.0 . . . 223.0 . . . 230.0 . . . 238.0 . . . 237.0 . . . 229.0 . . . 225.0 . . . 239.0 . . . 217.0 . . . 246.0 . . . 216.0 . . . 222.0 . . . 250.0 . . . 228.0 . . . 239.0 . . . 244.0 . . . 243.0 . . . 244.0 . . . 257.0 . . . 228.0 . . . 253.0 . . . 261.0 . . . 253.0 . . . 230.0 . . . 258.0 . . . 263.0 . . . 267.0 . . . 258.0 . . . 261.0 . . . 233.0 . . . 249.0 . . . 238.0 . . . 256.0 . . . 222.0 . . . 263.0 . . . 251.0 . . . 232.0 . . . 238.0 . . . 289.0 . . . 255.0 . . . 269.0 . . . 288.0 . . . 265.0 . . . 282.0 . . . 254.0 . . . 229.0 . . . 292.0 . . . 273.0 . . . 278.0 . . . 295.0 . . . 298.0 . . . 256.0 . . . 251.0 . . . 266.0 . . . 263.0 . . . 266.0 . . . 304.0 . . . 291.0 . . . 262.0 . . . 277.0 . . . 283.0 . . . 285.0 . . . 279.0 . . . 278.0 . . . 276.0 . . . 279.0 . . . 293.0 . . . 253.0 . . . 292.0 . . . 318.0 . . . 268.0 . . . 320.0 . . . 285.0 . . . 272.0 . . . 312.0 . . . 273.0 . . . 268.0 . . . 275.0 . . . 264.0 . . . 266.0 . . . 279.0 . . . 283.0 . . . 253.0 . . . 248.0 . . . 247.0 . . . 274.0 . . . 271.0 . . . 270.0 . . . 257.0 . . . 280.0 . . . 276.0 . . . 270.0 . . . 261.0 . . . 296.0 . . . 263.0 . . . 256.0 . . . 263.0 . . . 294.0 . . . 244.0 . . . 277.0 . . . 277.0 . . . 246.0 . . . 248.0 . . . 247.0 . . . 272.0 . . . 282.0 . . . 275.0 . . . 293.0 . . . 242.0 . . . 273.0 . . . 258.0 . . . 293.0 . . . 263.0 . . . 237.0 . . . 276.0 . . . 301.0 . . . 257.0 . . . 291.0 . . . 259.0 . . . 271.0 . . . 242.0 . . . 268.0 . . . 296.0 . . . 274.0 . . . 249.0 . . . 244.0 . . . 268.0 . . . 255.0 . . . 251.0 . . . 245.0 . . . 246.0 . . . 259.0 . . . 238.0 . . . 240.0 . . . 230.0 . . . 250.0 . . . 268.0 . . . 252.0 . . . 247.0 . . . 243.0 . . . 257.0 . . . 285.0 . . . 219.0 . . . 257.0 . . . 227.0 . . . 244.0 . . . 217.0 . . . 254.0 . . . 220.0 . . . 228.0 . . . 222.0 . . . 234.0 . . . 255.0 . . . 212.0 . . . 250.0 . . . 215.0 . . . 222.0 . . . 220.0 . . . 199.0 . . . 215.0 . . . 231.0 . . . 197.0 . . . 209.0 . . . 238.0 . . . 224.0 . . . 224.0 . . . 220.0 . . . 208.0 . . . 228.0 . . . 223.0 . . . 217.0 . . . 232.0 . . . 249.0 . . . 217.0 . . . 236.0 . . . 230.0 . . . 214.0 . . . 203.0 . . . 217.0 . . . 221.0 . . . 219.0 . . . 243.0 . . . 198.0 . . . 214.0 . . . 215.0 . . . 258.0 . . . 198.0 . . . 180.0 . . . 229.0 . . . 240.0 . . . 203.0 . . . 202.0 . . . 217.0 . . . 266.0 . . . 211.0 . . . 197.0 . . . 228.0 . . . 218.0 . . . 203.0 . . . 216.0 . . . 204.0 . . . 226.0 . . . 227.0 . . . 262.0 . . . 204.0 . . . 244.0 . . . 228.0 . . . 239.0 . . . 213.0 . . . 204.0 . . . 234.0 . . . 232.0 . . . 261.0 . . . 262.0 . . . 241.0 . . . 232.0 . . . 268.0 . . . 231.0 . . . 247.0 . . . 238.0 . . . 235.0 . . . 242.0 . . . 229.0 . . . 228.0 . . . 245.0 . . . 233.0 . . . 242.0 . . . 238.0 . . . 198.0 . . . 232.0 . . . 215.0 . . . 246.0 . . . 235.0 . . . 224.0 . . . 244.0 . . . 216.0 . . . 249.0 . . . 240.0 . . . 244.0 . . . 263.0 . . . 265.0 . . . 217.0 . . . 239.0 . . . 246.0 . . . 262.0 . . . 236.0 . . . 229.0 . . . 242.0 . . . 259.0 . . . 252.0 . . . 216.0 . . . 232.0 . . . 209.0 . . . 263.0 . . . 263.0 . . . 249.0 . . . 229.0 . . . 228.0 . . . 237.0 . . . 243.0 . . . 221.0 . . . 240.0 . . . 267.0 . . . 229.0 . . . 226.0 . . . 239.0 . . . 244.0 . . . 229.0 . . . 261.0 . . . 221.0 . . . 251.0 . . . 252.0 . . . 243.0 . . . 275.0 . . . 248.0 . . . 280.0 . . . 248.0 . . . 272.0 . . . 264.0 . . . 248.0 . . . 264.0 . . . 293.0 . . . 295.0 . . . 267.0 . . . 259.0 . . . 287.0 . . . 286.0 . . . 292.0 . . . 250.0 . . . 262.0 . . . 271.0 . . . 292.0 . . . 260.0 . . . 292.0 . . . 287.0 . . . 293.0 . . . 297.0 . . . 291.0 . . . 263.0 . . . 305.0 . . . 291.0 . . . 303.0 . . . 289.0 . . . 325.0 . . . 300.0 . . . 284.0 . . . 324.0 . . . 355.0 . . . 331.0 . . . 314.0 . . . 323.0 . . . 322.0 . . . 282.0 . . . 313.0 . . . 342.0 . . . 361.0 . . . 308.0 . . . 328.0 . . . 314.0 . . . 342.0 . . . 343.0 . . . 304.0 . . . 318.0 . . . 338.0 . . . 331.0 . . . 290.0 . . . 299.0 . . . 348.0 . . . 309.0 . . . 315.0 . . . 277.0 . . . 311.0 . . . 305.0 . . . 309.0 . . . 283.0 . . . 290.0 . . . 319.0 . . . 294.0 . . . 289.0 . . . 261.0 . . . 268.0 . . . 272.0 . . . 279.0 . . . 266.0 . . . 267.0 . . . 286.0 . . . 262.0 . . . 254.0 . . . 264.0 . . . 282.0 . . . 263.0 . . . 244.0 . . . 233.0 . . . 253.0 . . . 254.0 . . . 224.0 . . . 249.0 . . . 258.0 . . . 231.0 . . . 236.0 . . . 266.0 . . . 268.0 . . . 269.0 . . . 239.0 . . . 230.0 . . . 243.0 . . . 259.0 . . . 265.0 . . . 240.0 . . . 238.0 . . . 263.0 . . . 259.0 . . . 207.0 . . . 232.0 . . . 239.0 . . . 218.0 . . . 226.0 . . . 218.0 . . . 248.0 . . . 227.0 . . . 225.0 . . . 218.0 . . . 269.0 . . . 253.0 . . . 216.0 . . . 265.0 . . . 226.0 . . . 228.0 . . . 231.0 . . . 224.0 . . . 240.0 . . . 217.0 . . . 206.0 . . . 253.0 . . . 227.0 . . . 232.0 . . . 224.0 . . . 204.0 . . . 237.0 . . . 233.0 . . . 258.0 . . . 226.0 . . . 221.0 . . . 238.0 . . . 250.0 . . . 237.0 . . . 213.0 . . . 232.0 . . . 250.0 . . . 253.0 . . . 206.0 . . . 209.0 . . . 221.0 . . . 215.0 . . . 240.0 . . . 214.0 . . . 236.0 . . . 238.0 . . . 244.0 . . . 227.0 . . . 225.0 . . . 230.0 . . . 204.0 . . . 226.0 . . . 239.0 . . . 258.0 . . . 268.0 . . . 189.0 . . . 246.0 . . . 227.0 . . . 222.0 . . . 227.0 . . . 229.0 . . . 261.0 . . . 223.0 . . . 247.0 . . . 224.0 . . . 268.0 . . . 268.0 . . . 235.0 . . . 258.0 . . . 255.0 . . . 271.0 . . . 267.0 . . . 249.0 . . . 272.0 . . . 250.0 . . . 270.0 . . . 295.0 . . . 269.0 . . . 246.0 . . . 292.0 . . . 262.0 . . . 298.0 . . . 246.0 . . . 253.0 . . . 253.0 . . . 254.0 . . . 267.0 . . . 257.0 . . . 256.0 . . . 282.0 . . . 242.0 . . . 271.0 . . . 280.0 . . . 256.0 . . . 295.0 . . . 281.0 . . . 252.0 . . . 260.0 . . . 249.0 . . . 267.0 . . . 245.0 . . . 289.0 . . . 274.0 . . . 263.0 . . . 250.0 . . . 283.0 . . . 276.0 . . . 285.0 . . . 288.0 . . . 301.0 . . . 262.0 . . . 267.0 . . . 273.0 . . . 264.0 . . . 286.0 . . . 283.0 . . . 289.0 . . . 279.0 . . . 280.0 . . . 281.0 . . . 291.0 . . . 291.0 . . . 269.0 . . . 280.0 . . . 295.0 . . . 282.0 . . . 242.0 . . . 251.0 . . . 297.0 . . . 336.0 . . . 278.0 . . . 293.0 . . . 274.0 . . . 299.0 . . . 282.0 . . . 292.0 . . . 283.0 . . . 306.0 . . . 283.0 . . . 287.0 . . . 282.0 . . . 294.0 . . . 291.0 . . . 278.0 . . . 274.0 . . . 310.0 . . . 289.0 . . . 276.0 . . . 290.0 . . . 305.0 . . . 273.0 . . . 271.0 . . . 290.0 . . . 322.0 . . . 293.0 . . . 270.0 . . . 280.0 . . . 295.0 . . . 277.0 . . . 288.0 . . . 245.0 . . . 298.0 . . . 270.0 . . . 282.0 . . . 306.0 . . . 251.0 . . . 289.0 . . . 245.0 . . . 275.0 . . . 244.0 . . . 261.0 . . . 258.0 . . . 277.0 . . . 266.0 . . . 266.0 . . . 251.0 . . . 267.0 . . . 284.0 . . . 266.0 . . . 262.0 . . . 255.0 . . . 278.0 . . . 203.0 . . . 275.0 . . . 250.0 . . . 271.0 . . . 257.0 . . . 239.0 . . . 255.0 . . . 240.0 . . . 247.0 . . . 276.0 . . . 247.0 . . . 278.0 . . . 221.0 . . . 239.0 . . . 247.0 . . . 256.0 . . . 235.0 . . . 229.0 . . . 232.0 . . . 241.0 . . . 248.0 . . . 237.0 . . . 206.0 . . . 206.0 . . . 244.0 . . . 222.0 . . . 208.0 . . . 252.0 . . . 237.0 . . . 219.0 . . . 217.0 . . . 241.0 . . . 245.0 . . . 244.0 . . . 223.0 . . . 248.0 . . . 211.0 . . . 232.0 . . . 202.0 . . . 221.0 . . . 234.0 . . . 209.0 . . . 247.0 . . . 254.0 . . . 243.0 . . . 209.0 . . . 207.0 . . . _pd_meas_number_of_points 24200 _pd_proc_number_of_points 24200 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_observed_status _refln_F_squared_meas _refln_F_squared_calc _refln_phase_calc _refln_d_spacing _gsas_i100_meas 2 2 0 o 159205.70 159356.80 0.00 7.05438 100.00 1 1 1 o 32943.895 36869.45 120.24 5.91812 10.66 0 4 0 o 9549.730 9965.238 0.00 5.01630 1.52 4 0 0 o 6794.378 7420.736 0.00 4.96057 1.06 1 3 1 o 25276.939 27482.844 64.59 4.54442 6.77 3 1 1 o 23438.654 25738.244 13.80 4.52350 6.26 2 4 0 o 191.451 182.192 0.00 4.47661 0.05 4 2 0 o 5230.297 3489.154 0.00 4.44671 1.31 3 3 1 o 13755.052 13822.971 141.00 3.81410 3.09 4 4 0 o 32094.982 24480.063 0.00 3.52719 5.10 1 5 1 o 7600.391 6844.253 -51.37 3.36789 1.47 5 1 1 o 15385.814 13492.288 -60.60 3.34246 2.95 2 6 0 o 28923.674 31126.906 -180.00 3.16901 3.72 6 2 0 o 45407.74 45243.76 -180.00 3.14081 5.75 0 2 2 o 55371.14 55967.32 -5.86 3.10016 2.33 2 0 2 o 25121.688 24867.738 -37.57 3.09683 1.06 3 5 1 o 143732.64 146161.58 58.37 3.03614 24.31 5 3 1 o 128944.62 122090.21 20.76 3.02365 21.69 2 2 2 o 68599.00 65122.59 -112.74 2.95906 5.65 4 6 0 o 6281.927 1908.308 0.00 2.77292 0.62 6 4 0 o 8323.041 3454.354 -180.00 2.76103 0.82 2 4 2 o 11356.032 9608.396 -104.64 2.63512 0.88 4 2 2 o 23876.881 22970.576 46.15 2.62898 1.84 1 7 1 o 23372.018 26622.816 10.33 2.60137 3.18 5 5 1 o 17993.215 17004.965 117.23 2.58960 2.43 7 1 1 o 25371.240 26272.838 60.19 2.57798 3.41 0 8 0 o 27132.906 27287.555 180.00 2.50815 1.11 8 0 0 o 24837.846 19810.082 180.00 2.48029 0.99 3 7 1 o 11063.924 8441.280 -31.72 2.43908 1.37 2 8 0 o 127.281 101.549 -180.00 2.43165 0.01 7 3 1 o 17903.814 15223.343 -91.78 2.42296 2.19 8 2 0 o 19.734 12.139 0.00 2.40780 0.00 4 4 2 o 4031.438 3610.659 -106.59 2.39394 0.29 6 6 0 o 5.860 0.529 180.00 2.35146 0.00 0 6 2 o 14302.862 9209.144 -37.83 2.33426 0.51 6 0 2 o 9916.578 3926.042 54.36 2.32151 0.35 2 6 2 o 4205.440 2283.669 115.03 2.27221 0.29 6 2 2 o 7699.515 5094.790 31.27 2.26175 0.53 4 8 0 o 98.010 27.989 -180.00 2.23831 0.01 8 4 0 o 2568.108 1633.521 0.00 2.22335 0.17 5 7 1 o 30798.482 28462.490 47.64 2.18880 3.23 7 5 1 o 23725.113 21366.557 19.91 2.18178 2.47 1 1 3 o 3374.393 1404.276 -22.22 2.14780 0.13 4 6 2 o 3158.876 1307.839 -171.81 2.11210 0.21 6 4 2 o 3915.358 2203.216 160.13 2.10683 0.25 1 9 1 o 5433.076 3603.445 50.05 2.09770 0.53 9 1 1 o 3047.311 1512.305 173.78 2.07729 0.29 1 3 3 o 18750.711 11850.012 64.96 2.05566 0.72 3 1 3 o 17229.789 10745.474 151.37 2.05371 0.66 3 9 1 o 639.747 397.470 -71.93 2.00978 0.06 6 8 0 o 4272.579 2863.439 0.00 1.99841 0.23 9 3 1 o 900.659 739.830 159.13 1.99358 0.08 8 6 0 o 9789.600 8259.999 -180.00 1.99217 0.52 3 3 3 o 49277.52 36745.74 19.46 1.97271 1.87 2 10 0 o 5510.836 5386.895 180.00 1.96670 0.28 2 8 2 o 8594.339 8469.047 -24.11 1.94908 0.52 10 2 0 o 7707.589 8632.337 -180.00 1.94652 0.39 8 2 2 o 14480.342 13392.675 -4.37 1.93673 0.87 7 7 1 o 7290.444 5649.548 117.79 1.92561 0.63 6 6 2 o 2193.627 1552.454 157.38 1.90705 0.13 1 5 3 o 3147.698 1921.149 35.01 1.90214 0.12 5 1 3 o 2542.934 1133.228 26.24 1.89752 0.09 5 9 1 o 1564.215 971.570 -59.87 1.86271 0.13 4 10 0 o 560.926 364.712 180.00 1.86011 0.03 9 5 1 o 2727.232 2296.726 11.82 1.85263 0.22 4 8 2 o 12274.248 9871.997 108.25 1.84518 0.70 10 4 0 o 1100.197 886.513 0.00 1.84512 0.05 8 4 2 o 16720.748 13671.585 54.58 1.83678 0.95 3 5 3 o 11437.365 9292.874 36.32 1.83585 0.42 5 3 3 o 24797.629 19749.498 169.21 1.83308 0.91 8 8 0 o 149263.77 147230.44 0.00 1.76360 6.30 1 11 1 o 7850.916 9089.678 -111.25 1.74980 0.58 11 1 1 o 7996.683 7509.882 162.91 1.73204 0.58 1 7 3 o 3807.865 3940.446 87.97 1.72517 0.14 5 5 3 o 109869.16 97491.63 17.68 1.72172 3.91 7 1 3 o 54.322 50.796 -161.68 1.71830 0.00 6 10 0 o 50081.07 49676.92 0.00 1.71545 2.01 0 10 2 o 34039.492 34917.961 7.04 1.70874 0.90 10 6 0 o 51991.80 49846.52 0.00 1.70646 2.07 6 8 2 o 8869.669 8209.714 -104.79 1.70372 0.47 10 0 2 o 35080.49 31710.258 -58.87 1.69491 0.91 7 9 1 o 10026.033 8423.463 135.50 1.69232 0.70 8 6 2 o 17331.240 15881.334 43.11 1.69985 0.91 3 11 1 o 7227.721 6916.353 -91.25 1.69778 0.51 9 7 1 o 16630.402 14152.348 -71.92 1.68798 1.16 2 10 2 o 25069.318 21167.836 85.68 1.68395 1.30 11 3 1 o 4866.483 4154.418 -32.35 1.68261 0.34 3 7 3 o 7262.893 5924.409 38.52 1.67526 0.25 0 12 0 o 14440.447 12812.660 0.00 1.67210 0.28 10 2 2 o 25785.770 23092.834 54.80 1.67123 1.32 7 3 3 o 6494.321 5774.615 75.37 1.67001 0.23 12 0 0 o 15236.190 12173.120 0.00 1.65352 0.29 2 12 0 o 706.330 379.653 -180.00 1.64885 0.03 12 2 0 o 3695.722 2971.605 0.00 1.63151 0.14 0 0 4 o 106925.77 85583.70 132.33 1.62985 0.62 4 10 2 o 8516.020 7819.019 4.46 1.61558 0.42 5 11 1 o 7847.579 6798.628 -149.33 1.60631 0.51 10 4 2 o 9365.355 8224.772 -42.68 1.60573 0.46 11 5 1 o 12233.568 11488.566 -147.44 1.59526 0.78 2 2 4 o 4352.912 3370.401 -173.94 1.58802 0.10 5 7 3 o 15860.108 12232.025 -21.17 1.58719 0.54 7 5 3 o 13723.818 11239.409 -114.92 1.58451 0.47 4 12 0 o 1800.993 1475.088 0.00 1.58450 0.06 12 4 0 o 6292.128 8076.170 0.00 1.57041 0.22 8 10 0 o 14941.134 13746.632 0.00 1.55997 0.51 10 8 0 o 23845.273 21381.324 -180.00 1.55615 0.81 1 9 3 o 34.517 27.755 35.56 1.55141 0.00 8 8 2 o 16159.751 12842.312 80.96 1.55113 0.77 0 4 4 o 14788.717 11434.120 -57.03 1.55008 0.17 4 0 4 o 17423.861 12816.168 -6.92 1.54841 0.20 9 1 3 o 1929.499 1024.902 111.74 1.54309 0.06 2 4 4 o 1099.479 477.503 -163.33 1.53150 0.03 4 2 4 o 1762.674 857.590 -74.62 1.53029 0.04 9 9 1 o 3168.043 3116.891 110.90 1.52420 0.19 6 10 2 o 17332.186 17658.498 70.54 1.51807 0.80 3 9 3 o 9575.173 8344.205 -49.40 1.51481 0.32 10 6 2 o 22966.252 19133.502 79.19 1.51183 1.06 9 3 3 o 7692.064 5584.655 -94.83 1.50783 0.25 1 13 1 o 1507.764 1630.461 164.64 1.49767 0.09 7 11 1 o 3559.792 4387.464 -58.10 1.49317 0.21 6 12 0 o 638.010 764.192 0.00 1.49220 0.02 11 7 1 o 4180.833 4126.136 -70.04 1.48649 0.24 12 6 0 o 79.968 94.326 0.00 1.48224 0.00 13 1 1 o 333.434 395.352 65.94 1.48208 0.02 4 4 4 o 8531.173 9410.271 114.42 1.47953 0.19 7 7 3 o 28443.297 28173.379 21.14 1.47778 0.92 2 12 2 o 17269.406 16760.965 6.04 1.47133 0.77 3 13 1 o 16832.627 17868.975 -126.03 1.46467 0.94 12 2 2 o 15174.342 14271.178 -38.28 1.45897 0.67 13 3 1 o 21223.680 21696.313 -171.66 1.45076 1.17 2 6 4 o 24505.178 23241.176 -48.67 1.44939 0.55 5 9 3 o 7013.385 6393.113 -18.27 1.44876 0.23 6 2 4 o 27870.797 22915.668 -30.74 1.44666 0.63 9 5 3 o 4902.378 4070.537 79.72 1.44401 0.16 4 12 2 o 27559.650 27605.914 69.28 1.42506 1.19 2 14 0 o 11720.662 12938.354 0.00 1.41850 0.34 12 4 2 o 22317.396 21665.523 56.69 1.41478 0.96 10 10 0 o 19240.576 23118.053 0.00 1.41088 0.55 8 10 2 o 9779.490 9269.081 -67.75 1.40713 0.42 4 6 4 o 3776.563 3873.673 166.84 1.40511 0.08 5 13 1 o 26120.836 27012.416 -38.43 1.40472 1.38 10 8 2 o 15763.712 16277.526 26.88 1.40433 0.67 6 4 4 o 10405.781 10631.099 -57.65 1.40355 0.23 14 2 0 o 2905.183 2964.056 0.00 1.40337 0.08 1 11 3 o 2353.688 2060.805 -65.81 1.39370 0.07 13 5 1 o 17863.482 15647.032 -86.25 1.39365 0.93 8 12 0 o 2541.559 2559.532 0.00 1.38646 0.07 11 1 3 o 8576.515 8752.604 -31.16 1.38467 0.27 12 8 0 o 1585.418 2398.265 0.00 1.38052 0.04 4 14 0 o 4221.270 4819.816 -180.00 1.37691 0.12 9 11 1 o 16363.172 16838.090 71.65 1.37387 0.83 11 9 1 o 19317.266 19245.104 -2.84 1.37097 0.98 3 11 3 o 6583.073 5380.871 -118.26 1.36698 0.20 0 8 4 o 108052.88 88342.66 -32.95 1.36665 1.20 7 9 3 o 14661.132 12353.698 -44.44 1.36412 0.45 14 4 0 o 17418.832 14557.398 0.00 1.36391 0.47 8 0 4 o 101255.08 78894.98 -23.85 1.36209 1.13 9 7 3 o 8149.917 6356.111 -120.59 1.36185 0.25 11 3 3 o 14924.076 12582.894 125.72 1.35902 0.46 6 12 2 o 3270.802 2478.865 -37.69 1.35680 0.13 2 8 4 o 4335.135 3355.286 159.56 1.35386 0.10 8 2 4 o 9150.064 8182.509 -26.49 1.34970 0.20 12 6 2 o 8485.083 7612.072 18.59 1.34929 0.35 6 6 4 o 10573.512 6096.920 150.70 1.33954 0.23 7 13 1 o 18333.350 15226.033 77.19 1.32716 0.89 13 7 1 o 18727.320 16558.471 -5.14 1.31936 0.90 5 11 3 o 20997.211 18354.711 -71.13 1.31786 0.64 4 8 4 o 1464.080 1291.096 6.07 1.31756 0.03 6 14 0 o 10931.195 11093.996 180.00 1.31504 0.28 8 4 4 o 2744.305 2708.109 -17.41 1.31449 0.06 0 14 2 o 15016.264 13260.250 26.61 1.31201 0.30 11 5 3 o 21058.475 18543.660 -77.83 1.31174 0.64 1 15 1 o 5823.755 6856.667 -111.17 1.30753 0.28 14 6 0 o 5544.264 5925.166 -180.00 1.30495 0.14 2 14 2 o 541.490 516.732 114.47 1.30069 0.02 14 0 2 o 12398.720 11326.372 -103.78 1.29976 0.24 1 1 5 o 9262.342 7601.402 -99.93 1.29835 0.15 10 10 2 o 24178.098 22262.936 -115.89 1.29480 0.94 15 1 1 o 3560.136 3562.576 142.89 1.29370 0.17 14 2 2 o 1662.148 1723.773 -22.23 1.28899 0.06 3 15 1 o 10174.572 12380.184 -6.89 1.28540 0.47 10 12 0 o 9674.949 12162.306 0.00 1.27864 0.24 1 3 5 o 326.632 355.709 -172.31 1.27713 0.01 3 1 5 o 775.242 816.051 129.38 1.27667 0.01 12 10 0 o 8771.173 9042.639 -180.00 1.27606 0.22 8 12 2 o 11948.898 12313.759 -80.52 1.27585 0.46 15 3 1 o 13185.549 15308.413 -107.67 1.27271 0.60 9 9 3 o 4640.559 4933.617 -6.07 1.27137 0.14 12 8 2 o 9614.729 10152.550 -139.39 1.27121 0.37 4 14 2 o 13.743 15.514 -95.78 1.26839 0.00 6 8 4 o 5460.093 5606.557 161.23 1.26305 0.12 8 6 4 o 5435.771 5962.383 -61.53 1.26147 0.12 11 11 1 o 491.198 632.559 -64.81 1.25849 0.02 14 4 2 o 1178.528 1453.029 10.47 1.25821 0.04 3 3 5 o 27727.635 28741.359 -87.95 1.25648 0.44 1 13 3 o 2632.728 2786.373 -14.24 1.25585 0.08 2 10 4 o 45035.80 51404.19 -27.55 1.25493 0.98 0 16 0 o 18831.504 24470.926 0.00 1.25407 0.23 7 11 3 o 986.805 1393.312 110.33 1.25319 0.03 10 2 4 o 32241.135 41424.97 -41.31 1.24964 0.70 11 7 3 o 3236.551 4201.865 -105.12 1.24923 0.09 5 15 1 o 7107.559 10931.363 6.75 1.24430 0.32 2 16 0 o 13905.313 21556.268 -180.00 1.24417 0.33 13 1 3 o 6484.745 8400.061 52.36 1.24662 0.19 9 13 1 o 1800.917 3516.264 -112.03 1.24128 0.08 8 14 0 o 4200.376 8472.486 0.00 1.24094 0.10 16 0 0 o 4643.699 10385.307 0.00 1.24014 0.05 1 5 5 o 2405.583 3893.672 -20.84 1.23765 0.04 13 9 1 o 4932.603 6762.132 -7.40 1.23659 0.22 5 1 5 o 642.262 870.048 -133.02 1.23638 0.01 3 13 3 o 25445.760 34302.695 -80.51 1.23620 0.74 14 8 0 o 3325.213 4628.726 -180.00 1.23393 0.08 15 5 1 o 8527.488 11906.238 75.74 1.23363 0.38 16 2 0 o 21500.316 30731.535 0.00 1.23078 0.50 13 3 3 o 24567.408 26618.822 -64.93 1.22780 0.71 4 10 4 o 785.064 1005.087 132.88 1.22585 0.02 10 4 4 o 1910.368 2479.083 -12.49 1.22153 0.04 6 14 2 o 4368.578 4737.646 -72.99 1.21954 0.16 3 5 5 o 9509.550 9471.530 -145.97 1.21883 0.15 5 3 5 o 3821.549 3576.934 136.51 1.21802 0.06 4 16 0 o 800.949 657.630 180.00 1.21582 0.02 14 6 2 o 7264.121 6261.661 -123.23 1.21148 0.27 _reflns_number_total 222 _reflns_limit_h_min 0 _reflns_limit_h_max 25 _reflns_limit_k_min 0 _reflns_limit_k_max 25 _reflns_limit_l_min 0 _reflns_limit_l_max 8 _reflns_d_resolution_high 1.211 _reflns_d_resolution_low 7.054 #--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--#