#======================================================================= data_global _audit_update_record ; 2011-09-18 # Formatted by publCIF ; #======================================================================= _audit_creation_method 'Jana2006 Version : 22/10/2010' # 1. PROCESSING SUMMARY (IUCr Office Use Only) _journal_date_recd_electronic ? _journal_date_to_coeditor ? _journal_date_from_coeditor ? _journal_date_accepted ? _journal_date_printers_first ? _journal_date_printers_final ? _journal_date_proofs_out ? _journal_date_proofs_in ? _journal_coeditor_name ? _journal_coeditor_code ? _journal_coeditor_notes ? _journal_techeditor_code ? _journal_paper_category ? _journal_techeditor_notes ? _journal_coden_ASTM ? _journal_name_full ? _journal_year ? _journal_volume ? _journal_issue ? _journal_page_first ? _journal_page_last ? _journal_suppl_publ_number ? _journal_suppl_publ_pages ? #======================================================================= # 2. SUBMISSION DETAILS _publ_contact_author_name ? _publ_contact_author_address ? _publ_contact_author_email ? _publ_contact_author_fax ? _publ_contact_author_phone ? _publ_requested_journal ? _publ_requested_category ? _publ_contact_letter ? #======================================================================= # 3. TITLE AND AUTHOR LIST _publ_section_title ; Title (type here to add) ; _publ_section_title_footnote . loop_ _publ_author_name _publ_author_footnote _publ_author_address ? # name ; ? # footnote ; ; ? # address ; #======================================================================= # 4. TEXT _publ_section_synopsis . _publ_section_abstract ; (type here to add abstract) ; _publ_section_comment ; (type here to add) ; _publ_section_introduction ? _publ_section_experimental ? _publ_section_exptl_prep ; (type here to add preparation details) ; _publ_section_exptl_refinement ; (type here to add refinement details) ; _publ_section_exptl_solution ? _publ_section_discussion ? _publ_section_acknowledgements ; ? ; _publ_section_references ; (type here to add) ; _publ_section_figure_captions ; ; _publ_section_table_legends ? #======================================================================= data_I _atom_sites_solution_secondary difmap #Added by publCIF _atom_sites_solution_primary direct #Added by publCIF #======================================================================= # 5. CHEMICAL DATA _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_moiety ? _chemical_formula_structural ? _chemical_formula_analytical ? _chemical_formula_iupac ? _chemical_formula_sum 'K1.881 O20.922 Si5 U2' _chemical_formula_weight 1024.8 _chemical_melting_point ? _chemical_compound_source ? _chemical_absolute_configuration . #======================================================================= # 6. CRYSTAL DATA _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M 'C 1 2/m 1' _symmetry_space_group_name_Hall '-C 2y' loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz 1 x,y,z 2 -x,y,-z 3 -x,-y,-z 4 x,-y,z 5 x+1/2,y+1/2,z 6 -x+1/2,y+1/2,-z 7 -x+1/2,-y+1/2,-z 8 x+1/2,-y+1/2,z _cell_length_a 14.1957(4) _cell_length_b 14.2291(5) _cell_length_c 9.6305(3) _cell_angle_alpha 90 _cell_angle_beta 111.578(3) _cell_angle_gamma 90 _cell_volume 1808.95(11) _cell_formula_units_Z 4 _cell_measurement_reflns_used 4675 _cell_measurement_theta_min 2.857 _cell_measurement_theta_max 29.319 _cell_measurement_temperature 298.1 _cell_special_details ? _exptl_crystal_density_diffrn 3.7615 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 1828 _exptl_absorpt_coefficient_mu 18.80 _exptl_crystal_description ? _exptl_crystal_size_max 0.1218 _exptl_crystal_size_mid 0.0708 _exptl_crystal_size_min 0.0342 _exptl_crystal_size_rad ? _exptl_crystal_colour yellow _exptl_absorpt_correction_type analytical _exptl_absorpt_process_details ? _exptl_absorpt_correction_T_min 0.265 _exptl_absorpt_correction_T_max 0.570 #======================================================================= # 7. EXPERIMENTAL DATA _exptl_special_details ? _diffrn_ambient_temperature 298.1 _diffrn_source ? _diffrn_source_power ? _diffrn_source_voltage ? _diffrn_source_current ? _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_source 'X-ray tube' _diffrn_radiation_wavelength 0.7107 _diffrn_radiation_monochromator graphite _diffrn_measurement_device 'four-cycle diffractometer' _diffrn_measurement_device_type 'Oxford Diffraction CCD' _diffrn_detector ? _diffrn_detector_area_resol_mean 10.3784 _diffrn_measurement_method ? _diffrn_measurement_specimen_support ? _diffrn_reflns_number 28069 _diffrn_reflns_theta_min 2.8573 _diffrn_reflns_theta_max 29.3190 _diffrn_reflns_theta_full ? _diffrn_measured_fraction_theta_max ? _diffrn_measured_fraction_theta_full ? _diffrn_reflns_av_R_equivalents 0.0593 _diffrn_reflns_av_sigmaI/netI 0.2377 _diffrn_reflns_limit_h_min -19 _diffrn_reflns_limit_h_max 19 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_limit_l_max 13 _diffrn_reflns_reduction_process ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? loop_ _diffrn_standard_refln_index_h _diffrn_standard_refln_index_k _diffrn_standard_refln_index_l ? ? ? #======================================================================= # 8. REFINEMENT DATA _refine_special_details ? _reflns_number_total 2379 _reflns_number_gt 1632 _reflns_threshold_expression 'I>3\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_R_factor_gt 0.0284 _refine_ls_wR_factor_gt 0.0742 _refine_ls_R_factor_all 0.0542 _refine_ls_wR_factor_ref 0.0888 _refine_ls_goodness_of_fit_ref 1.13 _refine_ls_goodness_of_fit_gt 1.15 _refine_ls_restrained_S_gt ? _refine_ls_restrained_S_all ? _refine_ls_number_reflns 2379 _refine_ls_number_parameters 154 _refine_ls_number_restraints 0 _refine_ls_number_constraints 3 _refine_ls_weighting_scheme sigma _refine_ls_weighting_details 'w=1/(\s^2^(I)+0.0016I^2^)' _refine_ls_hydrogen_treatment ? _refine_ls_shift/su_max 0.0165 _refine_ls_shift/su_mean 0.0017 _refine_diff_density_max 0.84 _refine_diff_density_min -1.27 _refine_ls_extinction_method 'none' _refine_ls_extinction_coef ? _refine_ls_abs_structure_details ? _refine_ls_abs_structure_Flack ? _refine_ls_abs_structure_Rogers ? loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source O 0.011 0.006 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' H 0.000 0.000 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Si 0.082 0.070 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' K 0.201 0.249 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' U -9.677 9.665 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Ba -0.324 2.282 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Ca 0.226 0.306 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Na 0.036 0.025 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement ? _computing_molecular_graphics ? _computing_publication_material ? #======================================================================= # 9. ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group U1 U 0.099331(18) 0.246786(16) 0.89678(3) Uani 0.01189(11) 8 1 d . . . K1 K -0.0707(2) 0 0.8602(4) Uani 0.0369(14) 4 0.951(11) d . . . K2 K 0.2460(3) 0 0.8433(5) Uani 0.054(2) 4 0.930(12) d . . . Si1 Si 0 0.3068(2) 0.5 Uani 0.0166(11) 4 1 d . . . Si2 Si 0.18748(15) 0.24984(13) 0.2495(2) Uani 0.0116(7) 8 1 d . . . Si3 Si 0.29855(17) 0.10998(14) 0.5004(2) Uani 0.0184(8) 8 1 d . . . O1 O 0.4105(4) 0.1224(4) 0.4996(7) Uani 0.033(2) 8 1 d . . . O2 O 0.0712(4) 0.2440(4) 0.1370(6) Uani 0.023(2) 8 1 d . . . O3 O 0.2472(4) 0.2551(4) 0.1367(6) Uani 0.024(2) 8 1 d . . . O4 O 0.0366(4) 0.2437(3) 0.6473(6) Uani 0.023(2) 8 1 d . . . O5 O 0.2162(4) 0.1560(4) 0.3546(6) Uani 0.027(2) 8 1 d . . . O6 O 0.2705(6) 0 0.4998(8) Uani 0.022(3) 4 1 d . . . O7 O 0.2892(4) 0.1573(4) 0.6467(6) Uani 0.026(2) 8 1 d . . . O8 O 0.1020(4) 0.1201(4) 0.9055(6) Uani 0.029(3) 8 1 d . . . O9 O 0.0990(4) 0.3727(4) 0.8972(7) Uani 0.032(3) 8 1 d . . . O10 O 0.4310(7) 0 0.8411(13) Uani 0.053(5) 4 1 d . . . O11 O -0.2624(8) 0 0.8441(14) Uani 0.059(6) 4 0.98(3) d . . . O12 O 0 0 0.5 Uiso 0.036(4) 2 0.72(3) d . . . O13 O 0 -0.079(2) 0.5 Uiso 0.036(4) 4 0.259(18) d . . . O14 O -0.0464(16) -0.0614(14) 0.602(3) Uiso 0.036(4) 8 0.281(13) d . . . O15 O -0.0917(16) -0.0636(16) 0.398(3) Uiso 0.036(4) 8 0.264(14) d . . . O16 O -0.445(2) 0 0.702(4) Uiso 0.024(11) 4 0.24(2) d . . . loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 U1 U 0.00807(16) 0.01867(17) 0.00959(17) 0.00057(11) 0.00403(12) 0.00072(11) K1 K 0.0280(18) 0.0310(17) 0.057(3) 0 0.0224(17) 0 K2 K 0.058(3) 0.040(2) 0.089(4) 0 0.055(3) 0 Si1 Si 0.0133(15) 0.0244(16) 0.0121(16) 0 0.0046(13) 0 Si2 Si 0.0094(9) 0.0180(10) 0.0080(10) 0.0011(7) 0.0038(8) -0.0010(8) Si3 Si 0.0220(12) 0.0156(10) 0.0192(12) -0.0011(8) 0.0095(10) 0.0000(8) O1 O 0.020(3) 0.030(3) 0.052(4) -0.005(3) 0.018(3) -0.002(3) O2 O 0.006(2) 0.055(4) 0.007(3) 0.000(2) 0.001(2) -0.001(2) O3 O 0.009(3) 0.055(4) 0.009(3) 0.000(2) 0.005(2) -0.001(2) O4 O 0.024(3) 0.037(3) 0.008(3) 0.003(2) 0.006(2) 0.006(2) O5 O 0.028(3) 0.026(3) 0.021(3) -0.001(3) 0.002(3) 0.011(2) O6 O 0.029(5) 0.012(4) 0.029(5) 0 0.013(4) 0 O7 O 0.036(3) 0.018(3) 0.027(4) -0.003(2) 0.016(3) -0.007(2) O8 O 0.035(4) 0.019(3) 0.040(4) -0.001(2) 0.021(3) 0.001(2) O9 O 0.036(4) 0.020(3) 0.042(4) -0.003(3) 0.016(3) -0.003(3) O10 O 0.033(6) 0.040(6) 0.073(8) 0 0.005(6) 0 O11 O 0.059(8) 0.052(7) 0.073(10) 0 0.034(7) 0 #======================================================================= # 10. MOLECULAR GEOMETRY loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag U1 O2 . 1_556 2.489(6) yes U1 O2 . 2_556 2.322(6) yes U1 O3 . 1_556 2.488(5) yes U1 O3 . 7_556 2.317(6) yes U1 O4 . . 2.235(5) yes U1 O8 . . 1.804(6) yes U1 O9 . . 1.792(6) yes K1 K1 . 2_557 2.703(4) yes K1 O8 . . 2.888(6) yes K1 O8 . 2_557 2.991(7) yes K1 O8 . 3_557 2.991(7) yes K1 O8 . 4_555 2.888(6) yes K1 O11 . . 2.668(13) yes K1 O14 . . 2.77(3) yes K1 O14 . 4_555 2.77(3) yes K2 O8 . . 2.891(7) yes K2 O8 . 4_555 2.891(7) yes K2 O10 . . 2.633(11) yes K2 O11 . 2_557 2.933(14) yes K2 O15 . 2_556 2.70(2) yes K2 O15 . 3_556 2.70(2) yes Si1 O1 . 7_556 1.620(6) yes Si1 O1 . 8_455 1.620(6) yes Si1 O4 . . 1.596(6) yes Si1 O4 . 2_556 1.596(6) yes Si2 O2 . . 1.609(5) yes Si2 O3 . . 1.607(7) yes Si2 O5 . . 1.634(6) yes Si2 O7 . 7_556 1.615(6) yes Si3 O1 . . 1.602(7) yes Si3 O5 . . 1.600(5) yes Si3 O6 . . 1.614(3) yes Si3 O7 . . 1.611(7) yes O1 O1 . 2_656 2.539(9) yes O1 O4 . 7_556 2.641(9) yes O1 O4 . 8_555 2.643(7) yes O1 O5 . . 2.636(7) yes O1 O6 . . 2.644(9) yes O1 O7 . . 2.648(10) yes O1 O16 . 1_655 2.85(2) yes O1 O16 . 2_556 2.78(3) yes O2 O2 . 2_555 2.670(7) yes O2 O3 . . 2.504(8) yes O2 O4 . 2_556 3.000(10) yes O2 O5 . . 2.649(7) yes O2 O7 . 7_556 2.683(7) yes O2 O8 . 1_554 2.998(9) yes O2 O8 . 2_556 2.929(8) yes O2 O9 . 2_556 2.952(8) yes O3 O3 . 7_555 2.667(9) yes O3 O5 . . 2.695(9) yes O3 O7 . 7_556 2.639(9) yes O3 O8 . 7_556 2.922(9) yes O3 O9 . 1_554 2.997(7) yes O3 O9 . 7_556 2.951(9) yes O4 O4 . 2_556 2.638(8) yes O4 O8 . . 2.905(8) yes O4 O9 . . 2.895(8) yes O4 O13 . 3_556 2.69(3) yes O4 O14 . 4_555 2.82(2) yes O4 O15 . 3_556 2.76(2) yes O5 O6 . . 2.586(6) yes O5 O7 . . 2.617(8) yes O5 O7 . 7_556 2.657(7) yes O5 O14 . 3_556 2.92(2) yes O6 O7 . . 2.609(7) yes O6 O7 . 4_555 2.609(7) yes O7 O15 . 3_556 2.99(2) yes O8 O15 . 3_556 2.98(3) yes O9 O10 . 5_455 2.883(9) yes O9 O11 . 5_555 2.856(12) yes O9 O16 . 5_555 2.52(2) yes O10 O10 . 2_657 2.965(14) yes O10 O16 . 1_655 2.58(4) yes O11 O16 . . 2.44(3) yes O12 O13 . . 1.13(3) yes O12 O13 . 3_556 1.13(3) yes O12 O14 . . 1.63(3) yes O12 O14 . 2_556 1.63(3) yes O12 O14 . 3_556 1.63(3) yes O12 O14 . 4_555 1.63(3) yes O12 O15 . . 1.59(2) yes O12 O15 . 2_556 1.59(2) yes O12 O15 . 3_556 1.59(2) yes O12 O15 . 4_555 1.59(2) yes O13 O13 . 3_556 2.25(5) yes O13 O14 . . 1.40(3) yes O13 O14 . 2_556 1.40(3) yes O13 O14 . 3_556 2.43(4) yes O13 O14 . 4_555 2.43(4) yes O13 O15 . . 1.33(2) yes O13 O15 . 2_556 1.33(2) yes O13 O15 . 3_556 2.42(4) yes O13 O15 . 4_555 2.42(4) yes O14 O14 . 2_556 2.75(4) yes O14 O14 . 4_555 1.75(3) yes O14 O15 . . 1.83(3) yes O14 O15 . 2_556 1.96(3) yes O14 O15 . 3_556 2.65(3) yes O14 O15 . 4_555 2.55(3) yes O15 O15 . 2_556 2.62(3) yes O15 O15 . 4_555 1.81(3) yes loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag ? ? ? ? ? ? ? ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag ? ? ? ? ? ? ? ? ? ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_D _geom_hbond_site_symmetry_H _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag ? ? ? ? ? ? ? ? ? ? ? #======================================================================= # 11. STRUCTURE-FACTOR LIST loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4615.26 6417.90 274.40 o 4 0 0 77183.08 78105.84 863.35 o 6 0 0 377372.66 406100.50 2357.12 o 8 0 0 1760.66 1961.63 239.53 o 10 0 0 251975.88 263391.19 2810.50 o 12 0 0 24495.63 26907.41 1456.91 o 14 0 0 49632.10 52148.65 2788.79 o 16 0 0 29435.36 25074.76 3308.64 o 3 1 0 6479.61 4847.81 184.25 o 5 1 0 6813.13 6273.79 237.55 o 7 1 0 1218.66 1154.87 151.35 o 9 1 0 1334.72 1266.08 179.65 o 11 1 0 84.04 60.54 191.49 < 13 1 0 249.79 1.32 325.73 < 15 1 0 286.78 -155.30 456.68 < 17 1 0 187.93 23.69 468.53 < 0 2 0 502392.50 425391.06 5470.32 o 2 2 0 35198.29 32949.57 410.62 o 4 2 0 172225.86 170587.31 1024.57 o 6 2 0 84732.12 90559.32 991.67 o 8 2 0 7292.83 7554.34 318.49 o 10 2 0 190322.80 192805.50 1849.76 o 12 2 0 14308.67 14086.74 596.85 o 14 2 0 68490.48 66687.47 2417.65 o 16 2 0 34066.53 33175.27 2699.95 o 1 3 0 8433.46 8465.73 259.27 o 3 3 0 713.23 745.56 122.40 o 5 3 0 2025.14 1565.49 157.93 o 7 3 0 29.70 -0.66 125.03 < 9 3 0 27.23 -19.08 151.35 < 11 3 0 1428.76 1475.99 225.05 o 13 3 0 312.97 -127.66 268.48 < 15 3 0 2744.84 2679.55 709.37 o 17 3 0 11.31 -540.25 887.70 < 0 4 0 490237.69 517390.16 3080.96 o 2 4 0 33604.55 34511.10 567.23 o 4 4 0 62482.64 57125.43 710.69 o 6 4 0 173581.28 178373.94 1441.11 o 8 4 0 8472.92 8517.06 305.99 o 10 4 0 59651.91 59657.59 1080.51 o 12 4 0 34009.33 37076.16 1228.57 o 14 4 0 62404.83 61631.06 3135.58 o 16 4 0 18606.91 15745.01 2426.21 o 1 5 0 6494.60 6317.88 305.33 o 3 5 0 6464.57 5618.38 273.09 o 5 5 0 3529.36 3587.00 232.95 o 7 5 0 12238.55 12421.89 465.24 o 9 5 0 25.84 -227.03 178.99 < 11 5 0 1504.62 1372.68 254.66 o 13 5 0 853.10 1908.98 426.41 o 15 5 0 84.08 -377.72 430.36 < 0 6 0 241260.64 253286.94 2815.77 o 2 6 0 33329.12 36709.63 708.71 o 4 6 0 184500.14 195250.12 1630.63 o 6 6 0 73960.80 75818.48 1100.25 o 8 6 0 852.32 1175.27 203.34 o 10 6 0 136827.19 142859.98 1837.26 o 12 6 0 7970.42 6230.36 529.07 o 14 6 0 71146.30 69040.63 3456.70 o 16 6 0 29314.36 29989.68 3799.54 o 1 7 0 5540.19 5714.45 342.18 o 3 7 0 2337.63 2262.35 215.18 o 5 7 0 5684.84 6013.86 422.46 o 7 7 0 2801.03 2989.49 279.67 o 9 7 0 1373.15 1623.39 246.11 o 11 7 0 966.26 1048.92 240.19 o 13 7 0 743.73 570.52 362.58 < 15 7 0 2759.52 3993.67 1690.51 < 0 8 0 594266.69 618430.81 4940.59 o 2 8 0 1901.61 1503.63 205.97 o 4 8 0 100423.61 102275.12 1373.34 o 6 8 0 185819.92 190283.22 2018.88 o 8 8 0 301.55 352.71 248.74 < 10 8 0 111579.36 111112.66 1643.79 o 12 8 0 11386.42 11353.23 840.98 o 14 8 0 49273.31 48570.21 2582.16 o 16 8 0 24814.01 25077.39 3852.19 o 1 9 0 3036.13 3429.07 315.86 o 3 9 0 1332.91 1304.90 261.90 o 5 9 0 13222.96 12624.57 520.51 o 7 9 0 464.49 404.70 239.53 < 9 9 0 224.50 556.05 280.98 < 11 9 0 1810.62 1784.61 432.33 o 13 9 0 93.77 -76.33 465.24 < 15 9 0 1966.91 857.43 810.05 < 0 10 0 123467.81 127832.23 2179.44 o 2 10 0 6646.16 7516.17 402.72 o 4 10 0 90458.16 90146.73 1616.81 o 6 10 0 55698.04 53071.23 1224.62 o 8 10 0 1802.81 2008.35 347.45 o 10 10 0 72333.44 72370.99 2237.35 o 12 10 0 4287.86 4170.68 755.43 o 14 10 0 44935.51 39197.69 3125.71 o 1 11 0 4217.74 4635.26 354.03 o 3 11 0 237.51 40.80 262.56 < 5 11 0 539.00 720.56 261.90 < 7 11 0 201.23 407.33 236.90 < 9 11 0 3384.84 2784.18 558.02 o 11 11 0 1722.66 727.14 609.35 < 13 11 0 141.57 -729.77 611.32 < 0 12 0 158356.42 172184.38 2911.19 o 2 12 0 1275.74 1379.26 297.44 o 4 12 0 27249.88 26918.59 908.10 o 6 12 0 56431.39 58051.30 1733.29 o 8 12 0 995.42 1338.46 387.59 o 10 12 0 39994.52 38459.36 1857.66 o 12 12 0 6423.48 6555.43 965.35 o 1 13 0 14007.15 15479.16 736.35 o 3 13 0 221.97 392.19 288.88 < 5 13 0 1373.27 829.79 359.29 < 7 13 0 2302.30 1919.51 482.35 o 9 13 0 3235.29 3905.49 631.06 o 11 13 0 5492.76 5452.55 810.71 o 13 13 0 4.28 -835.06 708.71 < 0 14 0 85462.30 90067.76 2248.54 o 2 14 0 2389.28 2460.43 419.17 o 4 14 0 38807.64 39011.46 1588.52 o 6 14 0 18404.85 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