data_NH4-K-NAT_20_publ _pd_block_id 2011-03-16T09:26|NH4-K-NAT_20|x|qw _audit_creation_method "from EXP file using GSAS2CIF" _audit_creation_date 2011-03-16T09:26 _audit_author_name x _audit_update_record ; 2011-03-16T09:26 Initial CIF as created by GSAS2CIF ; #============================================================================= # this information describes the project, paper etc. for the CIF # # Acta Cryst. Section C papers and editorial correspondence is generated # # from the information in this section # # # # (from) CIF submission form for Rietveld refinements (Acta Cryst. C) # # Version 14 December 1998 # #============================================================================= # 1. SUBMISSION DETAILS _publ_contact_author_name ? # Name of author for correspondence _publ_contact_author_address # Address of author for correspondence ; ? ; _publ_contact_author_email ? _publ_contact_author_fax ? _publ_contact_author_phone ? _publ_contact_letter ; ? ; _publ_requested_journal ? _publ_requested_coeditor_name ? _publ_requested_category ? # Acta C: one of CI/CM/CO/FI/FM/FO #============================================================================== # 2. PROCESSING SUMMARY (IUCr Office Use Only) _journal_data_validation_number ? _journal_date_recd_electronic ? _journal_date_to_coeditor ? _journal_date_from_coeditor ? _journal_date_accepted ? _journal_date_printers_first ? _journal_date_printers_final ? _journal_date_proofs_out ? _journal_date_proofs_in ? _journal_coeditor_name ? _journal_coeditor_code ? _journal_coeditor_notes ; ? ; _journal_techeditor_code ? _journal_techeditor_notes ; ? ; _journal_coden_ASTM ? _journal_name_full ? _journal_year ? _journal_volume ? _journal_issue ? _journal_page_first ? _journal_page_last ? _journal_paper_category ? _journal_suppl_publ_number ? _journal_suppl_publ_pages ? #============================================================================== # 3. TITLE AND AUTHOR LIST _publ_section_title ; ? ; _publ_section_title_footnote ; ? ; # The loop structure below should contain the names and addresses of all # authors, in the required order of publication. Repeat as necessary. loop_ _publ_author_name _publ_author_footnote _publ_author_address ? #<--'Last name, first name' ; ? ; ; ? ; #============================================================================== # 4. TEXT _publ_section_synopsis ; ? ; _publ_section_abstract ; ? ; _publ_section_comment ; ? ; _publ_section_exptl_prep # Details of the preparation of the sample(s) # should be given here. ; ? ; _publ_section_exptl_refinement ; ? ; _publ_section_references ; ? ; _publ_section_figure_captions ; ? ; _publ_section_acknowledgements ; ? ; #============================================================================= # 5. OVERALL REFINEMENT & COMPUTING DETAILS _refine_special_details ; ? ; _pd_proc_ls_special_details ; ? ; # The following items are used to identify the programs used. _computing_molecular_graphics ? _computing_publication_material ? _refine_ls_weighting_scheme ? _refine_ls_weighting_details ? _refine_ls_hydrogen_treatment ? _refine_ls_extinction_method ? _refine_ls_extinction_coef ? _refine_ls_number_constraints ? _refine_ls_restrained_S_all ? _refine_ls_restrained_S_obs ? #============================================================================== # 6. SAMPLE PREPARATION DATA # (In the unusual case where multiple samples are used in a single # Rietveld study, this information should be moved into the phase # blocks) # The following three fields describe the preparation of the material. # The cooling rate is in K/min. The pressure at which the sample was # prepared is in kPa. The temperature of preparation is in K. _pd_prep_cool_rate ? _pd_prep_pressure ? _pd_prep_temperature ? _pd_char_colour ? # use ICDD colour descriptions _refine_ls_shift/su_max 4.92 _refine_ls_shift/su_mean 0.69 _computing_structure_refinement GSAS _refine_ls_number_parameters 46 _refine_ls_goodness_of_fit_all 1.62 _refine_ls_number_restraints 28 _refine_ls_matrix_type full #============================================================================== # 7. CHEMICAL, STRUCTURAL AND CRYSTAL DATA _pd_char_particle_morphology ? _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_formula_moiety ? _chemical_formula_structural ? _chemical_formula_analytical ? _chemical_melting_point ? _chemical_compound_source ? # for minerals and # natural products _symmetry_space_group_name_Hall ? _exptl_crystal_F_000 ? _exptl_crystal_density_diffrn ? _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _cell_measurement_temperature ? _cell_special_details ; ? ; _geom_special_details ? # The following item identifies the program(s) used (if appropriate). _computing_structure_solution ? #============================================================================== # 8. Phase information from GSAS _pd_phase_name NH4-K-NAT_20 _cell_length_a 19.55532(23) _cell_length_b 19.94423(21) _cell_length_c 6.49509(7) _cell_angle_alpha 90.0 _cell_angle_beta 90.0 _cell_angle_gamma 90.0 _cell_volume 2533.19(5) _symmetry_cell_setting orthorhombic _symmetry_space_group_name_H-M "F d d 2" loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz 1 +x,+y,+z 2 -x+1/4,+y+1/4,+z+1/4 3 +x+1/4,-y+1/4,+z+1/4 4 -x,-y+1/2,+z+1/2 101 +x,+y+1/2,+z+1/2 102 -x+1/4,+y+3/4,+z+3/4 103 +x+1/4,-y+3/4,+z+3/4 104 -x,-y,+z 201 +x+1/2,+y,+z+1/2 202 -x+3/4,+y+1/4,+z+3/4 203 +x+3/4,-y+1/4,+z+3/4 204 -x+1/2,-y+1/2,+z 301 +x+1/2,+y+1/2,+z 302 -x+3/4,+y+3/4,+z+1/4 303 +x+3/4,-y+3/4,+z+1/4 304 -x+1/2,-y,+z+1/2 # ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_occupancy _atom_site_thermal_displace_type _atom_site_U_iso_or_equiv _atom_site_symmetry_multiplicity Si Si1 0.0 0.0 0.0064(10) 1.0 Uiso 0.0043(5) 8 Si Si2 0.17232(11) 0.19354(12) 0.6271(9) 1.0 Uiso 0.0043(5) 16 Al Al 0.05699(12) 0.07473(11) 0.6198(9) 1.0 Uiso 0.0043(5) 16 O O1 0.05046(18) 0.04669(20) 0.8715(9) 1.0 Uiso 0.0192(10) 16 O O2 0.10487(17) 0.14717(16) 0.6026(11) 1.0 Uiso 0.0192(10) 16 O O3 0.09649(19) 0.01754(16) 0.4597(10) 1.0 Uiso 0.0192(10) 16 O O4 0.22571(16) 0.15626(19) 0.7780(10) 1.0 Uiso 0.0192(10) 16 O O5 0.20344(19) 0.20093(18) 0.3967(9) 1.0 Uiso 0.0192(10) 16 K K 0.15793(21) 0.09358(22) 0.1267(13) 0.683(8) Uiso 0.0644(23) 16 N N 0.1284(16) 0.1353(20) 0.129(8) 0.317(8) Uiso 0.0644(23) 16 O OW1A 0.2505(7) 0.0027(7) 0.5965(26) 0.630(11) Uiso 0.0618(23) 16 O OW1B 0.2773(10) 0.0463(11) 0.482(4) 0.354(11) Uiso 0.0618(23) 16 # If you change Z, be sure to change all 3 of the following _chemical_formula_sum "Al2 K1.37 N0.63 O11.97 Si3" _chemical_formula_weight 391.99 _cell_formula_units_Z 8 # MOLECULAR GEOMETRY loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_publ_flag Si1 O1 1.6150(11) . 1_554 N Si1 O1 1.6150(11) . 104_554 N Si1 O3 3.514(5) . 1_555 N Si1 O3 3.514(5) . 104_555 N Si1 O4 3.657(5) . 102_543 N Si1 O4 3.657(5) . 203_453 N Si1 O5 1.6179(11) . 102_544 N Si1 O5 1.6179(11) . 203_454 N Si1 K 3.692(4) . 1_555 N Si1 K 3.699(4) . 102_544 N Si1 K 3.692(4) . 104_555 N Si1 K 3.699(4) . 203_454 N Si2 Al 3.0814(27) . 2_555 N Si2 Al 3.0909(26) . 3_555 N Si2 O2 1.6187(15) . 1_555 N Si2 O3 1.6129(15) . 2_555 N Si2 O3 3.534(5) . 3_555 N Si2 O4 1.6135(15) . 1_555 N Si2 O5 1.6220(15) . 1_555 N Si2 O5 3.5458(35) . 204_555 N Si2 K 3.823(6) . 1_555 N Si2 K 3.819(6) . 1_556 N Si2 K 3.750(5) . 2_555 N Al Si2 3.0814(27) . 102_544 N Al Si2 3.0909(26) . 203_454 N Al O1 1.7328(15) . 1_555 N Al O1 3.5990(34) . 104_555 N Al O2 1.7251(15) . 1_555 N Al O3 1.7260(15) . 1_555 N Al O3 3.671(5) . 104_555 N Al O4 3.472(5) . 102_544 N Al O4 1.7395(15) . 203_454 N Al O5 3.715(4) . 203_454 N Al K 3.781(6) . 1_555 N Al K 3.857(6) . 1_556 N Al K 3.733(5) . 203_455 N Al OW1B 3.647(21) . 203_454 N O1 Si1 1.6150(11) . 1_556 N O1 Al 1.7328(15) . 1_555 N O1 Al 3.5990(34) . 104_555 N O1 O1 2.714(5) . 104_555 N O1 O2 2.863(4) . 1_555 N O1 O3 2.881(4) . 1_555 N O1 O3 3.968(5) . 1_556 N O1 O3 4.130(5) . 104_555 N O1 O4 4.110(4) . 1_555 N O1 O4 3.617(6) . 102_544 N O1 O4 2.828(4) . 203_454 N O1 O5 2.6169(31) . 102_545 N O1 O5 2.6071(32) . 203_455 N O1 K 2.835(6) . 1_556 N O1 K 4.132(5) . 102_545 N O1 K 3.544(7) . 203_455 N O1 N 2.87(4) . 1_556 N O1 OW1A 4.230(16) . 2_555 N O1 OW1A 4.271(14) . 304_555 N O1 OW1B 3.935(27) . 203_455 N O1 OW1B 3.911(20) . 304_555 N O2 Si2 1.6187(15) . 1_555 N O2 Al 1.7251(15) . 1_555 N O2 O1 2.863(4) . 1_555 N O2 O3 2.752(4) . 1_555 N O2 O3 2.6744(33) . 2_555 N O2 O4 2.629(4) . 1_555 N O2 O4 2.7839(34) . 203_454 N O2 O5 2.579(4) . 1_555 N O2 K 3.431(8) . 1_555 N O2 K 3.716(8) . 1_556 N O2 K 4.191(6) . 2_555 N O2 K 4.247(6) . 203_455 N O2 N 3.12(5) . 1_555 N O2 OW1A 4.053(13) . 1_555 N O2 OW1A 3.344(16) . 2_555 N O2 OW1A 3.305(16) . 203_454 N O2 OW1B 4.005(19) . 1_555 N O2 OW1B 4.030(22) . 2_555 N O2 OW1B 3.061(23) . 203_454 N O3 Si1 3.514(5) . 1_555 N O3 Si2 1.6129(15) . 102_544 N O3 Si2 3.534(5) . 203_454 N O3 Al 1.7260(15) . 1_555 N O3 Al 3.671(5) . 104_555 N O3 O1 3.968(5) . 1_554 N O3 O1 2.881(4) . 1_555 N O3 O1 4.130(5) . 104_555 N O3 O2 2.752(4) . 1_555 N O3 O2 2.6744(33) . 102_544 N O3 O3 3.838(7) . 104_555 N O3 O4 4.279(4) . 1_555 N O3 O4 2.667(4) . 102_544 N O3 O4 2.843(4) . 203_454 N O3 O5 4.233(4) . 1_555 N O3 O5 2.617(4) . 102_544 N O3 O5 3.515(5) . 203_454 N O3 K 2.902(6) . 1_555 N O3 K 4.745(6) . 1_556 N O3 K 4.402(6) . 102_545 N O3 N 3.24(5) . 1_555 N O3 OW1A 3.155(13) . 1_555 N O3 OW1A 3.831(14) . 304_554 N O3 OW1B 3.586(20) . 1_555 N O3 OW1B 4.219(21) . 203_454 N O3 OW1B 4.165(24) . 304_554 N O4 Si1 3.657(5) . 2_556 N O4 Si2 1.6135(15) . 1_555 N O4 Al 3.472(5) . 2_555 N O4 Al 1.7395(15) . 3_555 N O4 O1 4.110(4) . 1_555 N O4 O1 3.617(6) . 2_555 N O4 O1 2.828(4) . 3_555 N O4 O2 2.629(4) . 1_555 N O4 O2 2.7839(34) . 3_555 N O4 O3 4.279(4) . 1_555 N O4 O3 2.667(4) . 2_555 N O4 O3 2.843(4) . 3_555 N O4 O4 3.858(7) . 204_555 N O4 O5 2.668(4) . 1_555 N O4 O5 4.139(5) . 1_556 N O4 O5 4.021(5) . 204_555 N O4 K 4.606(7) . 1_555 N O4 K 2.907(6) . 1_556 N O4 K 4.415(6) . 3_555 N O4 N 3.00(5) . 1_556 N O4 OW1A 3.318(15) . 1_555 N O4 OW1A 3.813(14) . 304_555 N O4 OW1B 3.087(22) . 1_555 N O4 OW1B 4.252(21) . 304_555 N O5 Si1 1.6179(11) . 2_555 N O5 Si2 1.6220(15) . 1_555 N O5 Si2 3.5458(35) . 204_555 N O5 Al 3.715(4) . 3_555 N O5 O1 2.6169(31) . 2_554 N O5 O1 2.6071(32) . 3_554 N O5 O2 2.579(4) . 1_555 N O5 O3 4.233(4) . 1_555 N O5 O3 2.617(4) . 2_555 N O5 O3 3.515(5) . 3_555 N O5 O4 4.139(5) . 1_554 N O5 O4 2.668(4) . 1_555 N O5 O4 4.021(5) . 204_555 N O5 O5 2.674(5) . 204_555 N O5 K 2.907(6) . 1_555 N O5 K 3.585(6) . 2_555 N O5 K 4.098(6) . 3_555 N O5 N 2.63(4) . 1_555 N O5 OW1A 4.263(16) . 1_555 N O5 OW1A 4.087(14) . 203_454 N O5 OW1B 3.450(22) . 1_555 N O5 OW1B 3.607(19) . 203_454 N K Si1 3.692(4) . 1_555 N K Si1 3.699(4) . 2_555 N K Si2 3.819(6) . 1_554 N K Si2 3.823(6) . 1_555 N K Si2 3.750(5) . 102_544 N K Al 3.857(6) . 1_554 N K Al 3.781(6) . 1_555 N K Al 3.733(5) . 3_554 N K O1 2.835(6) . 1_554 N K O1 4.132(5) . 2_554 N K O1 3.544(7) . 3_554 N K O2 3.716(8) . 1_554 N K O2 3.431(8) . 1_555 N K O2 4.247(6) . 3_554 N K O2 4.191(6) . 102_544 N K O3 4.745(6) . 1_554 N K O3 2.902(6) . 1_555 N K O3 4.402(6) . 2_554 N K O4 2.907(6) . 1_554 N K O4 4.606(7) . 1_555 N K O4 4.415(6) . 203_454 N K O5 2.907(6) . 1_555 N K O5 3.585(6) . 102_544 N K O5 4.098(6) . 203_454 N K N 1.01(4) . 1_555 N K OW1A 4.293(17) . 1_554 N K OW1A 3.985(17) . 1_555 N K OW1A 4.573(18) . 203_454 N K OW1A 2.632(12) . 304_554 N K OW1B 3.415(24) . 1_555 N K OW1B 3.436(24) . 203_454 N K OW1B 3.205(23) . 304_554 N N O1 2.87(4) . 1_554 N N O2 3.12(5) . 1_555 N N O3 3.24(5) . 1_555 N N O4 3.00(5) . 1_554 N N O5 2.63(4) . 1_555 N N K 1.01(4) . 1_555 N N OW1B 2.49(5) . 203_454 N OW1A O1 4.230(16) . 102_544 N OW1A O1 4.271(14) . 304_554 N OW1A O2 4.053(13) . 1_555 N OW1A O2 3.305(16) . 3_555 N OW1A O2 3.344(16) . 102_544 N OW1A O3 3.155(13) . 1_555 N OW1A O3 3.831(14) . 304_555 N OW1A O4 3.318(15) . 1_555 N OW1A O4 3.813(14) . 304_554 N OW1A O5 4.263(16) . 1_555 N OW1A O5 4.087(14) . 3_555 N OW1A K 3.985(17) . 1_555 N OW1A K 4.293(17) . 1_556 N OW1A K 4.573(18) . 3_555 N OW1A K 2.632(12) . 304_555 N OW1A OW1A 3.2493(10) . 304_554 N OW1A OW1A 3.2493(10) . 304_555 N OW1A OW1B 1.260(23) . 1_555 N OW1A OW1B 4.146(32) . 304_554 N OW1A OW1B 2.741(29) . 304_555 N OW1B Al 3.647(21) . 3_555 N OW1B O1 3.935(27) . 3_554 N OW1B O1 3.911(20) . 304_554 N OW1B O2 4.005(19) . 1_555 N OW1B O2 3.061(23) . 3_555 N OW1B O2 4.030(22) . 102_544 N OW1B O3 3.586(20) . 1_555 N OW1B O3 4.219(21) . 3_555 N OW1B O3 4.165(24) . 304_555 N OW1B O4 3.087(22) . 1_555 N OW1B O4 4.252(21) . 304_554 N OW1B O5 3.450(22) . 1_555 N OW1B O5 3.607(19) . 3_555 N OW1B K 3.415(24) . 1_555 N OW1B K 3.436(24) . 3_555 N OW1B K 3.205(23) . 304_555 N OW1B N 2.49(5) . 3_555 N OW1B OW1A 1.260(23) . 1_555 N OW1B OW1A 2.741(29) . 304_554 N OW1B OW1A 4.146(32) . 304_555 N OW1B OW1B 3.886(25) . 304_554 N OW1B OW1B 3.886(25) . 304_555 N loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Si1 O1 114.30(32) 1_554 . 104_543 N O1 Si1 O5 108.08(18) 1_554 . 102_544 N O1 Si1 O5 107.50(18) 1_554 . 203_454 N O1 Si1 K 46.55(14) 1_554 . 1_555 N O1 Si1 K 93.74(20) 1_554 . 102_544 N O1 Si1 K 156.54(21) 1_554 . 104_544 N O1 Si1 K 71.80(18) 1_554 . 203_454 N O1 Si1 O5 107.50(18) 104_543 . 102_544 N O1 Si1 O5 108.08(18) 104_543 . 203_454 N O1 Si1 K 156.54(21) 104_543 . 1_555 N O1 Si1 K 71.80(18) 104_543 . 102_544 N O1 Si1 K 46.55(14) 104_543 . 104_544 N O1 Si1 K 93.74(20) 104_543 . 203_454 N O5 Si1 O5 111.43(33) 102_544 . 203_454 N O5 Si1 K 73.49(18) 102_544 . 1_555 N O5 Si1 K 49.02(15) 102_544 . 102_544 N O5 Si1 K 92.62(18) 102_544 . 104_544 N O5 Si1 K 155.83(21) 102_544 . 203_454 N O5 Si1 K 92.62(18) 203_454 . 1_555 N O5 Si1 K 155.83(21) 203_454 . 102_544 N O5 Si1 K 73.49(18) 203_454 . 104_544 N O5 Si1 K 49.02(15) 203_454 . 203_454 N K Si1 K 93.864(31) 1_555 . 102_544 N K Si1 K 155.56(20) 1_555 . 104_544 N K Si1 K 91.662(30) 1_555 . 203_454 N K Si1 K 91.662(30) 102_544 . 104_544 N K Si1 K 153.68(20) 102_544 . 203_454 N K Si1 K 93.864(31) 104_544 . 203_454 N O2 Si2 O3 111.70(21) 1_555 . 2_555 N O2 Si2 O4 108.88(23) 1_555 . 1_555 N O2 Si2 O5 105.49(24) 1_555 . 1_555 N O3 Si2 O4 111.53(25) 2_555 . 1_555 N O3 Si2 O5 108.02(23) 2_555 . 1_555 N O4 Si2 O5 111.07(25) 1_555 . 1_555 N O1 Al O2 111.80(23) 1_555 . 1_555 N O1 Al O3 112.83(23) 1_555 . 1_555 N O1 Al O4 109.06(22) 1_555 . 203_454 N O1 Al K 150.44(17) 1_555 . 1_555 N O1 Al K 70.22(19) 1_555 . 203_455 N O2 Al O3 105.76(21) 1_555 . 1_555 N O2 Al O4 106.94(20) 1_555 . 203_454 N O2 Al K 65.08(21) 1_555 . 1_555 N O2 Al K 95.01(18) 1_555 . 203_455 N O3 Al O4 110.27(23) 1_555 . 203_454 N O3 Al K 47.29(16) 1_555 . 1_555 N O3 Al K 155.12(17) 1_555 . 203_455 N O4 Al K 99.50(19) 203_454 . 1_555 N O4 Al K 49.05(16) 203_454 . 203_455 N K Al K 137.98(12) 1_555 . 203_455 N Si1 O1 Al 137.98(25) 1_556 . 1_555 N Si1 O1 K 109.03(17) 1_556 . 1_556 N Al O1 K 112.99(16) 1_555 . 1_556 N Si2 O2 Al 156.11(30) 1_555 . 1_555 N Si2 O3 Al 134.68(24) 102_544 . 1_555 N Si2 O3 K 108.94(20) 102_544 . 1_555 N Al O3 K 106.79(20) 1_555 . 1_555 N Si2 O4 Al 134.36(23) 1_555 . 3_555 N Si2 O4 K 112.11(20) 1_555 . 1_556 N Al O4 K 104.08(19) 3_555 . 1_556 N Si1 O5 Si2 141.79(28) 2_555 . 1_555 N Si1 O5 K 106.14(18) 2_555 . 1_555 N Si2 O5 K 112.01(18) 1_555 . 1_555 N Si1 K Si1 151.84(13) 1_555 . 2_555 N Si1 K Al 72.08(10) 1_555 . 1_555 N Si1 K Al 141.18(18) 1_555 . 3_554 N Si1 K O1 24.43(5) 1_555 . 1_554 N Si1 K O3 63.08(12) 1_555 . 1_555 N Si1 K O4 115.71(18) 1_555 . 1_554 N Si1 K O5 139.12(17) 1_555 . 1_555 N Si1 K N 86.6(17) 1_555 . 1_555 N Si1 K OW1A 100.6(4) 1_555 . 304_544 N Si1 K OW1B 80.1(4) 1_555 . 304_544 N Si1 K Al 98.34(14) 2_555 . 1_555 N Si1 K Al 49.73(7) 2_555 . 3_554 N Si1 K O1 140.54(18) 2_555 . 1_554 N Si1 K O3 118.20(18) 2_555 . 1_555 N Si1 K O4 65.97(12) 2_555 . 1_554 N Si1 K O5 24.84(5) 2_555 . 1_555 N Si1 K N 65.3(17) 2_555 . 1_555 N Si1 K OW1A 107.52(35) 2_555 . 304_544 N Si1 K OW1B 127.5(4) 2_555 . 304_544 N Al K Al 146.07(16) 1_555 . 3_554 N Al K O1 94.33(13) 1_555 . 1_554 N Al K O3 25.92(6) 1_555 . 1_555 N Al K O4 160.20(18) 1_555 . 1_554 N Al K O5 73.86(13) 1_555 . 1_555 N Al K N 76.8(29) 1_555 . 1_555 N Al K OW1A 110.2(4) 1_555 . 304_544 N Al K OW1B 111.6(4) 1_555 . 304_544 N Al K O1 117.48(18) 3_554 . 1_554 N Al K O3 152.19(18) 3_554 . 1_555 N Al K O4 26.87(5) 3_554 . 1_554 N Al K O5 73.10(10) 3_554 . 1_555 N Al K N 95.3(20) 3_554 . 1_555 N Al K OW1A 75.75(33) 3_554 . 304_544 N Al K OW1B 86.6(4) 3_554 . 304_544 N O1 K O3 87.50(14) 1_554 . 1_555 N O1 K O4 91.39(17) 1_554 . 1_554 N O1 K O5 145.34(21) 1_554 . 1_555 N O1 K N 81.8(23) 1_554 . 1_555 N O1 K OW1A 102.7(4) 1_554 . 304_544 N O1 K OW1B 80.4(5) 1_554 . 304_544 N O3 K O4 173.86(21) 1_555 . 1_554 N O3 K O5 93.56(18) 1_555 . 1_555 N O3 K N 100.5(26) 1_555 . 1_555 N O3 K OW1A 87.5(4) 1_555 . 304_544 N O3 K OW1B 85.8(4) 1_555 . 304_544 N O4 K O5 90.79(15) 1_554 . 1_555 N O4 K N 85.3(27) 1_554 . 1_555 N O4 K OW1A 86.9(4) 1_554 . 304_544 N O4 K OW1B 88.0(4) 1_554 . 304_544 N O5 K N 63.9(24) 1_555 . 1_555 N O5 K OW1A 112.0(4) 1_555 . 304_544 N O5 K OW1B 134.2(5) 1_555 . 304_544 N N K OW1A 171.1(20) 1_555 . 304_544 N N K OW1B 160.8(29) 1_555 . 304_544 N OW1A K OW1B 22.3(4) 304_544 . 304_544 N K OW1A OW1B 105.4(13) 304_545 . 1_555 N K OW1B OW1A 52.3(10) 304_545 . 1_555 N # Powder diffraction data for histogram 1 #============================================================================== # 9. INSTRUMENT CHARACTERIZATION _exptl_special_details ; ? ; # if regions of the data are excluded, the reason(s) are supplied here: _pd_proc_info_excluded_regions ; ? ; # The following item is used to identify the equipment used to record # the powder pattern when the diffractogram was measured at a laboratory # other than the authors' home institution, e.g. when neutron or synchrotron # radiation is used. _pd_instr_location ; ? ; _pd_calibration_special_details # description of the method used # to calibrate the instrument ; ? ; _diffrn_ambient_temperature ? _diffrn_source ? _diffrn_source_target ? _diffrn_source_type ? _diffrn_measurement_device_type ? _diffrn_detector ? _diffrn_detector_type ? # make or model of detector _pd_meas_scan_method ? # options are 'step', 'cont', # 'tof', 'fixed' or # 'disp' (= dispersive) _pd_meas_special_details ; ? ; # The following two items identify the program(s) used (if appropriate). _computing_data_collection ? _computing_data_reduction ? # Describe any processing performed on the data, prior to refinement. # For example: a manual Lp correction or a precomputed absorption correction _pd_proc_info_data_reduction ? # The following item is used for angular dispersive measurements only. _diffrn_radiation_monochromator ? # The following items are used to define the size of the instrument. # Not all distances are appropriate for all instrument types. _pd_instr_dist_src/mono ? _pd_instr_dist_mono/spec ? _pd_instr_dist_src/spec ? _pd_instr_dist_spec/anal ? _pd_instr_dist_anal/detc ? _pd_instr_dist_spec/detc ? # 10. Specimen size and mounting information # The next three fields give the specimen dimensions in mm. The equatorial # plane contains the incident and diffracted beam. _pd_spec_size_axial ? # perpendicular to # equatorial plane _pd_spec_size_equat ? # parallel to # scattering vector # in transmission _pd_spec_size_thick ? # parallel to # scattering vector # in reflection _pd_spec_mounting # This field should be # used to give details of the # container. ; ? ; _pd_spec_mount_mode ? # options are 'reflection' # or 'transmission' _pd_spec_shape ? # options are 'cylinder' # 'flat_sheet' or 'irregular' loop_ _atom_type_symbol _atom_type_number_in_cell _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source Si 24.0 0.000 0.000 6.29150 2.43860 3.03530 32.3337 1.98910 0.67850 1.54100 81.6937 1.14070 International_Tables_Vol_C Al 16.0 0.000 0.000 6.42020 3.03870 1.90020 0.74260 1.59360 31.5472 1.96460 85.0886 1.11510 International_Tables_Vol_C O 95.747 0.000 0.000 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700 32.9089 0.25080 International_Tables_Vol_C K 10.928 0.000 0.000 8.21860 12.7949 7.43980 0.77480 1.05190 213.187 0.86590 41.6841 1.42280 International_Tables_Vol_C N 5.072 0.000 0.000 12.2126 0.00570 3.13220 9.89330 2.01250 28.9975 1.16630 0.58260 -11.529 International_Tables_Vol_C _diffrn_radiation_probe x-ray _diffrn_radiation_polarisn_ratio 0.95 _diffrn_radiation_wavelength 1.5494 _diffrn_radiation_type ? _pd_proc_ls_prof_R_factor 0.1141 _pd_proc_ls_prof_wR_factor 0.1482 _pd_proc_ls_prof_wR_expected 0.0951 _refine_ls_R_Fsqd_factor 0.11230 _pd_proc_ls_background_function ; GSAS Background function number 1 with 10 terms. Shifted Chebyshev function of 1st kind 1: 63.7142 2: -33.2340 3: 28.4267 4: -15.0901 5: 13.4777 6: -12.1401 7: 3.98028 8: -4.02607 9: -1.06895 10: 0.422150 ; _exptl_absorpt_process_details ; GSAS Absorption/surface roughness correction: function number 0 No correction is applied. ; _exptl_absorpt_correction_T_min 1.00000 _exptl_absorpt_correction_T_max 1.00000 # Extinction correction _gsas_exptl_extinct_corr_T_min 1.00000 _gsas_exptl_extinct_corr_T_max 1.00000 _pd_proc_ls_pref_orient_corr ; March-Dollase AXIS 1 Ratio= 1.26399 h= 0.000 k= 0.000 l= 1.000 Prefered orientation correction range: Min= 0.49536, Max= 1.42082 ; _pd_proc_ls_profile_function ; CW Profile function number 2 with 18 terms Profile coefficients for Simpson's rule integration of pseudovoigt function C.J. Howard (1982). J. Appl. Cryst.,15,615-620. P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83. #1(GU) = 0.000 #2(GV) = -27.794 #3(GW) = 4.546 #4(LX) = 1.157 #5(LY) = 17.103 #6(trns) = 0.000 #7(asym) = 0.0245 #8(shft) = 0.0000 #9(GP) = 0.000 #10(stec)= -11.78 #11(ptec)= 1.25 #12(sfec)= 0.00 #13(L11) = 0.000 #14(L22) = 0.000 #15(L33) = 0.000 #16(L12) = 0.000 #17(L13) = 0.000 #18(L23) = 0.000 Peak tails are ignored where the intensity is below 0.0010 times the peak Aniso. broadening axis 0.0 0.0 1.0 ; _pd_proc_ls_peak_cutoff 0.00100 _pd_proc_info_datetime 2011-03-16T09:26:52 _pd_calc_method "Rietveld Refinement" #---- raw/calc data loop ----- _pd_meas_2theta_range_min 10.0 _pd_meas_2theta_range_max 130.995 _pd_meas_2theta_range_inc 0.005 _pd_proc_2theta_range_min 10.00646 _pd_proc_2theta_range_max 131.00146 _pd_proc_2theta_range_inc 0.005 loop_ _pd_meas_intensity_total _pd_proc_ls_weight _pd_proc_intensity_bkg_calc _pd_calc_intensity_total 250(26) 0.0 245.9 . 325(30) 0.0 245.6 . 262(27) 0.0 245.4 . 336(30) 0.0 245.2 . 259(27) 0.0 245.0 . 297(29) 0.0 244.8 . 270(27) 0.0 244.6 . 294(28) 0.0 244.4 . 311(29) 0.0 244.1 . 296(29) 0.0 243.9 . 308(29) 0.0 243.7 . 294(28) 0.0 243.5 . 308(29) 0.0 243.3 . 312(29) 0.0 243.1 . 319(30) 0.0 242.9 . 330(30) 0.0 242.7 . 309(29) 0.0 242.4 . 315(29) 0.0 242.2 . 286(28) 0.0 242.0 . 302(29) 0.0 241.8 . 278(27) 0.0 241.6 . 279(28) 0.0 241.4 . 326(30) 0.0 241.2 . 369(32) 0.0 241.0 . 296(28) 0.0 240.8 . 291(28) 0.0 240.6 . 264(27) 0.0 240.3 . 310(29) 0.0 240.1 . 317(29) 0.0 239.9 . 325(30) 0.0 239.7 . 244(26) 0.0 239.5 . 305(29) 0.0 239.3 . 294(28) 0.0 239.1 . 259(26) 0.0 238.9 . 270(27) 0.0 238.7 . 241(25) 0.0 238.5 . 277(27) 0.0 238.3 . 283(28) 0.0 238.0 . 283(28) 0.0 237.8 . 280(27) 0.0 237.6 . 270(27) 0.0 237.4 . 305(29) 0.0 237.2 . 320(29) 0.0 237.0 . 294(28) 0.0 236.8 . 272(27) 0.0 236.6 . 254(26) 0.0 236.4 . 303(28) 0.0 236.2 . 271(27) 0.0 236.0 . 279(27) 0.0 235.8 . 269(27) 0.0 235.6 . 228(24) 0.0 235.4 . 304(28) 0.0 235.1 . 291(28) 0.0 234.9 . 248(26) 0.0 234.7 . 302(28) 0.0 234.5 . 225(24) 0.0 234.3 . 251(26) 0.0 234.1 . 278(27) 0.0 233.9 . 285(27) 0.0 233.7 . 232(25) 0.0 233.5 . 275(27) 0.0 233.3 . 259(26) 0.0 233.1 . 327(29) 0.0 232.9 . 290(27) 0.0 232.7 . 231(24) 0.0 232.5 . 220(24) 0.0 232.3 . 254(26) 0.0 232.1 . 257(26) 0.0 231.9 . 266(26) 0.0 231.7 . 284(27) 0.0 231.5 . 267(26) 0.0 231.3 . 248(25) 0.0 231.1 . 283(27) 0.0 230.9 . 246(25) 0.0 230.7 . 307(28) 0.0 230.5 . 283(27) 0.0 230.3 . 250(25) 0.0 230.1 . 233(24) 0.0 229.9 . 304(28) 0.0 229.7 . 260(26) 0.0 229.5 . 275(27) 0.0 229.2 . 276(27) 0.0 229.0 . 292(27) 0.0 228.8 . 264(26) 0.0 228.6 . 277(27) 0.0 228.4 . 289(27) 0.0 228.2 . 278(27) 0.0 228.0 . 274(26) 0.0 227.8 . 253(25) 0.0 227.6 . 269(26) 0.0 227.4 . 262(26) 0.0 227.2 . 265(26) 0.0 227.0 . 285(27) 0.0 226.8 . 248(25) 0.0 226.6 . 246(25) 0.0 226.5 . 251(25) 0.0 226.3 . 235(24) 0.0 226.1 . 241(25) 0.0 225.9 . 213(23) 0.0 225.7 . 269(26) 0.0 225.5 . 236(24) 0.0 225.3 . 231(24) 0.0 225.1 . 309(28) 0.0 224.9 . 238(24) 0.0 224.7 . 247(25) 0.0 224.5 . 234(24) 0.0 224.3 . 182(21) 0.0 224.1 . 276(26) 0.0 223.9 . 233(24) 0.0 223.7 . 250(25) 0.0 223.5 . 252(25) 0.0 223.3 . 239(24) 0.0 223.1 . 266(26) 0.0 222.9 . 230(24) 0.0 222.7 . 248(25) 0.0 222.5 . 268(26) 0.0 222.3 . 269(26) 0.0 222.1 . 253(25) 0.0 221.9 . 238(24) 0.0 221.7 . 236(24) 0.0 221.5 . 246(25) 0.0 221.3 . 291(27) 0.0 221.1 . 230(24) 0.0 220.9 . 259(25) 0.0 220.7 . 240(24) 0.0 220.6 . 235(24) 0.0 220.4 . 233(24) 0.0 220.2 . 178(21) 0.0 220.0 . 281(26) 0.0 219.8 . 257(25) 0.0 219.6 . 224(23) 0.0 219.4 . 235(24) 0.0 219.2 . 232(24) 0.0 219.0 . 246(25) 0.0 218.8 . 274(26) 0.0 218.6 . 179(21) 0.0 218.4 . 210(23) 0.0 218.2 . 197(22) 0.0 218.0 . 213(23) 0.0 217.9 . 263(25) 0.0 217.7 . 250(25) 0.0 217.5 . 227(23) 0.0 217.3 . 249(25) 0.0 217.1 . 236(24) 0.0 216.9 . 245(24) 0.0 216.7 . 258(25) 0.0 216.5 . 263(25) 0.0 216.3 . 267(25) 0.0 216.1 . 274(26) 0.0 215.9 . 228(23) 0.0 215.8 . 261(25) 0.0 215.6 . 261(25) 0.0 215.4 . 297(27) 0.0 215.2 . 227(23) 0.0 215.0 . 240(24) 0.0 214.8 . 247(24) 0.0 214.6 . 243(24) 0.0 214.4 . 219(23) 0.0 214.2 . 236(24) 0.0 214.0 . 201(22) 0.0 213.9 . 231(23) 0.0 213.7 . 212(22) 0.0 213.5 . 233(24) 0.0 213.3 . 241(24) 0.0 213.1 . 222(23) 0.0 212.9 . 223(23) 0.0 212.7 . 268(25) 0.0 212.5 . 277(26) 0.0 212.4 . 255(25) 0.0 212.2 . 225(23) 0.0 212.0 . 273(25) 0.0 211.8 . 244(24) 0.0 211.6 . 235(24) 0.0 211.4 . 274(25) 0.0 211.2 . 227(23) 0.0 211.0 . 241(24) 0.0 210.9 . 228(23) 0.0 210.7 . 222(23) 0.0 210.5 . 215(22) 0.0 210.3 . 234(23) 0.0 210.1 . 245(24) 0.0 209.9 . 228(23) 0.0 209.7 . 207(22) 0.0 209.6 . 220(23) 0.0 209.4 . 251(24) 0.0 209.2 . 240(24) 0.0 209.0 . 223(23) 0.0 208.8 . 226(23) 0.0 208.6 . 213(22) 0.0 208.5 . 243(24) 0.0 208.3 . 252(24) 0.0 208.1 . 200(22) 0.0 207.9 . 225(23) 0.0 207.7 . 226(23) 0.0 207.5 . 231(23) 0.0 207.3 . 236(23) 0.0 207.2 . 212(22) 0.0 207.0 . 274(25) 0.0 206.8 . 244(24) 0.0 206.6 . 201(22) 0.0 206.4 . 191(21) 0.0 206.3 . 229(23) 0.0 206.1 . 219(22) 0.0 205.9 . 213(22) 0.0 205.7 . 243(24) 0.0 205.5 . 193(21) 0.0 205.3 . 202(22) 0.0 205.2 . 217(22) 0.0 205.0 . 220(22) 0.0 204.8 . 231(23) 0.0 204.6 . 236(23) 0.0 204.4 . 218(22) 0.0 204.3 . 250(24) 0.0 204.1 . 207(22) 0.0 203.9 . 237(23) 0.0 203.7 . 239(23) 0.0 203.5 . 253(24) 0.0 203.4 . 223(23) 0.0 203.2 . 193(21) 0.0 203.0 . 268(25) 0.0 202.8 . 244(24) 0.0 202.6 . 239(23) 0.0 202.5 . 231(23) 0.0 202.3 . 201(21) 0.0 202.1 . 240(23) 0.0 201.9 . 240(23) 0.0 201.7 . 202(21) 0.0 201.6 . 238(23) 0.0 201.4 . 199(21) 0.0 201.2 . 237(23) 0.0 201.0 . 234(23) 0.0 200.8 . 205(22) 0.0 200.7 . 197(21) 0.0 200.5 . 174(20) 0.0 200.3 . 223(22) 0.0 200.1 . 173(20) 0.0 200.0 . 203(21) 0.0 199.8 . 222(22) 0.0 199.6 . 251(24) 0.0 199.4 . 236(23) 0.0 199.3 . 203(21) 0.0 199.1 . 192(21) 0.0 198.9 . 177(20) 0.0 198.7 . 165(19) 0.0 198.6 . 198(21) 0.0 198.4 . 206(21) 0.0 198.2 . 213(22) 0.0 198.0 . 227(23) 0.0 197.8 . 221(22) 0.0 197.7 . 237(23) 0.0 197.5 . 228(23) 0.0 197.3 . 235(23) 0.0 197.1 . 241(23) 0.0 197.0 . 180(20) 0.0 196.8 . 185(20) 0.0 196.6 . 221(22) 0.0 196.5 . 179(20) 0.0 196.3 . 221(22) 0.0 196.1 . 212(22) 0.0 195.9 . 197(21) 0.0 195.8 . 196(21) 0.0 195.6 . 192(21) 0.0 195.4 . 187(20) 0.0 195.2 . 207(21) 0.0 195.1 . 213(22) 0.0 194.9 . 229(22) 0.0 194.7 . 204(21) 0.0 194.5 . 186(20) 0.0 194.4 . 267(24) 0.0 194.2 . 205(21) 0.0 194.0 . 218(22) 0.0 193.9 . 205(21) 0.0 193.7 . 207(21) 0.0 193.5 . 214(22) 0.0 193.3 . 216(22) 0.0 193.2 . 218(22) 0.0 193.0 . 172(19) 0.0 192.8 . 173(19) 0.0 192.7 . 211(21) 0.0 192.5 . 215(22) 0.0 192.3 . 253(24) 0.0 192.1 . 201(21) 0.0 192.0 . 208(21) 0.0 191.8 . 181(20) 0.0 191.6 . 215(22) 0.0 191.5 . 176(20) 0.0 191.3 . 211(21) 0.0 191.1 . 208(21) 0.0 191.0 . 177(20) 0.0 190.8 . 234(23) 0.0 190.6 . 197(21) 0.0 190.5 . 164(19) 0.0 190.3 . 218(22) 0.0 190.1 . 206(21) 0.0 189.9 . 179(20) 0.0 189.8 . 196(21) 0.0 189.6 . 209(21) 0.0 189.4 . 251(23) 0.0 189.3 . 232(22) 0.0 189.1 . 211(21) 0.0 188.9 . 184(20) 0.0 188.8 . 212(21) 0.0 188.6 . 176(19) 0.0 188.4 . 189(20) 0.0 188.3 . 252(23) 0.0 188.1 . 177(20) 0.0 187.9 . 200(21) 0.0 187.8 . 194(20) 0.0 187.6 . 197(20) 0.0 187.4 . 203(21) 0.0 187.3 . 176(19) 0.0 187.1 . 247(23) 0.0 186.9 . 183(20) 0.0 186.8 . 236(22) 0.0 186.6 . 226(22) 0.0 186.4 . 226(22) 0.0 186.3 . 215(21) 0.0 186.1 . 202(21) 0.0 185.9 . 217(22) 0.0 185.8 . 212(21) 0.0 185.6 . 208(21) 0.0 185.5 . 198(21) 0.0 185.3 . 239(23) 0.0 185.1 . 214(21) 0.0 185.0 . 192(20) 0.0 184.8 . 172(19) 0.0 184.6 . 200(21) 0.0 184.5 . 185(20) 0.0 184.3 . 222(22) 0.0 184.1 . 196(20) 0.0 184.0 . 212(21) 0.0 183.8 . 181(20) 0.0 183.7 . 133(17) 0.0 183.5 . 204(21) 0.0 183.3 . 215(21) 0.0 183.2 . 198(20) 0.0 183.0 . 202(21) 0.0 182.8 . 220(22) 0.0 182.7 . 193(20) 0.0 182.5 . 172(19) 0.0 182.4 . 180(19) 0.0 182.2 . 181(19) 0.0 182.0 . 207(21) 0.0 181.9 . 241(23) 0.0 181.7 . 153(18) 0.0 181.5 . 202(21) 0.0 181.4 . 199(20) 0.0 181.2 . 148(18) 0.0 181.1 . 188(20) 0.0 180.9 . 211(21) 0.0 180.7 . 206(21) 0.0 180.6 . 219(21) 0.0 180.4 . 189(20) 0.0 180.3 . 194(20) 0.0 180.1 . 196(20) 0.0 179.9 . 189(20) 0.0 179.8 . 189(20) 0.0 179.6 . 197(20) 0.0 179.5 . 196(20) 0.0 179.3 . 208(21) 0.0 179.1 . 212(21) 0.0 179.0 . 216(21) 0.0 178.8 . 231(22) 0.0 178.7 . 193(20) 0.0 178.5 . 199(20) 0.0 178.4 . 168(19) 0.0 178.2 . 172(19) 0.0 178.0 . 173(19) 0.0 177.9 . 198(20) 0.0 177.7 . 199(20) 0.0 177.6 . 175(19) 0.0 177.4 . 206(21) 0.0 177.2 . 188(20) 0.0 177.1 . 195(20) 0.0 176.9 . 214(21) 0.0 176.8 . 241(22) 0.0 176.6 . 162(18) 0.0 176.5 . 211(21) 0.0 176.3 . 156(18) 0.0 176.2 . 201(20) 0.0 176.0 . 168(19) 0.0 175.8 . 206(21) 0.0 175.7 . 188(20) 0.0 175.5 . 164(18) 0.0 175.4 . 192(20) 0.0 175.2 . 169(19) 0.0 175.1 . 206(21) 0.0 174.9 . 169(19) 0.0 174.8 . 201(20) 0.0 174.6 . 209(21) 0.0 174.4 . 198(20) 0.0 174.3 . 176(19) 0.0 174.1 . 190(20) 0.0 174.0 . 179(19) 0.0 173.8 . 189(20) 0.0 173.7 . 185(19) 0.0 173.5 . 179(19) 0.0 173.4 . 202(20) 0.0 173.2 . 192(20) 0.0 173.1 . 171(19) 0.0 172.9 . 207(21) 0.0 172.8 . 176(19) 0.002770 172.6 172.6 235(22) 0.002066 172.4 172.4 162(18) 0.003086 172.3 172.3 162(18) 0.003086 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120.0 120.0 132(15) 0.00444 119.9 119.9 137(15) 0.00444 119.8 119.8 122(15) 0.00444 119.7 119.7 115(14) 0.00510 119.6 119.6 111(14) 0.00510 119.5 119.5 142(16) 0.00391 119.4 119.4 151(16) 0.00391 119.3 119.3 137(15) 0.00444 119.2 119.2 119(14) 0.00510 119.1 119.1 107(14) 0.00510 119.0 119.0 121(14) 0.00510 118.9 118.9 105(13) 0.00592 118.8 118.8 140(15) 0.00444 118.7 118.7 130(15) 0.00444 118.6 118.6 142(16) 0.00391 118.5 118.5 124(14) 0.00510 118.5 118.5 101(13) 0.00592 118.4 118.4 140(15) 0.00444 118.3 118.3 112(14) 0.00510 118.2 118.2 132(15) 0.00444 118.1 118.1 113(14) 0.00510 118.0 118.0 137(15) 0.00444 117.9 117.9 122(14) 0.00510 117.8 117.8 120(14) 0.00510 117.7 117.7 118(14) 0.00510 117.6 117.6 113(14) 0.00510 117.5 117.5 123(14) 0.00510 117.4 117.4 145(16) 0.00391 117.3 117.3 127(15) 0.00444 117.2 117.2 121(14) 0.00510 117.1 117.1 128(15) 0.00444 117.0 117.0 116(14) 0.00510 116.9 116.9 107(13) 0.00592 116.8 116.8 82(12) 0.00694 116.7 116.7 110(14) 0.00510 116.6 116.6 147(16) 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0.002500 100.9 265.1 229(19) 0.002770 100.9 238.8 209(18) 0.003086 100.8 218.9 222(19) 0.002770 100.7 203.2 160(16) 0.00391 100.6 190.5 158(16) 0.00391 100.6 180.1 149(15) 0.00444 100.5 171.3 133(15) 0.00444 100.4 163.9 158(16) 0.00391 100.3 157.6 149(15) 0.00444 100.2 152.1 127(14) 0.00510 100.2 147.4 130(15) 0.00444 100.1 143.2 115(14) 0.00510 100.0 139.5 117(14) 0.00510 99.9 136.3 128(14) 0.00510 99.9 133.4 88(12) 0.00694 99.8 130.9 129(14) 0.00510 99.7 128.6 129(14) 0.00510 99.6 126.5 132(15) 0.00444 99.5 124.6 96(12) 0.00694 99.5 122.9 129(14) 0.00510 99.4 121.4 105(13) 0.00592 99.3 120.0 99(13) 0.00592 99.2 118.7 91(12) 0.00694 99.2 117.5 121(14) 0.00510 99.1 116.4 93(12) 0.00694 99.0 115.4 97(12) 0.00694 98.9 114.4 126(14) 0.00510 98.9 113.5 118(14) 0.00510 98.8 112.7 122(14) 0.00510 98.7 112.0 98(13) 0.00592 98.6 111.3 113(13) 0.00592 98.6 110.6 123(14) 0.00510 98.5 110.0 110(13) 0.00592 98.4 109.4 87(12) 0.00694 98.3 108.8 112(13) 0.00592 98.3 108.3 102(13) 0.00592 98.2 107.8 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80(10) 0.01000 53.1 93.1 115(12) 0.00694 53.1 98.0 126(12) 0.00694 53.1 103.5 121(12) 0.00694 53.1 109.9 119(12) 0.00694 53.1 117.1 124(12) 0.00694 53.1 125.2 148(13) 0.00592 53.1 134.2 134(12) 0.00694 53.1 144.1 136(12) 0.00694 53.1 154.8 200(15) 0.00444 53.0 166.1 154(13) 0.00592 53.0 177.8 183(15) 0.00444 53.0 189.6 205(15) 0.00444 53.0 200.9 204(15) 0.00444 53.0 211.2 213(16) 0.00391 53.0 219.7 222(16) 0.00391 53.0 225.7 285(18) 0.003086 53.0 228.7 241(17) 0.003460 53.0 228.2 266(17) 0.003460 53.0 224.4 245(17) 0.003460 53.0 217.7 222(16) 0.00391 53.0 208.6 209(15) 0.00444 53.0 198.0 227(16) 0.00391 53.0 186.5 190(15) 0.00444 53.0 174.6 169(14) 0.00510 53.0 162.9 149(13) 0.00592 53.0 151.7 151(13) 0.00592 52.9 141.2 127(12) 0.00694 52.9 131.5 116(12) 0.00694 52.9 122.7 104(11) 0.00826 52.9 114.8 112(11) 0.00826 52.9 107.7 96(11) 0.00826 52.9 101.4 104(11) 0.00826 52.9 95.9 84(10) 0.01000 52.9 91.2 99(11) 0.00826 52.9 87.2 81(10) 0.01000 52.9 83.7 87(10) 0.01000 52.9 80.7 69(9) 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65.4 76(9) 0.01235 43.3 67.7 74(9) 0.01235 43.3 70.3 78(10) 0.01000 43.3 73.3 74(9) 0.01235 43.3 76.6 64(9) 0.01235 43.3 80.2 69(9) 0.01235 43.2 84.1 69(9) 0.01235 43.2 88.4 95(11) 0.00826 43.2 92.9 111(11) 0.00826 43.2 97.6 87(10) 0.01000 43.2 102.4 86(10) 0.01000 43.2 107.2 124(12) 0.00694 43.2 111.8 103(11) 0.00826 43.2 116.1 127(12) 0.00694 43.2 119.7 127(12) 0.00694 43.2 122.6 132(12) 0.00694 43.2 124.4 116(12) 0.00694 43.2 125.0 120(12) 0.00694 43.2 124.5 133(12) 0.00694 43.2 122.7 106(11) 0.00826 43.2 120.0 125(12) 0.00694 43.2 116.4 86(10) 0.01000 43.2 112.1 81(10) 0.01000 43.2 107.5 89(10) 0.01000 43.2 102.7 83(10) 0.01000 43.2 97.9 84(10) 0.01000 43.2 93.1 88(10) 0.01000 43.2 88.5 60(8) 0.01563 43.2 84.2 68(9) 0.01235 43.2 80.2 69(9) 0.01235 43.2 76.5 63(9) 0.01235 43.2 73.1 72(9) 0.01235 43.2 70.1 55(8) 0.01563 43.2 67.4 52(8) 0.01563 43.2 65.0 55(8) 0.01563 43.2 62.9 66(9) 0.01235 43.2 61.1 61(8) 0.01563 43.2 59.5 47(7) 0.02041 43.2 58.2 51(8) 0.01563 43.2 57.0 62(9) 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0.02041 42.6 43.7 50(8) 0.01563 42.6 43.7 64(9) 0.01235 42.6 43.8 49(8) 0.01563 42.6 43.8 39(7) 0.02041 42.6 43.8 61(8) 0.01563 42.6 43.8 57(8) 0.01563 42.6 43.8 44(7) 0.02041 42.6 43.8 36(7) 0.02041 42.6 43.8 54(8) 0.01563 42.6 43.8 29(6) 0.02778 42.6 43.8 35(6) 0.02778 42.6 43.8 48(8) 0.01563 42.6 43.8 47(7) 0.02041 42.6 43.8 32(6) 0.02778 42.6 43.8 37(7) 0.02041 42.6 43.8 40(7) 0.02041 42.6 43.8 28(6) 0.02778 42.6 43.8 41(7) 0.02041 42.6 43.8 49(8) 0.01563 42.5 43.9 40(7) 0.02041 42.5 43.9 48(8) 0.01563 42.5 43.9 53(8) 0.01563 42.5 43.9 47(7) 0.02041 42.5 43.9 39(7) 0.02041 42.5 43.9 47(7) 0.02041 42.5 43.9 48(8) 0.01563 42.5 43.9 39(7) 0.02041 42.5 43.9 42(7) 0.02041 42.5 44.0 40(7) 0.02041 42.5 44.0 40(7) 0.02041 42.5 44.0 43(7) 0.02041 42.5 44.0 48(8) 0.01563 42.5 44.0 53(8) 0.01563 42.5 44.0 54(8) 0.01563 42.5 44.0 48(8) 0.01563 42.5 44.1 44(7) 0.02041 42.5 44.1 42(7) 0.02041 42.5 44.1 42(7) 0.02041 42.5 44.1 37(7) 0.02041 42.5 44.1 47(7) 0.02041 42.5 44.2 40(7) 0.02041 42.5 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0.01563 42.4 59.6 68(9) 0.01235 42.3 61.0 61(9) 0.01235 42.3 62.6 54(8) 0.01563 42.3 64.4 56(8) 0.01563 42.3 66.5 64(9) 0.01235 42.3 68.7 67(9) 0.01235 42.3 71.3 66(9) 0.01235 42.3 74.0 53(8) 0.01563 42.3 77.0 70(9) 0.01235 42.3 80.3 78(10) 0.01000 42.3 83.8 61(8) 0.01563 42.3 87.5 84(10) 0.01000 42.3 91.4 74(9) 0.01235 42.3 95.4 91(10) 0.01000 42.3 99.5 90(10) 0.01000 42.3 103.6 102(11) 0.00826 42.3 107.6 119(12) 0.00694 42.3 111.3 112(11) 0.00826 42.3 114.8 131(12) 0.00694 42.3 117.8 123(12) 0.00694 42.3 120.3 100(11) 0.00826 42.3 122.3 109(11) 0.00826 42.3 123.8 119(12) 0.00694 42.3 124.9 120(12) 0.00694 42.3 125.6 119(12) 0.00694 42.3 126.2 109(11) 0.00826 42.3 126.6 108(11) 0.00826 42.3 127.0 96(11) 0.00826 42.3 127.3 122(12) 0.00694 42.3 127.5 87(10) 0.01000 42.3 127.7 103(11) 0.00826 42.3 127.9 105(11) 0.00826 42.3 127.8 89(10) 0.01000 42.3 127.5 100(11) 0.00826 42.3 126.9 111(11) 0.00826 42.3 126.1 100(11) 0.00826 42.3 124.9 121(12) 0.00694 42.3 123.6 105(11) 0.00826 42.3 122.2 88(10) 0.01000 42.3 120.8 93(10) 0.01000 42.3 119.5 98(11) 0.00826 42.3 118.6 96(11) 0.00826 42.3 118.0 94(11) 0.00826 42.3 117.9 95(11) 0.00826 42.3 118.4 96(11) 0.00826 42.3 119.5 87(10) 0.01000 42.3 121.3 126(12) 0.00694 42.3 123.7 108(11) 0.00826 42.3 126.8 107(11) 0.00826 42.3 130.6 147(13) 0.00592 42.3 134.9 150(13) 0.00592 42.3 139.7 167(14) 0.00510 42.3 144.7 149(13) 0.00592 42.3 150.0 166(14) 0.00510 42.3 155.1 233(17) 0.003460 42.3 159.9 193(15) 0.00444 42.3 164.0 198(15) 0.00444 42.3 167.1 205(16) 0.00391 42.3 169.1 226(16) 0.00391 42.3 169.8 178(15) 0.00444 42.3 169.0 177(14) 0.00510 42.3 167.0 192(15) 0.00444 42.3 163.9 158(14) 0.00510 42.3 160.0 171(14) 0.00510 42.3 155.7 127(12) 0.00694 42.3 151.4 147(13) 0.00592 42.3 147.2 156(14) 0.00510 42.3 143.4 138(13) 0.00592 42.3 140.4 125(12) 0.00694 42.3 138.2 136(13) 0.00592 42.3 137.1 124(12) 0.00694 42.3 137.2 142(13) 0.00592 42.3 138.5 155(14) 0.00510 42.3 141.1 145(13) 0.00592 42.3 145.2 147(13) 0.00592 42.3 150.6 171(14) 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40.4 175.6 173(13) 0.00592 40.4 169.0 180(14) 0.00510 40.4 161.9 187(14) 0.00510 40.4 154.4 136(12) 0.00694 40.4 146.8 157(13) 0.00592 40.4 139.3 157(13) 0.00592 40.4 131.9 154(13) 0.00592 40.4 124.8 92(10) 0.01000 40.4 118.0 132(12) 0.00694 40.4 111.5 108(11) 0.00826 40.4 105.5 122(11) 0.00826 40.4 99.9 104(10) 0.01000 40.4 94.8 103(10) 0.01000 40.4 90.1 87(9) 0.01235 40.4 85.8 97(10) 0.01000 40.4 81.9 88(9) 0.01235 40.4 78.4 96(10) 0.01000 40.4 75.3 84(9) 0.01235 40.4 72.5 83(9) 0.01235 40.4 70.1 75(9) 0.01235 40.4 67.9 71(9) 0.01235 40.4 66.0 66(8) 0.01563 40.4 64.3 70(8) 0.01563 40.4 62.8 52(7) 0.02041 40.4 61.4 83(9) 0.01235 40.4 60.2 57(8) 0.01563 40.4 59.2 77(9) 0.01235 40.4 58.3 60(8) 0.01563 40.4 57.4 55(8) 0.01563 40.4 56.7 59(8) 0.01563 40.4 56.0 73(9) 0.01235 40.3 55.4 72(9) 0.01235 40.3 54.8 57(8) 0.01563 40.3 54.3 63(8) 0.01563 40.3 53.9 65(8) 0.01563 40.3 53.5 55(7) 0.02041 40.3 52.6 63(8) 0.01563 40.3 52.2 60(8) 0.01563 40.3 51.9 56(8) 0.01563 40.3 51.6 52(7) 0.02041 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86.2 74(9) 0.01235 41.0 87.6 76(9) 0.01235 41.0 89.2 85(10) 0.01000 41.1 91.0 83(9) 0.01235 41.1 93.0 80(9) 0.01235 41.1 95.2 90(10) 0.01000 41.1 97.6 74(9) 0.01235 41.1 100.3 90(10) 0.01000 41.1 103.3 102(11) 0.00826 41.1 106.6 109(11) 0.00826 41.1 110.2 111(11) 0.00826 41.1 114.2 115(11) 0.00826 41.1 118.4 109(11) 0.00826 41.1 123.1 112(11) 0.00826 41.1 128.1 102(11) 0.00826 41.1 133.4 140(12) 0.00694 41.2 139.2 127(12) 0.00694 41.2 145.2 131(12) 0.00694 41.2 151.6 134(12) 0.00694 41.2 158.2 149(13) 0.00592 41.2 165.0 175(14) 0.00510 41.2 171.9 182(14) 0.00510 41.2 178.9 184(14) 0.00510 41.2 185.9 194(14) 0.00510 41.2 192.8 234(16) 0.00391 41.2 199.4 229(16) 0.00391 41.2 205.7 253(17) 0.003460 41.2 211.6 235(16) 0.00391 41.2 216.9 274(17) 0.003460 41.3 221.5 267(17) 0.003460 41.3 225.3 257(17) 0.003460 41.3 228.2 267(17) 0.003460 41.3 230.1 291(18) 0.003086 41.3 231.0 265(17) 0.003460 41.3 230.9 272(17) 0.003460 41.3 229.7 259(17) 0.003460 41.3 227.6 261(17) 0.003460 41.3 224.5 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131(12) 0.00694 41.6 128.4 137(12) 0.00694 41.6 131.4 119(11) 0.00826 41.7 134.4 128(12) 0.00694 41.7 137.5 121(11) 0.00826 41.7 140.6 150(13) 0.00592 41.7 143.7 148(13) 0.00592 41.7 146.6 154(13) 0.00592 41.7 149.3 131(12) 0.00694 41.7 151.8 175(14) 0.00510 41.7 154.0 198(15) 0.00444 41.7 155.8 177(14) 0.00510 41.7 157.2 181(14) 0.00510 41.7 158.2 174(14) 0.00510 41.7 158.7 148(13) 0.00592 41.8 158.8 167(13) 0.00592 41.8 158.5 142(12) 0.00694 41.8 157.8 151(13) 0.00592 41.8 156.8 169(14) 0.00510 41.8 155.6 157(13) 0.00592 41.8 154.2 156(13) 0.00592 41.8 152.7 150(13) 0.00592 41.8 151.2 162(13) 0.00592 41.8 149.6 146(13) 0.00592 41.8 148.1 124(12) 0.00694 41.8 146.7 139(12) 0.00694 41.8 145.3 137(12) 0.00694 41.9 144.1 132(12) 0.00694 41.9 143.0 158(13) 0.00592 41.9 142.1 125(12) 0.00694 41.9 141.3 152(13) 0.00592 41.9 140.6 145(13) 0.00592 41.9 140.0 120(11) 0.00826 41.9 139.6 128(12) 0.00694 41.9 139.3 121(11) 0.00826 41.9 139.2 145(13) 0.00592 41.9 139.3 150(13) 0.00592 41.9 139.6 136(12) 0.00694 41.9 140.2 131(12) 0.00694 42.0 141.0 141(12) 0.00694 42.0 142.1 161(13) 0.00592 42.0 143.5 145(13) 0.00592 42.0 145.2 163(13) 0.00592 42.0 147.1 164(13) 0.00592 42.0 149.4 168(14) 0.00510 42.0 151.8 168(14) 0.00510 42.0 154.4 171(14) 0.00510 42.0 157.2 153(13) 0.00592 42.0 159.9 173(14) 0.00510 42.0 162.6 190(14) 0.00510 42.1 165.1 177(14) 0.00510 42.1 167.3 187(14) 0.00510 42.1 169.1 167(14) 0.00510 42.1 170.3 194(14) 0.00510 42.1 170.9 189(14) 0.00510 42.1 170.8 180(14) 0.00510 42.1 170.0 173(14) 0.00510 42.1 168.5 174(14) 0.00510 42.1 166.3 148(13) 0.00592 42.1 163.6 162(13) 0.00592 42.1 160.3 158(13) 0.00592 42.1 156.7 154(13) 0.00592 42.2 152.9 143(12) 0.00694 42.2 148.9 153(13) 0.00592 42.2 144.8 133(12) 0.00694 42.2 140.8 134(12) 0.00694 42.2 136.9 148(13) 0.00592 42.2 133.2 135(12) 0.00694 42.2 129.7 130(12) 0.00694 42.2 126.4 133(12) 0.00694 42.2 123.3 131(12) 0.00694 42.2 120.5 137(12) 0.00694 42.2 118.0 125(12) 0.00694 42.3 115.7 123(12) 0.00694 42.3 113.6 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0.00694 43.0 126.1 121(12) 0.00694 43.0 122.5 125(12) 0.00694 43.0 118.8 106(11) 0.00826 43.0 115.2 105(11) 0.00826 43.0 111.6 105(11) 0.00826 43.0 108.1 105(11) 0.00826 43.0 104.7 93(10) 0.01000 43.0 101.4 93(10) 0.01000 43.0 98.2 97(10) 0.01000 43.0 95.2 98(10) 0.01000 43.0 92.3 116(11) 0.00826 43.1 89.6 88(10) 0.01000 43.1 87.1 84(10) 0.01000 43.1 84.8 83(10) 0.01000 43.1 82.6 93(10) 0.01000 43.1 80.5 90(10) 0.01000 43.1 78.7 89(10) 0.01000 43.1 77.0 78(9) 0.01235 43.1 75.4 98(10) 0.01000 43.1 74.0 85(10) 0.01000 43.1 72.8 58(8) 0.01563 43.2 71.7 83(10) 0.01000 43.2 70.7 81(9) 0.01235 43.2 69.9 76(9) 0.01235 43.2 69.2 78(9) 0.01235 43.2 68.6 66(8) 0.01563 43.2 68.2 74(9) 0.01235 43.2 67.9 67(9) 0.01235 43.2 67.8 66(8) 0.01563 43.2 67.7 83(10) 0.01000 43.2 67.8 72(9) 0.01235 43.2 68.1 97(10) 0.01000 43.3 68.4 78(9) 0.01235 43.3 68.9 70(9) 0.01235 43.3 69.6 89(10) 0.01000 43.3 70.3 93(10) 0.01000 43.3 71.2 69(9) 0.01235 43.3 72.2 91(10) 0.01000 43.3 73.3 89(10) 0.01000 43.3 74.4 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48.7 158.8 155(14) 0.00510 48.7 160.9 151(14) 0.00510 48.7 162.7 180(15) 0.00444 48.6 164.1 166(14) 0.00510 48.6 165.3 192(15) 0.00444 48.6 166.2 165(14) 0.00510 48.6 166.8 150(14) 0.00510 48.6 167.2 166(14) 0.00510 48.5 167.4 175(15) 0.00444 48.5 167.4 163(14) 0.00510 48.5 167.2 159(14) 0.00510 48.5 166.9 182(15) 0.00444 48.4 166.5 165(14) 0.00510 48.4 165.9 202(16) 0.00391 48.4 165.2 192(15) 0.00444 48.4 164.4 181(15) 0.00444 48.3 163.4 200(16) 0.00391 48.3 162.3 166(14) 0.00510 48.3 161.1 168(14) 0.00510 48.3 159.7 158(14) 0.00510 48.2 158.1 200(16) 0.00391 48.2 156.5 183(15) 0.00444 48.2 154.7 144(13) 0.00592 48.2 152.8 169(14) 0.00510 48.1 150.9 164(14) 0.00510 48.1 148.9 142(13) 0.00592 48.1 146.9 162(14) 0.00510 48.1 144.8 164(14) 0.00510 48.0 142.8 149(14) 0.00510 48.0 140.8 136(13) 0.00592 48.0 138.8 154(14) 0.00510 48.0 136.9 128(13) 0.00592 47.9 134.9 154(14) 0.00510 47.9 133.1 137(13) 0.00592 47.9 131.3 125(12) 0.00694 47.9 129.5 151(14) 0.00510 47.8 127.7 132(13) 0.00592 47.8 125.9 146(13) 0.00592 47.8 124.1 136(13) 0.00592 47.8 122.4 127(13) 0.00592 47.7 120.6 121(12) 0.00694 47.7 118.7 122(12) 0.00694 47.7 116.8 123(12) 0.00694 47.6 114.9 121(12) 0.00694 47.6 112.9 121(12) 0.00694 47.6 110.9 121(12) 0.00694 47.6 108.9 113(12) 0.00694 47.5 106.9 113(12) 0.00694 47.5 104.8 116(12) 0.00694 47.5 102.7 119(12) 0.00694 47.5 100.7 106(11) 0.00826 47.4 98.7 112(12) 0.00694 47.4 96.6 104(11) 0.00826 47.4 94.7 89(10) 0.01000 47.4 92.7 113(12) 0.00694 47.3 90.8 95(11) 0.00826 47.3 88.9 90(11) 0.00826 47.3 87.0 101(11) 0.00826 47.2 85.2 86(10) 0.01000 47.2 83.5 103(11) 0.00826 47.2 81.8 81(10) 0.01000 47.2 80.1 80(10) 0.01000 47.1 78.6 89(10) 0.01000 47.1 77.1 91(11) 0.00826 47.1 75.6 75(10) 0.01000 47.1 74.3 79(10) 0.01000 47.0 73.0 81(10) 0.01000 47.0 71.8 60(9) 0.01235 47.0 70.6 83(10) 0.01000 46.9 69.5 87(10) 0.01000 46.9 68.5 71(9) 0.01235 46.9 67.6 64(9) 0.01235 46.9 66.7 63(9) 0.01235 46.8 65.9 67(9) 0.01235 46.8 65.1 63(9) 0.01235 46.8 64.4 53(8) 0.01563 46.7 63.8 60(9) 0.01235 46.7 63.2 78(10) 0.01000 46.7 62.6 63(9) 0.01235 46.7 62.1 51(8) 0.01563 46.6 61.6 67(9) 0.01235 46.6 61.2 70(9) 0.01235 46.6 60.8 58(9) 0.01235 46.5 60.4 55(8) 0.01563 46.5 60.1 68(9) 0.01235 46.5 59.8 63(9) 0.01235 46.5 59.5 53(8) 0.01563 46.4 59.3 58(9) 0.01235 46.4 59.1 64(9) 0.01235 46.4 58.9 53(8) 0.01563 46.3 58.7 57(8) 0.01563 46.3 58.6 44(7) 0.02041 46.3 58.4 62(9) 0.01235 46.2 58.3 39(7) 0.02041 46.2 58.2 56(8) 0.01563 46.2 58.1 57(8) 0.01563 46.2 58.0 50(8) 0.01563 46.1 57.9 53(8) 0.01563 46.1 57.9 63(9) 0.01235 46.1 57.8 52(8) 0.01563 46.0 57.7 45(7) 0.02041 46.0 57.7 46(8) 0.01563 46.0 57.6 54(8) 0.01563 45.9 57.5 60(9) 0.01235 45.9 57.4 65(9) 0.01235 45.9 57.3 52(8) 0.01563 45.9 57.1 53(8) 0.01563 45.8 57.0 48(8) 0.01563 45.8 56.8 39(7) 0.02041 45.8 56.6 55(8) 0.01563 45.7 56.4 59(9) 0.01235 45.7 56.2 62(9) 0.01235 45.7 56.0 51(8) 0.01563 45.6 55.7 43(7) 0.02041 45.6 55.5 47(8) 0.01563 45.6 55.2 66(9) 0.01235 45.5 55.0 43(7) 0.02041 45.5 54.7 39(7) 0.02041 45.5 54.4 48(8) 0.01563 45.4 54.1 53(8) 0.01563 45.4 53.9 53(8) 0.01563 45.4 53.6 43(7) 0.02041 45.4 53.4 50(8) 0.01563 45.3 53.1 33(6) 0.02778 45.3 52.9 44(7) 0.02041 45.3 52.6 46(8) 0.01563 45.2 52.4 50(8) 0.01563 45.2 52.2 51(8) 0.01563 45.2 51.9 52(8) 0.01563 45.1 51.7 56(8) 0.01563 45.1 51.5 42(7) 0.02041 45.1 51.3 56(8) 0.01563 45.0 51.1 43(7) 0.02041 45.0 50.9 66(9) 0.01235 45.0 50.7 41(7) 0.02041 44.9 50.6 41(7) 0.02041 44.9 50.4 41(7) 0.02041 44.9 50.2 47(8) 0.01563 44.8 50.1 48(8) 0.01563 44.8 49.9 46(8) 0.01563 44.8 49.8 50(8) 0.01563 44.7 49.6 45(7) 0.02041 44.7 49.5 52(8) 0.01563 44.7 49.4 70(9) 0.01235 44.6 49.2 41(7) 0.02041 44.6 49.1 41(7) 0.02041 44.6 49.0 47(8) 0.01563 44.5 48.9 51(8) 0.01563 44.5 48.8 52(8) 0.01563 44.5 48.7 48(8) . . . 38(7) . . . 42(7) . . . 45(7) . . . 54(8) . . . 40(7) . . . 38(7) . . . 32(6) . . . 40(7) . . . 44(7) . . . 42(7) . . . 43(7) . . . 46(8) . . . 37(7) . . . 43(7) . . . 47(8) . . . 33(6) . . . 46(8) . . . 36(7) . . . 51(8) . . . 39(7) . . . 56(8) . . . 53(8) . . . 41(7) . . . 44(7) . . . 40(7) . . . 62(9) . . . 48(8) . . . 44(7) . . . 53(8) . . . 40(7) . . . 42(7) . . . 46(8) . . . 56(8) . . . 44(7) . . . 32(6) . . . 36(7) . . . 40(7) . . . 53(8) . . . 36(7) . . . 46(8) . . . 45(7) . . . 69(9) . . . 53(8) . . . 52(8) . . . 33(6) . . . 47(8) . . . 50(8) . . . 42(7) . . . 63(9) . . . 44(7) . . . 48(8) . . . 49(8) . . . 41(7) . . . 43(7) . . . 47(8) . . . 44(7) . . . 55(8) . . . 55(8) . . . 58(9) . . . 48(8) . . . 54(8) . . . 47(8) . . . 50(8) . . . 47(8) . . . 42(7) . . . 46(8) . . . 44(7) . . . 62(9) . . . 56(8) . . . 47(8) . . . 53(8) . . . 47(8) . . . 47(8) . . . 37(7) . . . 49(8) . . . 30(6) . . . 55(8) . . . 43(7) . . . 54(8) . . . 40(7) . . . 38(7) . . . 57(8) . . . 42(7) . . . 36(7) . . . 48(8) . . . 65(9) . . . 36(7) . . . 49(8) . . . 62(9) . . . 51(8) . . . 59(9) . . . 53(8) . . . 34(6) . . . 52(8) . . . 53(8) . . . 45(7) . . . 47(8) . . . 47(8) . . . 47(8) . . . 49(8) . . . 65(9) . . . 45(7) . . . 35(7) . . . 50(8) . . . 53(8) . . . 50(8) . . . 54(8) . . . 45(8) . . . 38(7) . . . 57(8) . . . 47(8) . . . 51(8) . . . 47(8) . . . 59(9) . . . 52(8) . . . 58(9) . . . 58(9) . . . 42(7) . . . 65(9) . . . 55(8) . . . 48(8) . . . 69(9) . . . 50(8) . . . 55(8) . . . 58(9) . . . 52(8) . . . 60(9) . . . 51(8) . . . 52(8) . . . 52(8) . . . 53(8) . . . 56(8) . . . 65(9) . . . 54(8) . . . 68(9) . . . 47(8) . . . 52(8) . . . 70(9) . . . 65(9) . . . 66(9) . . . 62(9) . . . 45(7) . . . 55(8) . . . 59(9) . . . 58(9) . . . 49(8) . . . 51(8) . . . 50(8) . . . 57(8) . . . 52(8) . . . 54(8) . . . 62(9) . . . 56(8) . . . 41(7) . . . 57(8) . . . 46(8) . . . 50(8) . . . 51(8) . . . 40(7) . . . 47(8) . . . 46(8) . . . 51(8) . . . 37(7) . . . 58(9) . . . 43(7) . . . 48(8) . . . 43(7) . . . 64(9) . . . 39(7) . . . 32(6) . . . 61(9) . . . 57(9) . . . 49(8) . . . 41(7) . . . 46(8) . . . 44(7) . . . 37(7) . . . 63(9) . . . 46(8) . . . 55(8) . . . 55(8) . . . 56(8) . . . 49(8) . . . 55(8) . . . 53(8) . . . 50(8) . . . 63(9) . . . 44(7) . . . 60(9) . . . 42(7) . . . 38(7) . . . 62(9) . . . 46(8) . . . 42(7) . . . 62(9) . . . 57(9) . . . 54(8) . . . 55(8) . . . 67(9) . . . 66(9) . . . 68(9) . . . 54(8) . . . 73(10) . . . 77(10) . . . 72(10) . . . 81(10) . . . 71(9) . . . 73(10) . . . 68(9) . . . 69(9) . . . 73(10) . . . 73(10) . . . 75(10) . . . 77(10) . . . 76(10) . . . 64(9) . . . 68(9) . . . 60(9) . . . 74(10) . . . 51(8) . . . 45(8) . . . 62(9) . . . 65(9) . . . 50(8) . . . 65(9) . . . 47(8) . . . 62(9) . . . 50(8) . . . 66(9) . . . 55(8) . . . 64(9) . . . 71(9) . . . 66(9) . . . 58(9) . . . 54(8) . . . 60(9) . . . 65(9) . . . 69(9) . . . 67(9) . . . 70(9) . . . 58(9) . . . 52(8) . . . 62(9) . . . 55(8) . . . 55(8) . . . 77(10) . . . 60(9) . . . 77(10) . . . 86(10) . . . 69(9) . . . 77(10) . . . 70(9) . . . 67(9) . . . 85(10) . . . 69(9) . . . 78(10) . . . 88(11) . . . 122(12) . . . 103(11) . . . 122(12) . . . 102(11) . . . 111(12) . . . 105(12) . . . 117(12) . . . 86(10) . . . 127(13) . . . 91(11) . . . 81(10) . . . 102(11) . . . 101(11) . . . 111(12) . . . 82(10) . . . 104(11) . . . 66(9) . . . 72(9) . . . 59(9) . . . 62(9) . . . 68(9) . . . 80(10) . . . 75(10) . . . 81(10) . . . 66(9) . . . 80(10) . . . 75(10) . . . 76(10) . . . 70(9) . . . 69(9) . . . 48(8) . . . 54(8) . . . 61(9) . . . 69(9) . . . 69(9) . . . 60(9) . . . 74(10) . . . 39(7) . . . 57(8) . . . 52(8) . . . 55(8) . . . 47(8) . . . 61(9) . . . 51(8) . . . 50(8) . . . 51(8) . . . 56(8) . . . 53(8) . . . 63(9) . . . 41(7) . . . 59(9) . . . 59(9) . . . 57(9) . . . 58(9) . . . 50(8) . . . 58(9) . . . 65(9) . . . 59(9) . . . 50(8) . . . 40(7) . . . 50(8) . . . 38(7) . . . 52(8) . . . 42(7) . . . 59(9) . . . 33(6) . . . 55(8) . . . 32(6) . . . 59(9) . . . 33(6) . . . 63(9) . . . 47(8) . . . 58(9) . . . 43(7) . . . 54(8) . . . 47(8) . . . 53(8) . . . 53(8) . . . 56(8) . . . 55(8) . . . 59(9) . . . 43(7) . . . 46(8) . . . 54(8) . . . 59(9) . . . 51(8) . . . 46(8) . . . 50(8) . . . 50(8) . . . 42(7) . . . 59(9) . . . 53(8) . . . 53(8) . . . 40(7) . . . 50(8) . . . 64(9) . . . 57(8) . . . 45(8) . . . 46(8) . . . 60(9) . . . 55(8) . . . 44(7) . . . 56(8) . . . 59(9) . . . 45(8) . . . 59(9) . . . 60(9) . . . 73(10) . . . 50(8) . . . 56(8) . . . 59(9) . . . 49(8) . . . 64(9) . . . 64(9) . . . 72(10) . . . 66(9) . . . 70(9) . . . 74(10) . . . 64(9) . . . 65(9) . . . 62(9) . . . 72(10) . . . 61(9) . . . 79(10) . . . 77(10) . . . 95(11) . . . 76(10) . . . 69(9) . . . 78(10) . . . 86(10) . . . 112(12) . . . 112(12) . . . 85(10) . . . 116(12) . . . 109(12) . . . 108(12) . . . 98(11) . . . 110(12) . . . 132(13) . . . 116(12) . . . 131(13) . . . 133(13) . . . 154(14) . . . 130(13) . . . 120(12) . . . 130(13) . . . 130(13) . . . 163(14) . . . 154(14) . . . 161(14) . . . 144(13) . . . 115(12) . . . 159(14) . . . 151(14) . . . 136(13) . . . 159(14) . . . 146(14) . . . 138(13) . . . 141(13) . . . 127(13) . . . 131(13) . . . 136(13) . . . 117(12) . . . 120(12) . . . 103(11) . . . 102(11) . . . 110(12) . . . 106(12) . . . 114(12) . . . 94(11) . . . 110(12) . . . 104(11) . . . 99(11) . . . 86(10) . . . 115(12) . . . 125(13) . . . 113(12) . . . 134(13) . . . 117(12) . . . 130(13) . . . 128(13) . . . 117(12) . . . 127(13) . . . 114(12) . . . 110(12) . . . 111(12) . . . 128(13) . . . 113(12) . . . 168(15) . . . 125(13) . . . 145(14) . . . 132(13) . . . 107(12) . . . 116(12) . . . 106(12) . . . 124(13) . . . 131(13) . . . 128(13) . . . 118(12) . . . 110(12) . . . 118(12) . . . 121(12) . . . 106(12) . . . 104(11) . . . 102(11) . . . 105(12) . . . 110(12) . . . 108(12) . . . 104(11) . . . 109(12) . . . 122(12) . . . 123(12) . . . 104(11) . . . 108(12) . . . 121(12) . . . 105(11) . . . 96(11) . . . 108(12) . . . 97(11) . . . 98(11) . . . 123(12) . . . 86(10) . . . 99(11) . . . 107(12) . . . 97(11) . . . 99(11) . . . 104(12) . . . 93(11) . . . 89(11) . . . 95(11) . . . 101(11) . . . 73(10) . . . 70(9) . . . 100(11) . . . 89(11) . . . 96(11) . . . 89(11) . . . 78(10) . . . 106(12) . . . 89(11) . . . 101(11) . . . 78(10) . . . 84(10) . . . 76(10) . . . 94(11) . . . 84(10) . . . 72(10) . . . 87(10) . . . 107(12) . . . 85(10) . . . 75(10) . . . 90(11) . . . 88(11) . . . 71(10) . . . 78(10) . . . 63(9) . . . 74(10) . . . 76(10) . . . 84(10) . . . 60(9) . . . 69(9) . . . 70(9) . . . 57(9) . . . 49(8) . . . 62(9) . . . 45(8) . . . 63(9) . . . 71(10) . . . 48(8) . . . 67(9) . . . 74(10) . . . 54(8) . . . 63(9) . . . 49(8) . . . 59(9) . . . 50(8) . . . 63(9) . . . 48(8) . . . 63(9) . . . 61(9) . . . 74(10) . . . 53(8) . . . 60(9) . . . 57(8) . . . 50(8) . . . 59(9) . . . 59(9) . . . 54(8) . . . 46(8) . . . 59(9) . . . 53(8) . . . 40(7) . . . 54(8) . . . 57(8) . . . 61(9) . . . 57(8) . . . 48(8) . . . 58(9) . . . 55(8) . . . 65(9) . . . 58(9) . . . 71(9) . . . 81(10) . . . 64(9) . . . 75(10) . . . 55(8) . . . 68(9) . . . 64(9) . . . 69(9) . . . 62(9) . . . 73(10) . . . 58(9) . . . 60(9) . . . 61(9) . . . 57(9) . . . 73(10) . . . 69(9) . . . 64(9) . . . 61(9) . . . 50(8) . . . 65(9) . . . 71(10) . . . 76(10) . . . 70(9) . . . 72(10) . . . 53(8) . . . 58(9) . . . 56(8) . . . 43(7) . . . 74(10) . . . 62(9) . . . 73(10) . . . 57(9) . . . 58(9) . . . 82(10) . . . 54(8) . . . 59(9) . . . 66(9) . . . 62(9) . . . 59(9) . . . 63(9) . . . 69(9) . . . 88(11) . . . 62(9) . . . 58(9) . . . 60(9) . . . 75(10) . . . 63(9) . . . 74(10) . . . 59(9) . . . 68(9) . . . 53(8) . . . 95(11) . . . 50(8) . . . 63(9) . . . 68(9) . . . 75(10) . . . 65(9) . . . 66(9) . . . 72(10) . . . 60(9) . . . 63(9) . . . 81(10) . . . 71(9) . . . 48(8) . . . 58(9) . . . 85(10) . . . 74(10) . . . 61(9) . . . 62(9) . . . 60(9) . . . 66(9) . . . 71(9) . . . 62(9) . . . 81(10) . . . 74(10) . . . 51(8) . . . 76(10) . . . 81(10) . . . 63(9) . . . 68(9) . . . 76(10) . . . 79(10) . . . 69(9) . . . 84(10) . . . 99(11) . . . 82(10) . . . 71(10) . . . 87(11) . . . 85(10) . . . 69(9) . . . 78(10) . . . 58(9) . . . 85(10) . . . 88(11) . . . 77(10) . . . 79(10) . . . 75(10) . . . 86(10) . . . 66(9) . . . 65(9) . . . 54(8) . . . 67(9) . . . 58(9) . . . 66(9) . . . 61(9) . . . 68(9) . . . 84(10) . . . 69(9) . . . 81(10) . . . 54(8) . . . 56(8) . . . 76(10) . . . 69(9) . . . 57(9) . . . 49(8) . . . 63(9) . . . 68(9) . . . 66(9) . . . 64(9) . . . 60(9) . . . 67(9) . . . 73(10) . . . 53(8) . . . 65(9) . . . 67(9) . . . 47(8) . . . 48(8) . . . 63(9) . . . 63(9) . . . 68(9) . . . 71(10) . . . 74(10) . . . 56(8) . . . 78(10) . . . 81(10) . . . 59(9) . . . 67(9) . . . 67(9) . . . 65(9) . . . 61(9) . . . 62(9) . . . 64(9) . . . 79(10) . . . 51(8) . . . 97(11) . . . 56(8) . . . 56(8) . . . 63(9) . . . 62(9) . . . 73(10) . . . 62(9) . . . 76(10) . . . 39(7) . . . 38(7) . . . 59(9) . . . 54(8) . . . 52(8) . . . 60(9) . . . 72(10) . . . 48(8) . . . 64(9) . . . 49(8) . . . 44(8) . . . 62(9) . . . 50(8) . . . 61(9) . . . 60(9) . . . 52(8) . . . 65(9) . . . 52(8) . . . 59(9) . . . 59(9) . . . 56(8) . . . 58(9) . . . 67(9) . . . 55(8) . . . 58(9) . . . 39(7) . . . 62(9) . . . 67(9) . . . 51(8) . . . 50(8) . . . 52(8) . . . 43(7) . . . 69(9) . . . 43(7) . . . 44(8) . . . 56(8) . . . 67(9) . . . 39(7) . . . 48(8) . . . 52(8) . . . 44(8) . . . 43(7) . . . 49(8) . . . 45(8) . . . 48(8) . . . 44(8) . . . 51(8) . . . 54(8) . . . 39(7) . . . 55(8) . . . 56(8) . . . 39(7) . . . 44(8) . . . 50(8) . . . 41(7) . . . 51(8) . . . 49(8) . . . 54(8) . . . 50(8) . . . 39(7) . . . 48(8) . . . 39(7) . . . 54(8) . . . 58(9) . . . 58(9) . . . 51(8) . . . 41(7) . . . 39(7) . . . 46(8) . . . 37(7) . . . 39(7) . . . 48(8) . . . 47(8) . . . 39(7) . . . 42(7) . . . 52(8) . . . 41(7) . . . 40(7) . . . 44(8) . . . 48(8) . . . 39(7) . . . 35(7) . . . 37(7) . . . 52(8) . . . 38(7) . . . 37(7) . . . 52(8) . . . 43(7) . . . 41(7) . . . 38(7) . . . 41(7) . . . 43(7) . . . 39(7) . . . 36(7) . . . 48(8) . . . 27(6) . . . 47(8) . . . 42(7) . . . 46(8) . . . 52(8) . . . 46(8) . . . 48(8) . . . 46(8) . . . 29(6) . . . 56(8) . . . 60(9) . . . 50(8) . . . 52(8) . . . 43(7) . . . 39(7) . . . 42(7) . . . 31(6) . . . 42(7) . . . 43(7) . . . 52(8) . . . 49(8) . . . 58(9) . . . 43(7) . . . 51(8) . . . 40(7) . . . 55(8) . . . 48(8) . . . 29(6) . . . 51(8) . . . 43(7) . . . 55(8) . . . 41(7) . . . 34(7) . . . 43(7) . . . 53(8) . . . 52(8) . . . 37(7) . . . 55(8) . . . 43(7) . . . 56(8) . . . 32(6) . . . 43(7) . . . 62(9) . . . 48(8) . . . 61(9) . . . 43(7) . . . 65(9) . . . 51(8) . . . 50(8) . . . 59(9) . . . 48(8) . . . 58(9) . . . 37(7) . . . 64(9) . . . 61(9) . . . 48(8) . . . 48(8) . . . 50(8) . . . 65(9) . . . 52(8) . . . 72(10) . . . 50(8) . . . 62(9) . . . 54(8) . . . 71(10) . . . 69(9) . . . 73(10) . . . 61(9) . . . 65(9) . . . 88(11) . . . 67(9) . . . 78(10) . . . 66(9) . . . 75(10) . . . 74(10) . . . 82(10) . . . 60(9) . . . 66(9) . . . 73(10) . . . 83(10) . . . 96(11) . . . 72(10) . . . 82(10) . . . 87(11) . . . 76(10) . . . 79(10) . . . 64(9) . . . 78(10) . . . 75(10) . . . 68(9) . . . 95(11) . . . 68(9) . . . 68(9) . . . 61(9) . . . 64(9) . . . 87(11) . . . 84(10) . . . 79(10) . . . 98(11) . . . 90(11) . . . 60(9) . . . 83(10) . . . 66(9) . . . 81(10) . . . 82(10) . . . 67(9) . . . 75(10) . . . 68(9) . . . 79(10) . . . 80(10) . . . 61(9) . . . 90(11) . . . 61(9) . . . 74(10) . . . 67(9) . . . 73(10) . . . 60(9) . . . 55(8) . . . 65(9) . . . 66(9) . . . 77(10) . . . 61(9) . . . 59(9) . . . 61(9) . . . 45(8) . . . 60(9) . . . 58(9) . . . 65(9) . . . 50(8) . . . 63(9) . . . 58(9) . . . 69(9) . . . 72(10) . . . 53(8) . . . 51(8) . . . 48(8) . . . 47(8) . . . 60(9) . . . 56(8) . . . 63(9) . . . 43(7) . . . 45(8) . . . 47(8) . . . 47(8) . . . 32(6) . . . 55(8) . . . 63(9) . . . 37(7) . . . 43(7) . . . 47(8) . . . 52(8) . . . 43(7) . . . 58(9) . . . 40(7) . . . 45(8) . . . 45(8) . . . 41(7) . . . 49(8) . . . 41(7) . . . 50(8) . . . 53(8) . . . 56(8) . . . 52(8) . . . 58(9) . . . 52(8) . . . 52(8) . . . 43(7) . . . 52(8) . . . 45(8) . . . 46(8) . . . 56(8) . . . 45(8) . . . 56(8) . . . 54(8) . . . 47(8) . . . 58(9) . . . 45(8) . . . 51(8) . . . 50(8) . . . 51(8) . . . 52(8) . . . 57(9) . . . 58(9) . . . 49(8) . . . 59(9) . . . 51(8) . . . 55(8) . . . 61(9) . . . 51(8) . . . 42(7) . . . 46(8) . . . 39(7) . . . 54(8) . . . 48(8) . . . 61(9) . . . 62(9) . . . 55(8) . . . 51(8) . . . 54(8) . . . 71(10) . . . 59(9) . . . 47(8) . . . 49(8) . . . 45(8) . . . 46(8) . . . 60(9) . . . 54(8) . . . 50(8) . . . 55(8) . . . 57(9) . . . 60(9) . . . 46(8) . . . 54(8) . . . 54(8) . . . 65(9) . . . 57(9) . . . 41(7) . . . 61(9) . . . 46(8) . . . 67(9) . . . 51(8) . . . 63(9) . . . 46(8) . . . 57(9) . . . 66(9) . . . 55(8) . . . 65(9) . . . 50(8) . . . 59(9) . . . 69(9) . . . 74(10) . . . 60(9) . . . 70(10) . . . 84(10) . . . 63(9) . . . 74(10) . . . 71(10) . . . 73(10) . . . 79(10) . . . 92(11) . . . 66(9) . . . 79(10) . . . 92(11) . . . 79(10) . . . 93(11) . . . 104(12) . . . 113(12) . . . 126(13) . . . 111(12) . . . 115(12) . . . 110(12) . . . 112(12) . . . 122(13) . . . 98(11) . . . 116(12) . . . 107(12) . . . 102(11) . . . 125(13) . . . 98(11) . . . 91(11) . . . 124(13) . . . 103(12) . . . 104(12) . . . 84(10) . . . 107(12) . . . 78(10) . . . 102(11) . . . 97(11) . . . 87(11) . . . 87(11) . . . 98(11) . . . 74(10) . . . 88(11) . . . 68(9) . . . 98(11) . . . 86(11) . . . 82(10) . . . 83(10) . . . 79(10) . . . 72(10) . . . 72(10) . . . 59(9) . . . 57(9) . . . 94(11) . . . 78(10) . . . 60(9) . . . 82(10) . . . 69(9) . . . 68(9) . . . 63(9) . . . 82(10) . . . 72(10) . . . 85(10) . . . 67(9) . . . 67(9) . . . 99(11) . . . 85(11) . . . 67(9) . . . 81(10) . . . 75(10) . . . 94(11) . . . 101(11) . . . 88(11) . . . 78(10) . . . 87(11) . . . 91(11) . . . 82(10) . . . 110(12) . . . 95(11) . . . 97(11) . . . 87(11) . . . 87(11) . . . 96(11) . . . 118(12) . . . 126(13) . . . 122(13) . . . 105(12) . . . 99(11) . . . 134(13) . . . 152(14) . . . 106(12) . . . 122(13) . . . 129(13) . . . 115(12) . . . 124(13) . . . 112(12) . . . 122(13) . . . 106(12) . . . 102(12) . . . 108(12) . . . 97(11) . . . 78(10) . . . 114(12) . . . 103(12) . . . 100(11) . . . 90(11) . . . 68(9) . . . 84(10) . . . 73(10) . . . 77(10) . . . 66(9) . . . 83(10) . . . 65(9) . . . 72(10) . . . 80(10) . . . 80(10) . . . 62(9) . . . 66(9) . . . 79(10) . . . 67(9) . . . 69(9) . . . 72(10) . . . 64(9) . . . 61(9) . . . 83(10) . . . 42(7) . . . 68(9) . . . 86(11) . . . 67(9) . . . 71(10) . . . 58(9) . . . 74(10) . . . 81(10) . . . 51(8) . . . 49(8) . . . 67(9) . . . 62(9) . . . 71(10) . . . 77(10) . . . 73(10) . . . 66(9) . . . 67(9) . . . 78(10) . . . 70(10) . . . 78(10) . . . 76(10) . . . 62(9) . . . 71(10) . . . 65(9) . . . 79(10) . . . 62(9) . . . 63(9) . . . 72(10) . . . 73(10) . . . 77(10) . . . 65(9) . . . 68(9) . . . 68(9) . . . 55(9) . . . 72(10) . . . 62(9) . . . 51(8) . . . 55(8) . . . 67(9) . . . 62(9) . . . 45(8) . . . 71(10) . . . 50(8) . . . 60(9) . . . 59(9) . . . 82(10) . . . 57(9) . . . 53(8) . . . 56(9) . . . 81(10) . . . 63(9) . . . 46(8) . . . 50(8) . . . 53(8) . . . 39(7) . . . 57(9) . . . 54(8) . . . 53(8) . . . 46(8) . . . 64(9) . . . 55(8) . . . 59(9) . . . 50(8) . . . 44(8) . . . 56(9) . . . 65(9) . . . 57(9) . . . 63(9) . . . 39(7) . . . 46(8) . . . 49(8) . . . 49(8) . . . 66(9) . . . 50(8) . . . 42(7) . . . 80(10) . . . 50(8) . . . 59(9) . . . 64(9) . . . 63(9) . . . 58(9) . . . 67(9) . . . 49(8) . . . 66(9) . . . 66(9) . . . 69(9) . . . 67(9) . . . 77(10) . . . 73(10) . . . 65(9) . . . 77(10) . . . 66(9) . . . 71(10) . . . 75(10) . . . 86(11) . . . 85(10) . . . 88(11) . . . 86(11) . . . 86(11) . . . 72(10) . . . 79(10) . . . 88(11) . . . 77(10) . . . 100(11) . . . 89(11) . . . 73(10) . . . 108(12) . . . 99(11) . . . 98(11) . . . 116(12) . . . 103(12) . . . 99(11) . . . 111(12) . . . 128(13) . . . 140(13) . . . 110(12) . . . 149(14) . . . 130(13) . . . 140(13) . . . 130(13) . . . 159(14) . . . 133(13) . . . 148(14) . . . 148(14) . . . 151(14) . . . 153(14) . . . 144(14) . . . 147(14) . . . 135(13) . . . 147(14) . . . 143(14) . . . 125(13) . . . 139(13) . . . 129(13) . . . 115(12) . . . 127(13) . . . 145(14) . . . 121(12) . . . 122(13) . . . 141(14) . . . 116(12) . . . 120(12) . . . 129(13) . . . 115(12) . . . 91(11) . . . 119(12) . . . 96(11) . . . 122(13) . . . 87(11) . . . 116(12) . . . 97(11) . . . 111(12) . . . 106(12) . . . 77(10) . . . 95(11) . . . 113(12) . . . 98(11) . . . 87(11) . . . 82(10) . . . 81(10) . . . 77(10) . . . 98(11) . . . 82(10) . . . 92(11) . . . 93(11) . . . 81(10) . . . 80(10) . . . 87(11) . . . 76(10) . . . 75(10) . . . 72(10) . . . 66(9) . . . 71(10) . . . 73(10) . . . 61(9) . . . 54(8) . . . 51(8) . . . 48(8) . . . 63(9) . . . 48(8) . . . 65(9) . . . 70(10) . . . 54(8) . . . 52(8) . . . 67(9) . . . 41(7) . . . 41(7) . . . 56(9) . . . 45(8) . . . 42(7) . . . 64(9) . . . 49(8) . . . 55(9) . . . 45(8) . . . 48(8) . . . 50(8) . . . 58(9) . . . 54(8) . . . 59(9) . . . 40(7) . . . 43(7) . . . 49(8) . . . 48(8) . . . 41(7) . . . 48(8) . . . 49(8) . . . 34(7) . . . 45(8) . . . 46(8) . . . 53(8) . . . 55(9) . . . 42(7) . . . 47(8) . . . 43(7) . . . 48(8) . . . 40(7) . . . 53(8) . . . 45(8) . . . 48(8) . . . 50(8) . . . 22(5) . . . 45(8) . . . 40(7) . . . 43(7) . . . 55(8) . . . 29(6) . . . 48(8) . . . 28(6) . . . 38(7) . . . 57(9) . . . 40(7) . . . 32(6) . . . 48(8) . . . 54(8) . . . 40(7) . . . 34(7) . . . 42(7) . . . 41(7) . . . 48(8) . . . 54(8) . . . 45(8) . . . 36(7) . . . 53(8) . . . 34(7) . . . 36(7) . . . 44(8) . . . 31(6) . . . 49(8) . . . 45(8) . . . 41(7) . . . 34(7) . . . 42(7) . . . 45(8) . . . 36(7) . . . 48(8) . . . 41(7) . . . 51(8) . . . 40(7) . . . 40(7) . . . 35(7) . . . 32(7) . . . 47(8) . . . 36(7) . . . 48(8) . . . 57(9) . . . 38(7) . . . 47(8) . . . 43(8) . . . 31(6) . . . 35(7) . . . 40(7) . . . 45(8) . . . 35(7) . . . 34(7) . . . 62(9) . . . 39(7) . . . 27(6) . . . 42(7) . . . 39(7) . . . 39(7) . . . 54(8) . . . 33(7) . . . 43(7) . . . 44(8) . . . 37(7) . . . 44(8) . . . 49(8) . . . 56(9) . . . 32(7) . . . 42(7) . . . 34(7) . . . 49(8) . . . 34(7) . . . 38(7) . . . 40(7) . . . 45(8) . . . 35(7) . . . 52(8) . . . 62(9) . . . 60(9) . . . 45(8) . . . 45(8) . . . 37(7) . . . 45(8) . . . 48(8) . . . 44(8) . . . 35(7) . . . 29(6) . . . 45(8) . . . 48(8) . . . 67(9) . . . 40(7) . . . 39(7) . . . 54(8) . . . 59(9) . . . 43(7) . . . 49(8) . . . 45(8) . . . 57(9) . . . 46(8) . . . 62(9) . . . 43(7) . . . 51(8) . . . 52(8) . . . 41(7) . . . 61(9) . . . 48(8) . . . 38(7) . . . 42(7) . . . 48(8) . . . 32(7) . . . 30(6) . . . 42(7) . . . 64(9) . . . 63(9) . . . 58(9) . . . 51(8) . . . 47(8) . . . 58(9) . . . 50(8) . . . 52(8) . . . 65(9) . . . 48(8) . . . 57(9) . . . 80(10) . . . 53(8) . . . 69(10) . . . 70(10) . . . 64(9) . . . 64(9) . . . 66(9) . . . 60(9) . . . 57(9) . . . 61(9) . . . 68(9) . . . 74(10) . . . 61(9) . . . 66(9) . . . 91(11) . . . 66(9) . . . 68(9) . . . 76(10) . . . 69(9) . . . 58(9) . . . 80(10) . . . 60(9) . . . 45(8) . . . 69(10) . . . 71(10) . . . 76(10) . . . 67(9) . . . 76(10) . . . 65(9) . . . 64(9) . . . 72(10) . . . 83(10) . . . 77(10) . . . 82(10) . . . 71(10) . . . 75(10) . . . 88(11) . . . 92(11) . . . 91(11) . . . 86(11) . . . 100(11) . . . 97(11) . . . 95(11) . . . 108(12) . . . 96(11) . . . 106(12) . . . 98(11) . . . 102(12) . . . 129(13) . . . 124(13) . . . 107(12) . . . 109(12) . . . 112(12) . . . 119(12) . . . 118(12) . . . 146(14) . . . 116(12) . . . 134(13) . . . 121(13) . . . 123(13) . . . 121(13) . . . 109(12) . . . 119(12) . . . 153(14) . . . 113(12) . . . 110(12) . . . 128(13) . . . 125(13) . . . 120(13) . . . 110(12) . . . 116(12) . . . 95(11) . . . 93(11) . . . 112(12) . . . 110(12) . . . 110(12) . . . 123(13) . . . 93(11) . . . 107(12) . . . 110(12) . . . 115(12) . . . 135(13) . . . 122(13) . . . 117(12) . . . 102(12) . . . 114(12) . . . 107(12) . . . 138(13) . . . 106(12) . . . 108(12) . . . 140(14) . . . 96(11) . . . 98(11) . . . 109(12) . . . 120(12) . . . 109(12) . . . 127(13) . . . 99(11) . . . 105(12) . . . 89(11) . . . 120(13) . . . 88(11) . . . 100(11) . . . 104(12) . . . 110(12) . . . 90(11) . . . 100(11) . . . 87(11) . . . 90(11) . . . 69(10) . . . 101(12) . . . 88(11) . . . 87(11) . . . 82(10) . . . 112(12) . . . 66(9) . . . 92(11) . . . 78(10) . . . 67(9) . . . 78(10) . . . 52(8) . . . 85(11) . . . 72(10) . . . 65(9) . . . 50(8) . . . 55(8) . . . 50(8) . . . 69(9) . . . 60(9) . . . 75(10) . . . 71(10) . . . 58(9) . . . 57(9) . . . 58(9) . . . 64(9) . . . 65(9) . . . 53(8) . . . 56(9) . . . 60(9) . . . 29(6) . . . 54(8) . . . 48(8) . . . 54(8) . . . 51(8) . . . 69(9) . . . 40(7) . . . 47(8) . . . 46(8) . . . 41(7) . . . 55(8) . . . 59(9) . . . 46(8) . . . 57(9) . . . 62(9) . . . 42(7) . . . 69(10) . . . 59(9) . . . 42(7) . . . 55(8) . . . 56(9) . . . 48(8) . . . 52(8) . . . 46(8) . . . 61(9) . . . 48(8) . . . 51(8) . . . 39(7) . . . 65(9) . . . 58(9) . . . 38(7) . . . 52(8) . . . 39(7) . . . 55(9) . . . 29(6) . . . 35(7) . . . 46(8) . . . 48(8) . . . 34(7) . . . 59(9) . . . 47(8) . . . 39(7) . . . 44(8) . . . 46(8) . . . 48(8) . . . 41(7) . . . 59(9) . . . 40(7) . . . 38(7) . . . 60(9) . . . 43(8) . . . 56(9) . . . 50(8) . . . 47(8) . . . 48(8) . . . 51(8) . . . 42(7) . . . 39(7) . . . 49(8) . . . 57(9) . . . 35(7) . . . 42(7) . . . 44(8) . . . 37(7) . . . 39(7) . . . 56(9) . . . 38(7) . . . 46(8) . . . 47(8) . . . 53(8) . . . 47(8) . . . 42(7) . . . 38(7) . . . 43(8) . . . 42(7) . . . 40(7) . . . 54(8) . . . 41(7) . . . 34(7) . . . 38(7) . . . 68(9) . . . 53(8) . . . 48(8) . . . 52(8) . . . 34(7) . . . 46(8) . . . 46(8) . . . 42(7) . . . 45(8) . . . 45(8) . . . 52(8) . . . 52(8) . . . 68(9) . . . 51(8) . . . 73(10) . . . 56(9) . . . 66(9) . . . 41(7) . . . 59(9) . . . 43(8) . . . 55(9) . . . 44(8) . . . 61(9) . . . 73(10) . . . 72(10) . . . 80(10) . . . 62(9) . . . 72(10) . . . 63(9) . . . 82(10) . . . 76(10) . . . 55(9) . . . 47(8) . . . 69(10) . . . 87(11) . . . 73(10) . . . 65(9) . . . 75(10) . . . 68(9) . . . 74(10) . . . 65(9) . . . 88(11) . . . 65(9) . . . 60(9) . . . 72(10) . . . 64(9) . . . 49(8) . . . 72(10) . . . 60(9) . . . 57(9) . . . 73(10) . . . 64(9) . . . 51(8) . . . 80(10) . . . 71(10) . . . 53(8) . . . 56(9) . . . 61(9) . . . 47(8) . . . 38(7) . . . 47(8) . . . 37(7) . . . 46(8) . . . 66(9) . . . 57(9) . . . 45(8) . . . 47(8) . . . 55(9) . . . 42(7) . . . 56(9) . . . 51(8) . . . 58(9) . . . 53(8) . . . 37(7) . . . 31(6) . . . 45(8) . . . 55(8) . . . 46(8) . . . 39(7) . . . 64(9) . . . 67(9) . . . 43(8) . . . 38(7) . . . 46(8) . . . 37(7) . . . 53(8) . . . 41(7) . . . 40(7) . . . 52(8) . . . 51(8) . . . 41(7) . . . 60(9) . . . 48(8) . . . 43(8) . . . 39(7) . . . 54(8) . . . 53(8) . . . 46(8) . . . 50(8) . . . 46(8) . . . 41(7) . . . 43(8) . . . 51(8) . . . 46(8) . . . 43(8) . . . 54(8) . . . 51(8) . . . 41(7) . . . 42(7) . . . 33(7) . . . 50(8) . . . 54(8) . . . 46(8) . . . 49(8) . . . 51(8) . . . 42(8) . . . 32(6) . . . 45(8) . . . 49(8) . . . 35(7) . . . 34(7) . . . 39(7) . . . 39(7) . . . 46(8) . . . 45(8) . . . 42(7) . . . 39(7) . . . 44(8) . . . 61(9) . . . 47(8) . . . 54(8) . . . 48(8) . . . 55(9) . . . 59(9) . . . 56(9) . . . 41(7) . . . 55(9) . . . 50(8) . . . 60(9) . . . 59(9) . . . 50(8) . . . 49(8) . . . 39(7) . . . 74(10) . . . 47(8) . . . 59(9) . . . 45(8) . . . 54(8) . . . 59(9) . . . 45(8) . . . 64(9) . . . 51(8) . . . 42(8) . . . 60(9) . . . 50(8) . . . 53(8) . . . 71(10) . . . 51(8) . . . 62(9) . . . 62(9) . . . 75(10) . . . 58(9) . . . 58(9) . . . 80(10) . . . 49(8) . . . 47(8) . . . 64(9) . . . 57(9) . . . 64(9) . . . 61(9) . . . 63(9) . . . 61(9) . . . 54(9) . . . 41(7) . . . 33(7) . . . 68(9) . . . 56(9) . . . 48(8) . . . 57(9) . . . 65(9) . . . 60(9) . . . 41(7) . . . 58(9) . . . 50(8) . . . 64(9) . . . 50(8) . . . 44(8) . . . 33(7) . . . 50(8) . . . 42(7) . . . 55(9) . . . 52(8) . . . 42(7) . . . 37(7) . . . 50(8) . . . 49(8) . . . 51(8) . . . 42(7) . . . 54(8) . . . 73(10) . . . 38(7) . . . 44(8) . . . 59(9) . . . 46(8) . . . 63(9) . . . 50(8) . . . 41(7) . . . 34(7) . . . 43(8) . . . 54(8) . . . 33(7) . . . 41(7) . . . 41(7) . . . 34(7) . . . 33(7) . . . 50(8) . . . 34(7) . . . 29(6) . . . 37(7) . . . 43(8) . . . 49(8) . . . 50(8) . . . 42(7) . . . 58(9) . . . 48(8) . . . 32(6) . . . 33(7) . . . 46(8) . . . 41(7) . . . 42(8) . . . 44(8) . . . 42(8) . . . 40(7) . . . 43(8) . . . 44(8) . . . 46(8) . . . 46(8) . . . 29(6) . . . 54(8) . . . 47(8) . . . 46(8) . . . 41(7) . . . 33(7) . . . 34(7) . . . 52(8) . . . 44(8) . . . 38(7) . . . 29(6) . . . 40(7) . . . 41(7) . . . 50(8) . . . 45(8) . . . 54(8) . . . 56(9) . . . 51(8) . . . 51(8) . . . 62(9) . . . 42(7) . . . 44(8) . . . 53(8) . . . 55(9) . . . 37(7) . . . 51(8) . . . 42(7) . . . 41(7) . . . 46(8) . . . 66(9) . . . 38(7) . . . 53(8) . . . 50(8) . . . 42(8) . . . 42(8) . . . 58(9) . . . 49(8) . . . 49(8) . . . 37(7) . . . 53(8) . . . 57(9) . . . 67(9) . . . 42(7) . . . 44(8) . . . 41(7) . . . 36(7) . . . 44(8) . . . 47(8) . . . 40(7) . . . 42(8) . . . 29(6) . . . 49(8) . . . 36(7) . . . 34(7) . . . 36(7) . . . 41(7) . . . 39(7) . . . 46(8) . . . 38(7) . . . 38(7) . . . 30(6) . . . 41(7) . . . 36(7) . . . 32(7) . . . 29(6) . . . 50(8) . . . 41(7) . . . 33(7) . . . 25(6) . . . 49(8) . . . 22(5) . . . 37(7) . . . 28(6) . . . 34(7) . . . 36(7) . . . 31(6) . . . 38(7) . . . 29(6) . . . 38(7) . . . 41(7) . . . 29(6) . . . 44(8) . . . 46(8) . . . 30(6) . . . 40(7) . . . 42(8) . . . 36(7) . . . 39(7) . . . 42(8) . . . 29(6) . . . 45(8) . . . 38(7) . . . 30(6) . . . 43(8) . . . 33(7) . . . 37(7) . . . 31(6) . . . 34(7) . . . 40(7) . . . 50(8) . . . 35(7) . . . 38(7) . . . 44(8) . . . 34(7) . . . 29(6) . . . 40(7) . . . 41(7) . . . 25(6) . . . 34(7) . . . 53(8) . . . 37(7) . . . 37(7) . . . 32(7) . . . 30(6) . . . 43(8) . . . 44(8) . . . 25(6) . . . 36(7) . . . 40(7) . . . 36(7) . . . 48(8) . . . 32(7) . . . 45(8) . . . 49(8) . . . 33(7) . . . 34(7) . . . 45(8) . . . 52(8) . . . 50(8) . . . 31(6) . . . 34(7) . . . 45(8) . . . 48(8) . . . 25(6) . . . 37(7) . . . 45(8) . . . 41(7) . . . 34(7) . . . 25(6) . . . 36(7) . . . 45(8) . . . 48(8) . . . 45(8) . . . 37(7) . . . 41(7) . . . 42(8) . . . 39(7) . . . 32(7) . . . 32(7) . . . 37(7) . . . 40(7) . . . 46(8) . . . 40(7) . . . 38(7) . . . 31(6) . . . 42(7) . . . 57(9) . . . 35(7) . . . 52(8) . . . 54(9) . . . 37(7) . . . 45(8) . . . 36(7) . . . 56(9) . . . 41(7) . . . 55(9) . . . 46(8) . . . 56(9) . . . 52(8) . . . 44(8) . . . 49(8) . . . 49(8) . . . 49(8) . . . 69(10) . . . 69(10) . . . 48(8) . . . 66(9) . . . 77(10) . . . 72(10) . . . 65(9) . . . 85(11) . . . 78(10) . . . 61(9) . . . 43(8) . . . 70(10) . . . 64(9) . . . 64(9) . . . 59(9) . . . 92(11) . . . 56(9) . . . 67(9) . . . 60(9) . . . 71(10) . . . 61(9) . . . 57(9) . . . 78(10) . . . 63(9) . . . 61(9) . . . 73(10) . . . 68(10) . . . 45(8) . . . 54(9) . . . 65(9) . . . 56(9) . . . 42(8) . . . 66(9) . . . 61(9) . . . 42(8) . . . 63(9) . . . 41(7) . . . 46(8) . . . 44(8) . . . 49(8) . . . 65(9) . . . 45(8) . . . 49(8) . . . 36(7) . . . 51(8) . . . 44(8) . . . 44(8) . . . 41(7) . . . 41(7) . . . 48(8) . . . 37(7) . . . 47(8) . . . 40(7) . . . 38(7) . . . 60(9) . . . 29(6) . . . 48(8) . . . 48(8) . . . 49(8) . . . 36(7) . . . 64(9) . . . 38(7) . . . 40(7) . . . 36(7) . . . 49(8) . . . 53(8) . . . 45(8) . . . 42(6) . . . 47(7) . . . 46(7) . . . 43(6) . . . 45(6) . . . 53(7) . . . 50(7) . . . 47(7) . . . 52(7) . . . 49(7) . . . 41(6) . . . 53(7) . . . 47(7) . . . 38(6) . . . 48(7) . . . 49(7) . . . 52(7) . . . 56(7) . . . 43(6) . . . 42(6) . . . 52(7) . . . 47(7) . . . 61(8) . . . 55(7) . . . 52(7) . . . 41(6) . . . 38(6) . . . 42(6) . . . 46(7) . . . 40(6) . . . 43(6) . . . 45(6) . . . 42(6) . . . 45(7) . . . 42(6) . . . 42(6) . . . 48(7) . . . 33(6) . . . 43(6) . . . 38(6) . . . 33(6) . . . 44(6) . . . 47(7) . . . 35(6) . . . 40(6) . . . 37(6) . . . 47(7) . . . 30(5) . . . 41(6) . . . 33(6) . . . 56(7) . . . 35(6) . . . 42(6) . . . 25(5) . . . 33(6) . . . 44(6) . . . 46(7) . . . 40(6) . . . 43(6) . . . 28(5) . . . 45(7) . . . 33(6) . . . 38(6) . . . 47(7) . . . 36(6) . . . 36(6) . . . 39(6) . . . 46(7) . . . 43(6) . . . 36(6) . . . 37(6) . . . 42(6) . . . 38(6) . . . 43(6) . . . 33(6) . . . 46(7) . . . 43(6) . . . 35(6) . . . 40(6) . . . 41(6) . . . 47(7) . . . 35(6) . . . 37(6) . . . 46(7) . . . 45(7) . . . 48(7) . . . 41(6) . . . 48(7) . . . 38(6) . . . 48(7) . . . 51(7) . . . 53(7) . . . 45(7) . . . 47(7) . . . 49(7) . . . 39(6) . . . 37(6) . . . 50(7) . . . 36(6) . . . 43(6) . . . 48(7) . . . 49(7) . . . 42(6) . . . 45(7) . . . 45(7) . . . 38(6) . . . 47(7) . . . 33(6) . . . 48(7) . . . 61(8) . . . 44(6) . . . 45(7) . . . 48(7) . . . 45(7) . . . 53(7) . . . 47(7) . . . 43(6) . . . 54(7) . . . 47(7) . . . 48(7) . . . 45(7) . . . 70(8) . . . 41(6) . . . 34(6) . . . 50(7) . . . 49(7) . . . 49(7) . . . 43(6) . . . 47(7) . . . 36(6) . . . 60(8) . . . 37(6) . . . 34(6) . . . 46(7) . . . 45(7) . . . 54(7) . . . 46(7) . . . 39(6) . . . 49(7) . . . 41(6) . . . 57(7) . . . 53(7) . . . 53(7) . . . 29(5) . . . 41(6) . . . 40(6) . . . 45(7) . . . 53(7) . . . 50(7) . . . 57(7) . . . 35(6) . . . 52(7) . . . 49(7) . . . 36(6) . . . 47(7) . . . 58(7) . . . 50(7) . . . 47(7) . . . 44(6) . . . 45(6) . . . 49(7) . . . 45(7) . . . 38(6) . . . 45(7) . . . 41(6) . . . 48(7) . . . 45(7) . . . 49(7) . . . 43(6) . . . 43(6) . . . 39(6) . . . 38(6) . . . 51(7) . . . 50(7) . . . 45(7) . . . 34(6) . . . 45(7) . . . 42(6) . . . 42(6) . . . 45(7) . . . 52(7) . . . 50(7) . . . 50(7) . . . 64(8) . . . 38(6) . . . 51(7) . . . 58(7) . . . 39(6) . . . 52(7) . . . 53(7) . . . 48(7) . . . 62(8) . . . 40(6) . . . 48(7) . . . 50(7) . . . 55(7) . . . 54(7) . . . 41(6) . . . 54(7) . . . 36(6) . . . 54(7) . . . 57(7) . . . 44(6) . . . 47(7) . . . 56(7) . . . 40(6) . . . 36(6) . . . 54(7) . . . 51(7) . . . 54(7) . . . 50(7) . . . 52(7) . . . 49(7) . . . 67(8) . . . 60(8) . . . 54(7) . . . 43(6) . . . 44(6) . . . 45(7) . . . 43(6) . . . 43(6) . . . 41(6) . . . 48(7) . . . 41(6) . . . 43(6) . . . 55(7) . . . 41(6) . . . 40(6) . . . 51(7) . . . 45(7) . . . 44(6) . . . 47(7) . . . 39(6) . . . 41(6) . . . 58(7) . . . 55(7) . . . 54(7) . . . 53(7) . . . 49(7) . . . 46(7) . . . 48(7) . . . 42(6) . . . 45(7) . . . 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40(6) . . . 51(7) . . . 45(7) . . . 51(7) . . . 58(7) . . . 47(7) . . . 49(7) . . . 41(6) . . . 57(7) . . . 48(7) . . . 58(7) . . . 45(7) . . . 69(8) . . . 64(8) . . . 54(7) . . . 62(8) . . . 64(8) . . . 62(8) . . . 73(8) . . . 62(8) . . . 62(8) . . . 77(9) . . . 71(8) . . . 82(9) . . . 68(8) . . . 57(7) . . . 67(8) . . . 59(8) . . . 73(8) . . . 85(9) . . . 79(9) . . . 89(9) . . . 75(8) . . . 87(9) . . . 84(9) . . . 69(8) . . . 99(10) . . . 75(8) . . . 64(8) . . . 100(10) . . . 79(9) . . . 79(9) . . . 63(8) . . . 81(9) . . . 73(8) . . . 69(8) . . . 69(8) . . . 50(7) . . . 72(8) . . . 64(8) . . . 60(8) . . . 59(8) . . . 68(8) . . . 45(7) . . . 49(7) . . . 49(7) . . . 81(9) . . . 64(8) . . . 58(7) . . . 69(8) . . . 52(7) . . . 64(8) . . . 49(7) . . . 40(6) . . . 67(8) . . . 32(6) . . . 54(7) . . . 49(7) . . . 41(6) . . . 48(7) . . . 42(6) . . . 53(7) . . . 53(7) . . . 34(6) . . . 52(7) . . . 62(8) . . . 57(7) . . . 48(7) . . . 48(7) . . . 41(6) . . . 57(7) . . . 44(6) . . . 65(8) . . . 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41(7) . . . 44(7) . . . 50(7) . . . 49(7) . . . 43(7) . . . 45(7) . . . 43(7) . . . 51(7) . . . 33(6) . . . 46(7) . . . 48(7) . . . 42(7) . . . 50(7) . . . 47(7) . . . 33(6) . . . 36(6) . . . 34(6) . . . 35(6) . . . 55(8) . . . 34(6) . . . 35(6) . . . 53(7) . . . 43(7) . . . 45(7) . . . 43(7) . . . 28(5) . . . 39(6) . . . 38(6) . . . 33(6) . . . 50(7) . . . 46(7) . . . 27(5) . . . 43(7) . . . 43(7) . . . 38(6) . . . 42(7) . . . 48(7) . . . 45(7) . . . 42(7) . . . 44(7) . . . 56(8) . . . 39(6) . . . 51(7) . . . 36(6) . . . 45(7) . . . 33(6) . . . 39(6) . . . 37(6) . . . 48(7) . . . 30(6) . . . 34(6) . . . 41(7) . . . 37(6) . . . 44(7) . . . 57(8) . . . 46(7) . . . 35(6) . . . 47(7) . . . 26(5) . . . 39(6) . . . 35(6) . . . 47(7) . . . 52(7) . . . 42(7) . . . 31(6) . . . 40(6) . . . 41(7) . . . 44(7) . . . 36(6) . . . 40(6) . . . 47(7) . . . 37(6) . . . 52(7) . . . 36(6) . . . 48(7) . . . 42(7) . . . 47(7) . . . 36(6) . . . 54(8) . . . 32(6) . . . 41(7) . . . 53(7) . . . 44(7) . . . 34(6) . . . 47(7) . . . 56(8) . . . 55(8) . . . 49(7) . . . 44(7) . . . 46(7) . . . 50(7) . . . 46(7) . . . 47(7) . . . 37(6) . . . 36(6) . . . 48(7) . . . 52(7) . . . 45(7) . . . 39(6) . . . 45(7) . . . 54(8) . . . 47(7) . . . 39(6) . . . 55(8) . . . 58(8) . . . 45(7) . . . 54(8) . . . 50(7) . . . 47(7) . . . 48(7) . . . 44(7) . . . 42(7) . . . 52(7) . . . 66(8) . . . 40(7) . . . 33(6) . . . 61(8) . . . 42(7) . . . 33(6) . . . 39(6) . . . 46(7) . . . 34(6) . . . 39(6) . . . 52(7) . . . 38(6) . . . 50(7) . . . 50(7) . . . 48(7) . . . 33(6) . . . 49(7) . . . 37(6) . . . 54(8) . . . 57(8) . . . 39(6) . . . 28(5) . . . 43(7) . . . 50(7) . . . 49(7) . . . 43(7) . . . 42(7) . . . 37(6) . . . 37(6) . . . 40(7) . . . 46(7) . . . 49(7) . . . 43(7) . . . 40(7) . . . 50(7) . . . 48(7) . . . 43(7) . . . 56(8) . . . 54(8) . . . 47(7) . . . 48(7) . . . 51(7) . . . 35(6) . . . 37(6) . . . 42(7) . . . 43(7) . . . 49(7) . . . 47(7) . . . 38(6) . . . 44(7) . . . 40(6) . . . 37(6) . . . 42(7) . . . 43(7) . . . 46(7) . . . 41(7) . . . 60(8) . . . 39(6) . . . 28(5) . . . 40(7) . . . 52(7) . . . 34(6) . . . 37(6) . . . 33(6) . . . 38(6) . . . 47(7) . . . 41(7) . . . 35(6) . . . 51(7) . . . 52(7) . . . 42(7) . . . 50(7) . . . 61(8) . . . 34(6) . . . 47(7) . . . 54(8) . . . 54(8) . . . 26(5) . . . 43(7) . . . 37(6) . . . 37(6) . . . 33(6) . . . 50(7) . . . 55(8) . . . 39(6) . . . 56(8) . . . 40(7) . . . 42(7) . . . 41(7) . . . 46(7) . . . 39(6) . . . 47(7) . . . 43(7) . . . 44(7) . . . 41(7) . . . 43(7) . . . 45(7) . . . 38(6) . . . 38(6) . . . 47(7) . . . 38(6) . . . 41(7) . . . 55(8) . . . 40(7) . . . 40(7) . . . 31(6) . . . 37(6) . . . 45(7) . . . 47(7) . . . 41(7) . . . 41(7) . . . 39(6) . . . 39(6) . . . 41(7) . . . 41(7) . . . 52(7) . . . 46(7) . . . 49(7) . . . 50(7) . . . 49(7) . . . 44(7) . . . 42(7) . . . 40(7) . . . 40(7) . . . 58(8) . . . 52(7) . . . 54(8) . . . 39(6) . . . 40(6) . . . 55(8) . . . 51(7) . . . 40(7) . . . 30(6) . . . 40(6) . . . 42(7) . . . 49(7) . . . 35(6) . . . 40(7) . . . 50(7) . . . 49(7) . . . 43(7) . . . 40(7) . . . 40(7) . . . 47(7) . . . 53(8) . . . 42(7) . . . 56(8) . . . 43(7) . . . 53(7) . . . 43(7) . . . 35(6) . . . 49(7) . . . 46(7) . . . 66(8) . . . 60(8) . . . 50(7) . . . 43(7) . . . 54(8) . . . 52(7) . . . 52(7) . . . 58(8) . . . 47(7) . . . 42(7) . . . 52(7) . . . 67(8) . . . 47(7) . . . 51(7) . . . 45(7) . . . 37(6) . . . 51(7) . . . 39(7) . . . 39(6) . . . 50(7) . . . 41(7) . . . 57(8) . . . 43(7) . . . 56(8) . . . 58(8) . . . 49(7) . . . 51(7) . . . 59(8) . . . 44(7) . . . 41(7) . . . 47(7) . . . 53(8) . . . 49(7) . . . 54(8) . . . 41(7) . . . 52(7) . . . 51(7) . . . 42(7) . . . 45(7) . . . 39(6) . . . 42(7) . . . 60(8) . . . 44(7) . . . 47(7) . . . 33(6) . . . 60(8) . . . 44(7) . . . 45(7) . . . 48(7) . . . 44(7) . . . 48(7) . . . 45(7) . . . 34(6) . . . 47(7) . . . 45(7) . . . 46(7) . . . 39(6) . . . 58(8) . . . 47(7) . . . 46(7) . . . 56(8) . . . 40(7) . . . 49(7) . . . 48(7) . . . 51(7) . . . 38(6) . . . 48(7) . . . 36(6) . . . 37(6) . . . 39(6) . . . 43(7) . . . 34(6) . . . 38(6) . . . 45(7) . . . 46(7) . . . 40(7) . . . 41(7) . . . 46(7) . . . 34(6) . . . 61(8) . . . 35(6) . . . 40(7) . . . 43(7) . . . 54(8) . . . 46(7) . . . 53(7) . . . 49(7) . . . 35(6) . . . 44(7) . . . 41(7) . . . 30(6) . . . 38(6) . . . 28(5) . . . 43(7) . . . 41(7) . . . 40(7) . . . 46(7) . . . 48(7) . . . 40(7) . . . 39(6) . . . 46(7) . . . 40(7) . . . 43(7) . . . 44(7) . . . 47(7) . . . 43(7) . . . 45(7) . . . 44(7) . . . 50(7) . . . 52(7) . . . 42(7) . . . 53(8) . . . 46(7) . . . 52(8) . . . 49(7) . . . 54(8) . . . 53(8) . . . 33(6) . . . 47(7) . . . 34(6) . . . 52(7) . . . 29(6) . . . 53(8) . . . 52(7) . . . 34(6) . . . 35(6) . . . 39(7) . . . 31(6) . . . 46(7) . . . 33(6) . . . 45(7) . . . 32(6) . . . 36(6) . . . 46(7) . . . 35(6) . . . 42(7) . . . 47(7) . . . 37(6) . . . 46(7) . . . 45(7) . . . 43(7) . . . 52(7) . . . 40(7) . . . 41(7) . . . 42(7) . . . 30(6) . . . 50(7) . . . 45(7) . . . 39(6) . . . 35(6) . . . 34(6) . . . 36(6) . . . 45(7) . . . 48(7) . . . 37(6) . . . 37(6) . . . 41(7) . . . 36(6) . . . 35(6) . . . 59(8) . . . 46(7) . . . 36(6) . . . 40(7) . . . 49(7) . . . 32(6) . . . 33(6) . . . 37(6) . . . 42(7) . . . 43(7) . . . 43(7) . . . 33(6) . . . 45(7) . . . 32(6) . . . 42(7) . . . 43(7) . . . 45(7) . . . 48(7) . . . 50(7) . . . 51(7) . . . 49(7) . . . 53(8) . . . 29(6) . . . 42(7) . . . 41(7) . . . 51(7) . . . 35(6) . . . 40(7) . . . 36(6) . . . 42(7) . . . 37(6) . . . 35(6) . . . 35(6) . . . 48(7) . . . 51(7) . . . 34(6) . . . 46(7) . . . 34(6) . . . 34(6) . . . 42(7) . . . 38(6) . . . 25(5) . . . 44(7) . . . 42(7) . . . 41(7) . . . 33(6) . . . 37(6) . . . 45(7) . . . 31(6) . . . 38(6) . . . 33(6) . . . 34(6) . . . 38(6) . . . 33(6) . . . 42(7) . . . 39(7) . . . 34(6) . . . 47(7) . . . 38(6) . . . 42(7) . . . 38(6) . . . 45(7) . . . 42(7) . . . 36(6) . . . 42(7) . . . 53(8) . . . 41(7) . . . 48(7) . . . 26(5) . . . 36(6) . . . 42(7) . . . 42(7) . . . 34(6) . . . 37(6) . . . 28(5) . . . 31(6) . . . 36(6) . . . 41(7) . . . 34(6) . . . 37(6) . . . 39(7) . . . 41(7) . . . 44(7) . . . 43(7) . . . 37(6) . . . 40(7) . . . 36(6) . . . 47(7) . . . 45(7) . . . 49(7) . . . 47(7) . . . 34(6) . . . 38(6) . . . 36(6) . . . 33(6) . . . 32(6) . . . 44(7) . . . 46(7) . . . 30(6) . . . 49(7) . . . 36(6) . . . 36(6) . . . 31(6) . . . 39(6) . . . 33(6) . . . 35(6) . . . 27(5) . . . 51(7) . . . 42(7) . . . 37(6) . . . 44(7) . . . 44(7) . . . 34(6) . . . 44(7) . . . 39(6) . . . 32(6) . . . 33(6) . . . 40(7) . . . 33(6) . . . 37(6) . . . 39(7) . . . 50(7) . . . 35(6) . . . 38(6) . . . 39(7) . . . 35(6) . . . 35(6) . . . 30(6) . . . 42(7) . . . 43(7) . . . 46(7) . . . 44(7) . . . 45(7) . . . 30(6) . . . 39(6) . . . 53(8) . . . 40(7) . . . 43(7) . . . 32(6) . . . 35(6) . . . 28(5) . . . 52(7) . . . 42(7) . . . 43(7) . . . 46(7) . . . 48(7) . . . 45(7) . . . 31(6) . . . 37(6) . . . 41(7) . . . 41(7) . . . 40(7) . . . 45(7) . . . 48(7) . . . 37(6) . . . 49(7) . . . 30(6) . . . 37(6) . . . 37(6) . . . 41(7) . . . 47(7) . . . 41(7) . . . 29(6) . . . 39(6) . . . 31(6) . . . 34(6) . . . 34(6) . . . 43(7) . . . 56(8) . . . 39(7) . . . 35(6) . . . 39(6) . . . 37(6) . . . 37(6) . . . 42(7) . . . 40(7) . . . 48(7) . . . 39(6) . . . 41(7) . . . 44(7) . . . 50(7) . . . 32(6) . . . 45(7) . . . 39(6) . . . 38(6) . . . 46(7) . . . 40(7) . . . 38(6) . . . 46(7) . . . 33(6) . . . 44(7) . . . 39(6) . . . 38(6) . . . _pd_meas_number_of_points 24200 _pd_proc_number_of_points 24200 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_observed_status _refln_F_squared_meas _refln_F_squared_calc _refln_phase_calc _refln_d_spacing _gsas_i100_meas 2 2 0 o 147824.98 143715.84 0.00 6.98158 100.00 1 1 1 o 15076.562 15171.002 119.42 5.88914 5.84 0 4 0 o 6147.515 147.144 0.00 4.98606 1.06 4 0 0 o 6634.933 158.749 180.00 4.88883 1.10 1 3 1 o 18584.018 19736.279 98.42 4.52006 5.81 3 1 1 o 17841.588 17868.410 -11.87 4.48321 5.53 2 4 0 o 209.678 163.098 -180.00 4.44186 0.06 4 2 0 o 7521.589 4826.342 0.00 4.38969 2.02 3 3 1 o 11139.187 9122.952 150.14 3.78328 2.86 4 4 0 o 51844.07 43937.05 0.00 3.49079 8.87 1 5 1 o 5240.696 4042.737 -44.71 3.34882 1.15 5 1 1 o 13596.782 11412.930 -41.17 3.30421 2.94 2 6 0 o 22191.313 23435.711 180.00 3.14715 3.10 6 2 0 o 40997.83 36285.37 180.00 3.09796 5.55 0 2 2 o 54621.89 48953.04 2.00 3.08792 2.76 2 0 2 o 25151.889 21785.607 -13.52 3.08199 1.27 3 5 1 o 174193.44 187525.45 69.39 3.01389 33.21 5 3 1 o 166491.09 168081.67 25.84 2.99201 31.42 2 2 2 o 104600.65 99969.87 -93.14 2.94457 10.30 4 6 0 o 5977.997 107.135 -180.00 2.74883 0.64 6 4 0 o 220.500 0.949 0.00 2.72809 0.02 2 4 2 o 11841.171 10410.286 -87.89 2.62160 1.08 4 2 2 o 24971.352 25404.609 60.25 2.61075 2.27 1 7 1 o 32834.738 39395.48 17.28 2.58626 5.00 5 5 1 o 7938.131 7942.529 132.97 2.56554 1.19 7 1 1 o 36948.70 33055.063 75.59 2.54532 5.49 0 8 0 o 35202.29 31851.291 180.00 2.49303 1.56 8 0 0 o 36300.09 24131.766 180.00 2.44441 1.55 3 7 1 o 8172.720 6762.253 6.11 2.42233 1.13 2 8 0 o 1462.910 1282.926 0.00 2.41574 0.12 7 3 1 o 15404.125 12163.629 -113.12 2.39412 2.08 8 2 0 o 3467.005 3635.484 -180.00 2.37413 0.28 4 4 2 o 904.904 971.917 -129.72 2.37771 0.08 6 6 0 o 4218.035 2522.435 180.00 2.32719 0.33 0 6 2 o 24130.434 20122.891 -53.06 2.32293 1.00 6 0 2 o 23689.990 24557.910 86.68 2.30048 0.97 2 6 2 o 10118.190 6719.252 116.04 2.26003 0.82 4 8 0 o 846.861 283.912 0.00 2.22093 0.06 6 2 2 o 14870.010 11931.153 50.68 2.24160 1.19 8 4 0 o 3484.854 1969.325 0.00 2.19484 0.24 5 7 1 o 22452.971 21652.541 80.92 2.17050 2.60 7 5 1 o 19923.615 19934.289 -3.20 2.15822 2.29 1 1 3 o 1039.429 629.752 -19.80 2.13946 0.05 4 6 2 o 1541.612 553.884 159.05 2.09813 0.12 6 4 2 o 322.228 181.120 147.47 2.08886 0.02 1 9 1 o 8472.378 5194.140 18.58 2.08536 0.92 9 1 1 o 3908.346 3289.195 -94.34 2.04966 0.41 1 3 3 o 21029.445 17404.711 48.33 2.04730 0.97 3 1 3 o 16713.793 11630.381 -157.04 2.04384 0.77 3 9 1 o 4737.406 4479.271 -62.57 1.99652 0.48 6 8 0 o 5527.286 5144.044 0.00 1.98016 0.32 8 6 0 o 7965.310 7457.291 -180.00 1.96927 0.45 9 3 1 o 5695.863 5351.043 149.63 1.96820 0.57 2 10 0 o 10179.601 12366.169 180.00 1.95418 0.57 3 3 3 o 31464.408 29241.537 45.64 1.96305 1.43 2 8 2 o 9072.557 9816.760 -24.24 1.93828 0.63 10 2 0 o 10744.434 11776.999 180.00 1.91898 0.58 7 7 1 o 6002.184 7412.235 131.74 1.90684 0.57 8 2 2 o 11064.707 11283.231 16.76 1.91659 0.76 1 5 3 o 4859.449 3367.476 57.03 1.89387 0.22 6 6 2 o 310.837 227.008 -134.97 1.89164 0.02 5 1 3 o 4118.270 3711.930 53.98 1.88569 0.18 4 10 0 o 205.353 265.595 -180.00 1.84667 0.01 5 9 1 o 1827.112 2021.046 -91.22 1.84833 0.16 9 5 1 o 5104.550 6016.014 12.13 1.83073 0.45 10 4 0 o 2372.286 2081.779 0.00 1.82052 0.12 4 8 2 o 6092.582 7123.881 160.10 1.83323 0.40 8 4 2 o 3680.318 3106.475 61.79 1.81848 0.24 3 5 3 o 21044.836 19786.803 78.09 1.82658 0.92 5 3 3 o 42609.89 37739.99 -162.88 1.82168 1.86 8 8 0 o 146695.42 141454.31 0.00 1.74540 6.68 1 11 1 o 5900.670 6576.185 -105.86 1.73942 0.48 11 1 1 o 7037.850 7436.231 -167.98 1.70839 0.56 6 10 0 o 89137.48 95615.16 0.00 1.70118 3.87 1 7 3 o 2338.734 2701.320 101.07 1.71716 0.10 5 5 3 o 73290.89 68605.13 43.85 1.71105 3.08 0 10 2 o 40460.88 45104.70 52.11 1.69952 1.21 7 1 3 o 814.268 938.730 150.51 1.70501 0.03 3 11 1 o 8463.935 8540.962 -92.11 1.68686 0.66 10 6 0 o 93375.95 92193.37 0.00 1.68549 3.99 6 8 2 o 8509.824 9413.587 -71.70 1.69066 0.51 7 9 1 o 10157.913 9662.092 128.07 1.67725 0.78 8 6 2 o 19021.170 18872.113 58.24 1.68387 1.13 9 7 1 o 12956.155 11015.002 -58.43 1.66967 0.99 10 0 2 o 56883.02 55489.04 -54.72 1.67526 1.68 2 10 2 o 28852.332 28222.398 105.94 1.67441 1.70 0 12 0 o 16219.865 15062.979 0.00 1.66202 0.34 11 3 1 o 7110.373 6567.797 14.45 1.66035 0.54 3 7 3 o 11231.439 9942.574 51.27 1.66653 0.46 10 2 2 o 30008.205 25823.826 70.75 1.65211 1.74 7 3 3 o 5299.035 4821.264 77.55 1.65725 0.22 2 12 0 o 6966.810 6060.398 -180.00 1.63852 0.28 12 0 0 o 14801.587 13082.295 0.00 1.62961 0.30 12 2 0 o 7889.862 7159.831 0.00 1.60828 0.31 0 0 4 o 150558.03 122573.95 176.77 1.62377 1.05 4 10 2 o 11109.710 11056.635 6.21 1.60528 0.62 5 11 1 o 9063.820 11478.914 -159.35 1.59460 0.64 4 12 0 o 5350.997 4257.569 0.00 1.57357 0.20 10 4 2 o 9518.045 7942.101 -2.59 1.58802 0.53 11 5 1 o 15558.813 13379.152 -119.71 1.57530 1.08 5 7 3 o 28856.664 24742.930 10.96 1.57740 1.15 2 2 4 o 4582.641 4377.960 -165.08 1.58156 0.13 7 5 3 o 24419.627 18506.803 -107.47 1.57266 0.97 12 4 0 o 8408.063 8001.609 0.00 1.54898 0.31 8 10 0 o 16175.942 14110.104 0.00 1.54532 0.59 10 8 0 o 25564.604 19633.592 -180.00 1.53865 0.93 8 8 2 o 33123.492 24818.258 95.63 1.53742 1.77 1 9 3 o 166.693 139.401 -143.20 1.54379 0.01 0 4 4 o 23912.982 19996.789 -31.70 1.54396 0.33 4 0 4 o 32515.467 26590.736 19.60 1.54100 0.45 9 1 3 o 3482.555 2358.793 134.41 1.52914 0.14 2 4 4 o 134.649 64.574 113.07 1.52507 0.00 4 2 4 o 1305.496 568.257 -65.91 1.52292 0.04 9 9 1 o 784.425 559.809 122.58 1.50901 0.05 6 10 2 o 16881.482 11825.116 82.47 1.50694 0.88 3 9 3 o 14791.017 10427.128 -24.66 1.50669 0.57 10 6 2 o 20047.318 14027.707 91.00 1.49601 1.04 1 13 1 o 4056.619 3573.736 -124.13 1.48875 0.26 9 3 3 o 16218.141 12588.476 -48.73 1.49440 0.62 7 11 1 o 5359.797 5141.010 -38.76 1.48082 0.34 6 12 0 o 2335.006 2207.032 0.00 1.48062 0.08 11 7 1 o 4497.174 4663.291 -54.24 1.46915 0.28 12 6 0 o 1088.980 1065.577 -180.00 1.46323 0.04 13 1 1 o 4853.833 5046.338 9.37 1.46153 0.30 4 4 4 o 6340.619 5545.566 142.27 1.47228 0.17 2 12 2 o 19096.605 18604.424 34.80 1.46287 0.96 3 13 1 o 20184.094 21335.277 -101.88 1.45539 1.24 7 7 3 o 31262.945 34132.344 47.39 1.46701 1.18 12 2 2 o 16640.119 15027.377 -42.37 1.44123 0.83 5 9 3 o 7107.610 6139.723 -18.59 1.43986 0.27 13 3 1 o 21578.100 19504.928 -173.79 1.43111 1.30 2 6 4 o 27088.271 25012.182 -15.37 1.44302 0.73 6 2 4 o 35679.55 30850.848 15.26 1.43819 0.96 9 5 3 o 8530.479 7866.587 123.14 1.43149 0.32 2 14 0 o 13169.462 12354.043 0.00 1.40970 0.41 4 12 2 o 36928.01 38998.67 88.06 1.41609 1.80 10 10 0 o 2139.201 2074.052 0.00 1.39632 0.07 5 13 1 o 20811.410 19452.447 -16.82 1.39490 1.20 12 4 2 o 29582.219 29597.527 83.09 1.39809 1.42 14 2 0 o 7767.124 8497.379 0.00 1.38330 0.24 8 10 2 o 12444.377 11674.183 -53.60 1.39539 0.60 4 6 4 o 4799.433 4859.459 -168.99 1.39807 0.13 10 8 2 o 16497.533 14341.783 51.38 1.39048 0.79 6 4 4 o 13010.830 12087.680 -22.66 1.39532 0.35 1 11 3 o 7970.039 7768.018 -51.52 1.38655 0.29 8 12 0 o 8850.665 8453.941 0.00 1.37442 0.27 13 5 1 o 20706.496 19300.787 -86.89 1.37557 1.17 4 14 0 o 12528.664 11983.100 -180.00 1.36770 0.38 12 8 0 o 5177.686 6009.428 0.00 1.36405 0.15 11 1 3 o 13244.043 11319.715 -12.05 1.37068 0.48 9 11 1 o 18086.551 18070.729 83.28 1.36119 1.01 11 9 1 o 22848.350 22893.777 1.84 1.35612 1.27 3 11 3 o 9472.604 9491.566 -73.63 1.35948 0.34 14 4 0 o 23948.434 21465.027 0.00 1.34503 0.70 0 8 4 o 86296.45 83267.23 3.72 1.36062 1.14 7 9 3 o 10011.093 9877.211 -11.87 1.35444 0.36 6 12 2 o 9717.718 8637.257 -50.43 1.34721 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