data_agaite 
 
_audit_creation_method            SHELXL-97 
_chemical_name_systematic 
; 
 ? 
; 
_chemical_name_common             ? 
_chemical_melting_point           ? 
_chemical_formula_moiety          ? 
_chemical_formula_sum 
 'C H2 Cu O10 Pb3 Te' 
_chemical_formula_weight          986.74 
 
loop_ 
 _atom_type_symbol 
 _atom_type_description 
 _atom_type_scat_dispersion_real 
 _atom_type_scat_dispersion_imag 
 _atom_type_scat_source 
 'Pb'  'Pb'  -3.3944  10.1111 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'Te'  'Te'  -0.5308   1.6751 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'Cu'  'Cu'   0.3201   1.2651 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'O'  'O'   0.0106   0.0060 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'C'  'C'   0.0033   0.0016 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'H'  'H'   0.0000   0.0000 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 
_symmetry_cell_setting            ? 
_symmetry_space_group_name_H-M    Pca21 
 
loop_ 
 _symmetry_equiv_pos_as_xyz 
 'x, y, z' 
 '-x+1/2, y, z+1/2' 
 'x+1/2, -y, z' 
 '-x, -y, z+1/2' 
 
_cell_length_a                    10.6522(7) 
_cell_length_b                    9.1630(5) 
_cell_length_c                    9.6011(7) 
_cell_angle_alpha                 90.00 
_cell_angle_beta                  90.00 
_cell_angle_gamma                 90.00 
_cell_volume                      937.12(11) 
_cell_formula_units_Z             4 
_cell_measurement_temperature     293(2) 
_cell_measurement_reflns_used     ? 
_cell_measurement_theta_min       ? 
_cell_measurement_theta_max       ? 
 
_exptl_crystal_description        ? 
_exptl_crystal_colour             ? 
_exptl_crystal_size_max           0.07 
_exptl_crystal_size_mid           0.04 
_exptl_crystal_size_min           0.01 
_exptl_crystal_density_meas       ? 
_exptl_crystal_density_diffrn     6.994 
_exptl_crystal_density_method     'not measured' 
_exptl_crystal_F_000              1660 
_exptl_absorpt_coefficient_mu     59.065 
_exptl_absorpt_correction_type    ? 
_exptl_absorpt_correction_T_min   0.1040 
_exptl_absorpt_correction_T_max   0.5896 
_exptl_absorpt_process_details    ? 
 
_exptl_special_details 
; 
 ? 
; 
 
_diffrn_ambient_temperature       293(2) 
_diffrn_radiation_wavelength      0.71075 
_diffrn_radiation_type            MoK\a 
_diffrn_radiation_source          'fine-focus sealed tube' 
_diffrn_radiation_monochromator   graphite 
_diffrn_measurement_device_type   ? 
_diffrn_measurement_method        ? 
_diffrn_detector_area_resol_mean  ? 
_diffrn_standards_number          ? 
_diffrn_standards_interval_count  ? 
_diffrn_standards_interval_time   ? 
_diffrn_standards_decay_%         ? 
_diffrn_reflns_number             8887 
_diffrn_reflns_av_R_equivalents   0.0667 
_diffrn_reflns_av_sigmaI/netI     0.0724 
_diffrn_reflns_limit_h_min        -13 
_diffrn_reflns_limit_h_max        13 
_diffrn_reflns_limit_k_min        -11 
_diffrn_reflns_limit_k_max        11 
_diffrn_reflns_limit_l_min        -12 
_diffrn_reflns_limit_l_max        12 
_diffrn_reflns_theta_min          3.62 
_diffrn_reflns_theta_max          27.45 
_reflns_number_total              2143 
_reflns_number_gt                 1913 
_reflns_threshold_expression      >2sigma(I) 
 
_computing_data_collection        ? 
_computing_cell_refinement        ? 
_computing_data_reduction         ? 
_computing_structure_solution     'SHELXS-97 (Sheldrick, 1990)' 
_computing_structure_refinement   'SHELXL-97 (Sheldrick, 1997)' 
_computing_molecular_graphics     ? 
_computing_publication_material   ? 
 
_refine_special_details 
; 
 Refinement of F^2^ against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F^2^, conventional R-factors R are based 
 on F, with F set to zero for negative F^2^. The threshold expression of 
 F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F^2^ are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
; 
 
_refine_ls_structure_factor_coef  Fsqd  
_refine_ls_matrix_type            full 
_refine_ls_weighting_scheme       calc  
_refine_ls_weighting_details 
 'calc w=1/[\s^2^(Fo^2^)+(0.0000P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' 
_atom_sites_solution_primary      direct 
_atom_sites_solution_secondary    difmap 
_atom_sites_solution_hydrogens    geom 
_refine_ls_hydrogen_treatment     mixed 
_refine_ls_extinction_method      SHELXL 
_refine_ls_extinction_coef        0.00000(5) 
_refine_ls_extinction_expression 
 'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^' 
_refine_ls_abs_structure_details 
 'Flack H D (1983), Acta Cryst. A39, 876-881' 
_refine_ls_abs_structure_Flack    0.007(8) 
_refine_ls_number_reflns          2143 
_refine_ls_number_parameters      146 
_refine_ls_number_restraints      1 
_refine_ls_R_factor_all           0.0387 
_refine_ls_R_factor_gt            0.0328 
_refine_ls_wR_factor_ref          0.0608 
_refine_ls_wR_factor_gt           0.0584 
_refine_ls_goodness_of_fit_ref    0.966 
_refine_ls_restrained_S_all       0.965 
_refine_ls_shift/su_max           6.290 
_refine_ls_shift/su_mean          0.043 
 
loop_ 
 _atom_site_label 
 _atom_site_type_symbol 
 _atom_site_fract_x 
 _atom_site_fract_y 
 _atom_site_fract_z 
 _atom_site_U_iso_or_equiv 
 _atom_site_adp_type 
 _atom_site_occupancy 
 _atom_site_symmetry_multiplicity 
 _atom_site_calc_flag 
 _atom_site_refinement_flags 
 _atom_site_disorder_assembly 
 _atom_site_disorder_group 
Pb1 Pb 0.38350(4) 0.73371(6) 0.57261(5) 0.01575(13) Uani 1 1 d . . . 
Pb2 Pb 0.80327(4) 0.71021(6) 0.56008(7) 0.01820(14) Uani 1 1 d . . . 
Pb3 Pb 0.61180(5) 0.03814(7) 0.42405(7) 0.02222(16) Uani 1 1 d . . . 
Te Te 0.37010(7) 0.52602(11) 0.26536(10) 0.0103(2) Uani 1 1 d . . . 
Cu Cu 0.60759(14) 0.4391(2) 0.40337(18) 0.0128(4) Uani 1 1 d . . . 
C C 0.3597(13) 0.0182(16) 0.285(2) 0.022(4) Uani 1 1 d . . . 
O1 O 0.3605(8) 0.0268(11) 0.4147(12) 0.027(3) Uani 1 1 d . . . 
O2 O 0.2545(10) 0.0212(11) 0.2157(12) 0.028(3) Uani 1 1 d . . . 
O3 O 0.4655(9) 0.0042(13) 0.2140(13) 0.033(3) Uani 1 1 d . . . 
O4 O 0.2538(10) 0.6677(9) 0.3293(11) 0.014(2) Uani 1 1 d . . . 
O5 O 0.2579(10) 0.3716(10) 0.3093(12) 0.019(2) Uani 1 1 d . . . 
O6 O 0.6933(7) 0.4803(9) 0.5782(11) 0.015(2) Uani 1 1 d . . . 
O7 O 0.5136(8) 0.4012(10) 0.2338(9) 0.0121(19) Uani 1 1 d . . . 
O8 O 0.4461(8) 0.5275(10) 0.4492(10) 0.016(2) Uani 1 1 d . . . 
OH9 O 0.4810(8) 0.6911(11) 0.2088(9) 0.020(2) Uani 1 1 d . . . 
OH10 O 0.5938(7) 0.8010(12) 0.4712(10) 0.020(2) Uani 1 1 d . . . 
 
loop_ 
 _atom_site_aniso_label 
 _atom_site_aniso_U_11 
 _atom_site_aniso_U_22 
 _atom_site_aniso_U_33 
 _atom_site_aniso_U_23 
 _atom_site_aniso_U_13 
 _atom_site_aniso_U_12 
Pb1 0.0170(2) 0.0174(3) 0.0129(3) 0.0008(3) -0.0011(3) 0.00409(18) 
Pb2 0.0148(2) 0.0210(3) 0.0188(2) 0.0014(3) 0.0004(3) -0.0020(2) 
Pb3 0.0201(3) 0.0174(3) 0.0292(4) -0.0003(3) 0.0005(3) -0.0006(2) 
Te 0.0089(4) 0.0150(5) 0.0071(4) -0.0001(4) -0.0003(3) 0.0009(4) 
Cu 0.0105(7) 0.0187(10) 0.0093(9) -0.0010(8) -0.0004(6) 0.0020(7) 
C 0.013(7) 0.015(8) 0.036(11) -0.008(7) -0.002(7) 0.002(6) 
O1 0.020(5) 0.039(7) 0.022(6) -0.001(5) 0.011(5) 0.004(5) 
O2 0.022(5) 0.030(7) 0.032(7) 0.010(5) -0.008(5) -0.009(5) 
O3 0.023(6) 0.046(8) 0.029(7) 0.006(5) 0.005(5) 0.018(6) 
O4 0.011(4) 0.015(5) 0.016(5) -0.005(5) -0.004(4) -0.004(5) 
O5 0.020(4) 0.030(6) 0.009(4) 0.005(5) 0.002(3) -0.013(6) 
O6 0.008(4) 0.028(5) 0.008(5) -0.002(5) 0.006(4) 0.000(4) 
O7 0.015(4) 0.011(5) 0.011(5) 0.001(4) 0.000(4) 0.003(4) 
O8 0.013(4) 0.023(6) 0.011(5) 0.000(4) 0.000(4) -0.001(4) 
OH9 0.013(5) 0.029(7) 0.018(5) 0.003(5) 0.014(4) -0.005(4) 
OH10 0.007(4) 0.028(6) 0.025(6) -0.005(5) -0.001(4) -0.005(4) 
 
_geom_special_details 
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
; 
 
loop_ 
 _geom_bond_atom_site_label_1 
 _geom_bond_atom_site_label_2 
 _geom_bond_distance 
 _geom_bond_site_symmetry_2 
 _geom_bond_publ_flag 
Pb1 O7 2.264(8) 4_665 ? 
Pb1 O8 2.327(9) . ? 
Pb1 OH10 2.519(9) . ? 
Pb1 O4 2.780(10) . ? 
Pb1 O6 2.820(8) 3_465 ? 
Pb1 O4 2.929(10) 2 ? 
Pb1 O1 3.094(11) 1_565 ? 
Pb1 O3 3.193(12) 4_665 ? 
Pb1 O2 3.315(11) 2_565 ? 
Pb1 OH9 3.665(9) . ? 
Pb2 O6 2.417(8) . ? 
Pb2 OH10 2.530(9) . ? 
Pb2 O5 2.567(11) 3_565 ? 
Pb2 O5 2.591(11) 4_665 ? 
Pb2 OH9 2.711(8) 2_655 ? 
Pb2 O1 2.851(11) 3_565 ? 
Pb2 O8 2.862(9) 3_565 ? 
Pb2 O2 2.945(10) 4_665 ? 
Pb2 O7 3.821(9) 2_655 ? 
Pb3 OH10 2.228(11) 1_545 ? 
Pb3 O3 2.568(12) . ? 
Pb3 O2 2.570(11) 3 ? 
Pb3 O1 2.680(9) . ? 
Pb3 O1 2.717(9) 3 ? 
Pb3 O3 2.929(13) 4_655 ? 
Pb3 O2 3.188(12) 4_655 ? 
Pb3 O4 3.222(9) 3_565 ? 
Pb3 OH9 3.822(10) 4_665 ? 
Te O4 1.896(10) . ? 
Te O5 1.900(10) . ? 
Te O6 1.921(10) 4_664 ? 
Te O7 1.933(8) . ? 
Te O8 1.942(9) . ? 
Te OH9 1.994(9) . ? 
Cu O7 1.942(9) . ? 
Cu O6 1.948(10) . ? 
Cu O8 1.952(9) . ? 
Cu O4 1.972(10) 3_565 ? 
Cu O5 2.527(11) 3_565 ? 
C O1 1.25(2) . ? 
C O2 1.304(18) . ? 
C O3 1.323(18) . ? 
O1 Pb3 2.717(9) 3_455 ? 
O1 Pb2 2.851(10) 3_465 ? 
O1 Pb1 3.094(11) 1_545 ? 
O2 Pb3 2.570(11) 3_455 ? 
O2 Pb2 2.944(10) 4_664 ? 
O2 Pb3 3.188(12) 4_654 ? 
O2 Pb1 3.315(11) 2_544 ? 
O2 Pb2 4.154(11) 3_465 ? 
O3 Pb3 2.929(13) 4_654 ? 
O3 Pb1 3.193(12) 4_664 ? 
O3 Pb2 3.938(10) 2_644 ? 
O3 Pb2 4.150(10) 4_664 ? 
O4 Cu 1.972(10) 3_465 ? 
O4 Pb1 2.929(10) 2_554 ? 
O4 Pb3 3.222(9) 3_465 ? 
O4 Pb2 4.144(9) 3_465 ? 
O5 Cu 2.527(11) 3_465 ? 
O5 Pb2 2.567(11) 3_465 ? 
O5 Pb2 2.591(11) 4_664 ? 
O6 Te 1.921(10) 4_665 ? 
O6 Pb1 2.820(8) 3_565 ? 
O6 Cu 3.793(10) 2_655 ? 
O7 Pb1 2.264(8) 4_664 ? 
O7 Cu 3.725(9) 4_664 ? 
O7 Pb2 3.821(9) 2_654 ? 
O7 Pb2 3.901(9) 4_664 ? 
O7 Pb2 3.985(9) 3_465 ? 
O8 Pb2 2.862(9) 3_465 ? 
O8 Cu 3.645(8) 3_465 ? 
OH9 Pb2 2.711(8) 2_654 ? 
OH9 O3 2.875(15) 1_565 ? 
OH9 Cu 3.303(9) 4_664 ? 
OH9 Pb3 3.822(10) 4_664 ? 
OH9 Pb3 4.041(10) 1_565 ? 
OH9 Pb1 4.115(9) 2_554 ? 
OH10 Pb3 2.228(11) 1_565 ? 
OH10 O5 2.823(14) 3_565 ? 
 
loop_ 
 _geom_angle_atom_site_label_1 
 _geom_angle_atom_site_label_2 
 _geom_angle_atom_site_label_3 
 _geom_angle 
 _geom_angle_site_symmetry_1 
 _geom_angle_site_symmetry_3 
 _geom_angle_publ_flag 
O7 Pb1 O8 76.5(3) 4_665 . ? 
O7 Pb1 OH10 88.1(3) 4_665 . ? 
O8 Pb1 OH10 75.3(3) . . ? 
O7 Pb1 O4 134.1(3) 4_665 . ? 
O8 Pb1 O4 62.5(3) . . ? 
OH10 Pb1 O4 99.8(3) . . ? 
O7 Pb1 O6 87.4(3) 4_665 3_465 ? 
O8 Pb1 O6 69.6(3) . 3_465 ? 
OH10 Pb1 O6 144.7(3) . 3_465 ? 
O4 Pb1 O6 60.5(3) . 3_465 ? 
O7 Pb1 O4 63.5(3) 4_665 2 ? 
O8 Pb1 O4 113.8(3) . 2 ? 
OH10 Pb1 O4 145.1(3) . 2 ? 
O4 Pb1 O4 114.45(12) . 2 ? 
O6 Pb1 O4 58.8(3) 3_465 2 ? 
O7 Pb1 O1 147.9(3) 4_665 1_565 ? 
O8 Pb1 O1 118.6(3) . 1_565 ? 
OH10 Pb1 O1 70.6(3) . 1_565 ? 
O4 Pb1 O1 74.8(3) . 1_565 ? 
O6 Pb1 O1 123.8(3) 3_465 1_565 ? 
O4 Pb1 O1 123.5(3) 2 1_565 ? 
O7 Pb1 O3 82.9(3) 4_665 4_665 ? 
O8 Pb1 O3 133.0(3) . 4_665 ? 
OH10 Pb1 O3 62.1(3) . 4_665 ? 
O4 Pb1 O3 140.5(3) . 4_665 ? 
O6 Pb1 O3 151.3(3) 3_465 4_665 ? 
O4 Pb1 O3 92.8(3) 2 4_665 ? 
O1 Pb1 O3 66.1(3) 1_565 4_665 ? 
O7 Pb1 O2 111.4(3) 4_665 2_565 ? 
O8 Pb1 O2 169.4(3) . 2_565 ? 
OH10 Pb1 O2 111.1(3) . 2_565 ? 
O4 Pb1 O2 107.5(3) . 2_565 ? 
O6 Pb1 O2 103.1(2) 3_465 2_565 ? 
O4 Pb1 O2 66.0(2) 2 2_565 ? 
O1 Pb1 O2 58.5(3) 1_565 2_565 ? 
O3 Pb1 O2 56.6(3) 4_665 2_565 ? 
O7 Pb1 Te 107.3(2) 4_665 . ? 
O8 Pb1 Te 31.2(2) . . ? 
OH10 Pb1 Te 81.0(2) . . ? 
O4 Pb1 Te 32.5(2) . . ? 
O6 Pb1 Te 67.1(2) 3_465 . ? 
O4 Pb1 Te 125.05(18) 2 . ? 
O1 Pb1 Te 93.2(2) 1_565 . ? 
O3 Pb1 Te 141.7(2) 4_665 . ? 
O2 Pb1 Te 139.5(2) 2_565 . ? 
O7 Pb1 Cu 29.8(2) 4_665 4_665 ? 
O8 Pb1 Cu 94.9(2) . 4_665 ? 
OH10 Pb1 Cu 115.5(2) . 4_665 ? 
O4 Pb1 Cu 131.9(2) . 4_665 ? 
O6 Pb1 Cu 72.1(2) 3_465 4_665 ? 
O4 Pb1 Cu 33.7(2) 2 4_665 ? 
O1 Pb1 Cu 145.9(2) 1_565 4_665 ? 
O3 Pb1 Cu 86.7(2) 4_665 4_665 ? 
O2 Pb1 Cu 89.74(19) 2_565 4_665 ? 
Te Pb1 Cu 120.71(4) . 4_665 ? 
O7 Pb1 OH9 117.1(3) 4_665 . ? 
O8 Pb1 OH9 49.2(3) . . ? 
OH10 Pb1 OH9 53.5(3) . . ? 
O4 Pb1 OH9 46.9(3) . . ? 
O6 Pb1 OH9 98.5(3) 3_465 . ? 
O4 Pb1 OH9 157.1(2) 2 . ? 
O1 Pb1 OH9 69.4(3) 1_565 . ? 
O3 Pb1 OH9 110.0(3) 4_665 . ? 
O2 Pb1 OH9 127.3(2) 2_565 . ? 
Te Pb1 OH9 32.17(15) . . ? 
Cu Pb1 OH9 142.89(16) 4_665 . ? 
O7 Pb1 Cu 116.7(2) 4_665 3_465 ? 
O8 Pb1 Cu 70.0(2) . 3_465 ? 
OH10 Pb1 Cu 129.7(2) . 3_465 ? 
O4 Pb1 Cu 31.4(2) . 3_465 ? 
O6 Pb1 Cu 31.0(2) 3_465 3_465 ? 
O4 Pb1 Cu 83.4(2) 2 3_465 ? 
O1 Pb1 Cu 95.3(2) 1_565 3_465 ? 
O3 Pb1 Cu 154.89(18) 4_665 3_465 ? 
O2 Pb1 Cu 99.7(2) 2_565 3_465 ? 
Te Pb1 Cu 50.91(3) . 3_465 ? 
Cu Pb1 Cu 102.86(4) 4_665 3_465 ? 
OH9 Pb1 Cu 76.21(14) . 3_465 ? 
O7 Pb1 Te 74.7(2) 4_665 2 ? 
O8 Pb1 Te 92.6(2) . 2 ? 
OH10 Pb1 Te 161.1(2) . 2 ? 
O4 Pb1 Te 86.9(2) . 2 ? 
O6 Pb1 Te 29.4(2) 3_465 2 ? 
O4 Pb1 Te 29.41(19) 2 2 ? 
O1 Pb1 Te 128.26(16) 1_565 2 ? 
O3 Pb1 Te 122.0(2) 4_665 2 ? 
O2 Pb1 Te 83.13(18) 2_565 2 ? 
Te Pb1 Te 96.26(2) . 2 ? 
Cu Pb1 Te 50.05(3) 4_665 2 ? 
OH9 Pb1 Te 127.89(15) . 2 ? 
Cu Pb1 Te 55.59(3) 3_465 2 ? 
O7 Pb1 C 154.5(3) 4_665 1_565 ? 
O8 Pb1 C 101.9(3) . 1_565 ? 
OH10 Pb1 C 67.1(3) . 1_565 ? 
O4 Pb1 C 60.4(3) . 1_565 ? 
O6 Pb1 C 116.3(3) 3_465 1_565 ? 
O4 Pb1 C 135.9(3) 2 1_565 ? 
O1 Pb1 C 17.2(3) 1_565 1_565 ? 
O3 Pb1 C 80.0(3) 4_665 1_565 ? 
O2 Pb1 C 74.1(3) 2_565 1_565 ? 
Te Pb1 C 76.1(2) . 1_565 ? 
Cu Pb1 C 163.0(2) 4_665 1_565 ? 
OH9 Pb1 C 53.2(3) . 1_565 ? 
Cu Pb1 C 85.5(2) 3_465 1_565 ? 
Te Pb1 C 130.6(2) 2 1_565 ? 
O6 Pb2 OH10 83.3(3) . . ? 
O6 Pb2 O5 73.8(3) . 3_565 ? 
OH10 Pb2 O5 67.2(3) . 3_565 ? 
O6 Pb2 O5 63.9(3) . 4_665 ? 
OH10 Pb2 O5 100.7(3) . 4_665 ? 
O5 Pb2 O5 137.3(3) 3_565 4_665 ? 
O6 Pb2 OH9 108.4(3) . 2_655 ? 
OH10 Pb2 OH9 161.2(3) . 2_655 ? 
O5 Pb2 OH9 129.4(3) 3_565 2_655 ? 
O5 Pb2 OH9 73.0(3) 4_665 2_655 ? 
O6 Pb2 O1 151.1(3) . 3_565 ? 
OH10 Pb2 O1 75.3(3) . 3_565 ? 
O5 Pb2 O1 80.1(3) 3_565 3_565 ? 
O5 Pb2 O1 138.6(3) 4_665 3_565 ? 
OH9 Pb2 O1 97.5(3) 2_655 3_565 ? 
O6 Pb2 O8 67.7(3) . 3_565 ? 
OH10 Pb2 O8 126.4(3) . 3_565 ? 
O5 Pb2 O8 61.9(3) 3_565 3_565 ? 
O5 Pb2 O8 104.9(3) 4_665 3_565 ? 
OH9 Pb2 O8 72.3(3) 2_655 3_565 ? 
O1 Pb2 O8 110.3(3) 3_565 3_565 ? 
O6 Pb2 O2 126.2(3) . 4_665 ? 
OH10 Pb2 O2 73.3(3) . 4_665 ? 
O5 Pb2 O2 132.9(3) 3_565 4_665 ? 
O5 Pb2 O2 73.8(3) 4_665 4_665 ? 
OH9 Pb2 O2 87.9(3) 2_655 4_665 ? 
O1 Pb2 O2 65.6(3) 3_565 4_665 ? 
O8 Pb2 O2 159.4(3) 3_565 4_665 ? 
O6 Pb2 Te 32.4(2) . 4_665 ? 
OH10 Pb2 Te 85.8(2) . 4_665 ? 
O5 Pb2 Te 104.5(2) 3_565 4_665 ? 
O5 Pb2 Te 32.8(2) 4_665 4_665 ? 
OH9 Pb2 Te 96.4(2) 2_655 4_665 ? 
O1 Pb2 Te 157.15(19) 3_565 4_665 ? 
O8 Pb2 Te 91.11(19) 3_565 4_665 ? 
O2 Pb2 Te 97.0(2) 4_665 4_665 ? 
O6 Pb2 Cu 30.9(2) . . ? 
OH10 Pb2 Cu 64.7(2) . . ? 
O5 Pb2 Cu 45.0(2) 3_565 . ? 
O5 Pb2 Cu 92.4(2) 4_665 . ? 
OH9 Pb2 Cu 132.1(2) 2_655 . ? 
O1 Pb2 Cu 120.4(2) 3_565 . ? 
O8 Pb2 Cu 67.95(18) 3_565 . ? 
O2 Pb2 Cu 132.3(2) 4_665 . ? 
Te Pb2 Cu 59.60(4) 4_665 . ? 
O6 Pb2 Te 68.4(2) . 3_565 ? 
OH10 Pb2 Te 96.1(2) . 3_565 ? 
O5 Pb2 Te 29.9(2) 3_565 3_565 ? 
O5 Pb2 Te 126.6(2) 4_665 3_565 ? 
OH9 Pb2 Te 101.9(2) 2_655 3_565 ? 
O1 Pb2 Te 94.6(2) 3_565 3_565 ? 
O8 Pb2 Te 32.09(19) 3_565 3_565 ? 
O2 Pb2 Te 159.1(2) 4_665 3_565 ? 
Te Pb2 Te 100.11(3) 4_665 3_565 ? 
Cu Pb2 Te 51.13(3) . 3_565 ? 
O6 Pb2 C 136.1(4) . 3_565 ? 
OH10 Pb2 C 71.3(3) . 3_565 ? 
O5 Pb2 C 63.6(4) 3_565 3_565 ? 
O5 Pb2 C 154.2(4) 4_665 3_565 ? 
OH9 Pb2 C 106.5(3) 2_655 3_565 ? 
O1 Pb2 C 16.6(4) 3_565 3_565 ? 
O8 Pb2 C 99.3(3) 3_565 3_565 ? 
O2 Pb2 C 80.4(4) 4_665 3_565 ? 
Te Pb2 C 156.8(2) 4_665 3_565 ? 
Cu Pb2 C 105.3(3) . 3_565 ? 
Te Pb2 C 79.2(3) 3_565 3_565 ? 
O6 Pb2 C 108.4(3) . 4_665 ? 
OH10 Pb2 C 64.2(3) . 4_665 ? 
O5 Pb2 C 130.6(3) 3_565 4_665 ? 
O5 Pb2 C 62.6(3) 4_665 4_665 ? 
OH9 Pb2 C 97.6(3) 2_655 4_665 ? 
O1 Pb2 C 79.6(3) 3_565 4_665 ? 
O8 Pb2 C 166.4(3) 3_565 4_665 ? 
O2 Pb2 C 18.2(3) 4_665 4_665 ? 
Te Pb2 C 80.7(2) 4_665 4_665 ? 
Cu Pb2 C 115.9(2) . 4_665 ? 
Te Pb2 C 160.2(3) 3_565 4_665 ? 
C Pb2 C 92.3(3) 3_565 4_665 ? 
O6 Pb2 O7 64.5(2) . 2_655 ? 
OH10 Pb2 O7 147.3(3) . 2_655 ? 
O5 Pb2 O7 106.8(2) 3_565 2_655 ? 
O5 Pb2 O7 60.7(3) 4_665 2_655 ? 
OH9 Pb2 O7 44.7(2) 2_655 2_655 ? 
O1 Pb2 O7 136.9(2) 3_565 2_655 ? 
O8 Pb2 O7 47.7(2) 3_565 2_655 ? 
O2 Pb2 O7 120.3(3) 4_665 2_655 ? 
Te Pb2 O7 63.93(13) 4_665 2_655 ? 
Cu Pb2 O7 88.08(13) . 2_655 ? 
Te Pb2 O7 78.37(13) 3_565 2_655 ? 
C Pb2 O7 137.0(2) 3_565 2_655 ? 
C Pb2 O7 118.7(3) 4_665 2_655 ? 
O6 Pb2 Cu 97.3(2) . 3_565 ? 
OH10 Pb2 Cu 137.1(2) . 3_565 ? 
O5 Pb2 Cu 71.7(2) 3_565 3_565 ? 
O5 Pb2 Cu 118.2(2) 4_665 3_565 ? 
OH9 Pb2 Cu 57.7(2) 2_655 3_565 ? 
O1 Pb2 Cu 85.90(19) 3_565 3_565 ? 
O8 Pb2 Cu 29.71(18) 3_565 3_565 ? 
O2 Pb2 Cu 132.5(2) 4_665 3_565 ? 
Te Pb2 Cu 116.89(4) 4_665 3_565 ? 
Cu Pb2 Cu 94.59(3) . 3_565 ? 
Te Pb2 Cu 46.75(3) 3_565 3_565 ? 
C Pb2 Cu 79.7(2) 3_565 3_565 ? 
C Pb2 Cu 149.5(2) 4_665 3_565 ? 
O7 Pb2 Cu 58.29(13) 2_655 3_565 ? 
OH10 Pb3 O3 89.4(3) 1_545 . ? 
OH10 Pb3 O2 90.2(3) 1_545 3 ? 
O3 Pb3 O2 73.9(3) . 3 ? 
OH10 Pb3 O1 83.3(3) 1_545 . ? 
O3 Pb3 O1 50.4(3) . . ? 
O2 Pb3 O1 123.8(3) 3 . ? 
OH10 Pb3 O1 82.9(3) 1_545 3 ? 
O3 Pb3 O1 122.7(3) . 3 ? 
O2 Pb3 O1 49.6(3) 3 3 ? 
O1 Pb3 O1 164.65(13) . 3 ? 
OH10 Pb3 O3 69.7(3) 1_545 4_655 ? 
O3 Pb3 O3 124.05(10) . 4_655 ? 
O2 Pb3 O3 151.4(3) 3 4_655 ? 
O1 Pb3 O3 75.3(3) . 4_655 ? 
O1 Pb3 O3 106.0(3) 3 4_655 ? 
OH10 Pb3 C 89.9(3) 1_545 3 ? 
O3 Pb3 C 99.4(4) . 3 ? 
O2 Pb3 C 25.6(4) 3 3 ? 
O1 Pb3 C 148.9(4) . 3 ? 
O1 Pb3 C 24.5(4) 3 3 ? 
O3 Pb3 C 130.3(4) 4_655 3 ? 
OH10 Pb3 C 87.4(4) 1_545 . ? 
O3 Pb3 C 26.0(4) . . ? 
O2 Pb3 C 99.8(4) 3 . ? 
O1 Pb3 C 24.5(4) . . ? 
O1 Pb3 C 147.5(4) 3 . ? 
O3 Pb3 C 99.4(4) 4_655 . ? 
C Pb3 C 125.3(6) 3 . ? 
OH10 Pb3 O2 72.2(3) 1_545 4_655 ? 
O3 Pb3 O2 160.1(3) . 4_655 ? 
O2 Pb3 O2 112.54(14) 3 4_655 ? 
O1 Pb3 O2 117.9(3) . 4_655 ? 
O1 Pb3 O2 63.6(3) 3 4_655 ? 
O3 Pb3 O2 43.0(3) 4_655 4_655 ? 
C Pb3 O2 88.2(4) 3 4_655 ? 
C Pb3 O2 141.2(4) . 4_655 ? 
OH10 Pb3 O4 156.0(3) 1_545 3_565 ? 
O3 Pb3 O4 99.5(3) . 3_565 ? 
O2 Pb3 O4 71.3(3) 3 3_565 ? 
O1 Pb3 O4 119.5(3) . 3_565 ? 
O1 Pb3 O4 73.5(3) 3 3_565 ? 
O3 Pb3 O4 120.7(3) 4_655 3_565 ? 
C Pb3 O4 66.8(3) 3 3_565 ? 
C Pb3 O4 110.2(4) . 3_565 ? 
O2 Pb3 O4 100.4(3) 4_655 3_565 ? 
OH10 Pb3 C 70.4(3) 1_545 4_655 ? 
O3 Pb3 C 144.0(3) . 4_655 ? 
O2 Pb3 C 133.2(3) 3 4_655 ? 
O1 Pb3 C 96.5(3) . 4_655 ? 
O1 Pb3 C 85.2(3) 3 4_655 ? 
O3 Pb3 C 21.3(3) 4_655 4_655 ? 
C Pb3 C 109.7(3) 3 4_655 ? 
C Pb3 C 120.4(4) . 4_655 ? 
O2 Pb3 C 21.7(3) 4_655 4_655 ? 
O4 Pb3 C 111.1(3) 3_565 4_655 ? 
OH10 Pb3 Cu 169.7(2) 1_545 . ? 
O3 Pb3 Cu 94.1(3) . . ? 
O2 Pb3 Cu 100.2(2) 3 . ? 
O1 Pb3 Cu 91.4(2) . . ? 
O1 Pb3 Cu 103.2(2) 3 . ? 
O3 Pb3 Cu 100.4(2) 4_655 . ? 
C Pb3 Cu 99.1(3) 3 . ? 
C Pb3 Cu 91.5(3) . . ? 
O2 Pb3 Cu 102.89(19) 4_655 . ? 
O4 Pb3 Cu 32.35(18) 3_565 . ? 
C Pb3 Cu 101.6(2) 4_655 . ? 
OH10 Pb3 OH9 117.8(3) 1_545 4_665 ? 
O3 Pb3 OH9 118.9(3) . 4_665 ? 
O2 Pb3 OH9 147.9(3) 3 4_665 ? 
O1 Pb3 OH9 77.9(3) . 4_665 ? 
O1 Pb3 OH9 114.7(3) 3 4_665 ? 
O3 Pb3 OH9 48.2(3) 4_655 4_665 ? 
C Pb3 OH9 131.1(4) 3 4_665 ? 
C Pb3 OH9 97.2(3) . 4_665 ? 
O2 Pb3 OH9 66.3(2) 4_655 4_665 ? 
O4 Pb3 OH9 77.3(2) 3_565 4_665 ? 
C Pb3 OH9 54.0(3) 4_655 4_665 ? 
Cu Pb3 OH9 52.21(15) . 4_665 ? 
OH10 Pb3 Pb1 121.3(2) 1_545 3_565 ? 
O3 Pb3 Pb1 144.5(3) . 3_565 ? 
O2 Pb3 Pb1 87.6(2) 3 3_565 ? 
O1 Pb3 Pb1 141.7(2) . 3_565 ? 
O1 Pb3 Pb1 52.9(2) 3 3_565 ? 
O3 Pb3 Pb1 86.0(2) 4_655 3_565 ? 
C Pb3 Pb1 66.2(3) 3 3_565 ? 
C Pb3 Pb1 150.5(3) . 3_565 ? 
O2 Pb3 Pb1 55.29(18) 4_655 3_565 ? 
O4 Pb3 Pb1 45.28(18) 3_565 3_565 ? 
C Pb3 Pb1 69.5(2) 4_655 3_565 ? 
Cu Pb3 Pb1 59.09(3) . 3_565 ? 
OH9 Pb3 Pb1 64.93(13) 4_665 3_565 ? 
OH10 Pb3 Pb2 38.5(2) 1_545 1_545 ? 
O3 Pb3 Pb2 119.5(2) . 1_545 ? 
O2 Pb3 Pb2 77.7(2) 3 1_545 ? 
O1 Pb3 Pb2 120.6(2) . 1_545 ? 
O1 Pb3 Pb2 47.6(2) 3 1_545 ? 
O3 Pb3 Pb2 74.0(2) 4_655 1_545 ? 
C Pb3 Pb2 63.4(3) 3 1_545 ? 
C Pb3 Pb2 125.1(3) . 1_545 ? 
O2 Pb3 Pb2 48.24(18) 4_655 1_545 ? 
O4 Pb3 Pb2 119.92(17) 3_565 1_545 ? 
C Pb3 Pb2 60.4(2) 4_655 1_545 ? 
Cu Pb3 Pb2 143.33(3) . 1_545 ? 
OH9 Pb3 Pb2 113.58(14) 4_665 1_545 ? 
Pb1 Pb3 Pb2 84.260(17) 3_565 1_545 ? 
O4 Te O5 91.5(5) . . ? 
O4 Te O6 95.4(4) . 4_664 ? 
O5 Te O6 87.9(4) . 4_664 ? 
O4 Te O7 166.5(4) . . ? 
O5 Te O7 95.3(4) . . ? 
O6 Te O7 96.5(4) 4_664 . ? 
O4 Te O8 88.4(4) . . ? 
O5 Te O8 93.8(4) . . ? 
O6 Te O8 175.8(4) 4_664 . ? 
O7 Te O8 79.5(4) . . ? 
O4 Te OH9 87.5(4) . . ? 
O5 Te OH9 176.3(4) . . ? 
O6 Te OH9 88.6(4) 4_664 . ? 
O7 Te OH9 86.4(4) . . ? 
O8 Te OH9 89.7(4) . . ? 
O4 Te Cu 126.6(3) . . ? 
O5 Te Cu 103.7(3) . . ? 
O6 Te Cu 135.3(2) 4_664 . ? 
O7 Te Cu 40.2(3) . . ? 
O8 Te Cu 40.5(3) . . ? 
OH9 Te Cu 79.6(3) . . ? 
O4 Te Cu 37.3(3) . 3_465 ? 
O5 Te Cu 54.3(3) . 3_465 ? 
O6 Te Cu 94.9(2) 4_664 3_465 ? 
O7 Te Cu 147.0(3) . 3_465 ? 
O8 Te Cu 89.2(3) . 3_465 ? 
OH9 Te Cu 124.8(3) . 3_465 ? 
Cu Te Cu 127.18(7) . 3_465 ? 
O4 Te Pb2 105.3(3) . 4_664 ? 
O5 Te Pb2 47.5(3) . 4_664 ? 
O6 Te Pb2 42.3(3) 4_664 4_664 ? 
O7 Te Pb2 87.9(3) . 4_664 ? 
O8 Te Pb2 138.1(3) . 4_664 ? 
OH9 Te Pb2 129.4(3) . 4_664 ? 
Cu Te Pb2 122.80(4) . 4_664 ? 
Cu Te Pb2 80.05(4) 3_465 4_664 ? 
O4 Te Cu 107.7(3) . 4_664 ? 
O5 Te Cu 109.4(3) . 4_664 ? 
O6 Te Cu 25.5(3) 4_664 4_664 ? 
O7 Te Cu 81.1(3) . 4_664 ? 
O8 Te Cu 150.9(3) . 4_664 ? 
OH9 Te Cu 67.7(3) . 4_664 ? 
Cu Te Cu 114.24(4) . 4_664 ? 
Cu Te Cu 118.35(5) 3_465 4_664 ? 
Pb2 Te Cu 61.82(4) 4_664 4_664 ? 
O4 Te Pb1 52.0(3) . . ? 
O5 Te Pb1 104.0(3) . . ? 
O6 Te Pb1 144.7(3) 4_664 . ? 
O7 Te Pb1 114.8(3) . . ? 
O8 Te Pb1 38.4(3) . . ? 
OH9 Te Pb1 78.1(3) . . ? 
Cu Te Pb1 74.67(4) . . ? 
Cu Te Pb1 67.86(4) 3_465 . ? 
Pb2 Te Pb1 146.98(3) 4_664 . ? 
Cu Te Pb1 141.43(5) 4_664 . ? 
O4 Te Pb2 91.6(3) . 3_465 ? 
O5 Te Pb2 42.3(3) . 3_465 ? 
O6 Te Pb2 129.9(3) 4_664 3_465 ? 
O7 Te Pb2 85.7(3) . 3_465 ? 
O8 Te Pb2 51.5(3) . 3_465 ? 
OH9 Te Pb2 141.3(3) . 3_465 ? 
Cu Te Pb2 70.07(4) . 3_465 ? 
Cu Te Pb2 63.47(4) 3_465 3_465 ? 
Pb2 Te Pb2 88.07(2) 4_664 3_465 ? 
Cu Te Pb2 147.31(5) 4_664 3_465 ? 
Pb1 Te Pb2 71.14(2) . 3_465 ? 
O7 Cu O6 176.9(3) . . ? 
O7 Cu O8 79.0(4) . . ? 
O6 Cu O8 98.0(4) . . ? 
O7 Cu O4 90.9(4) . 3_565 ? 
O6 Cu O4 92.1(4) . 3_565 ? 
O8 Cu O4 169.6(4) . 3_565 ? 
O7 Cu O5 98.6(4) . 3_565 ? 
O6 Cu O5 83.0(4) . 3_565 ? 
O8 Cu O5 110.7(4) . 3_565 ? 
O4 Cu O5 73.2(3) 3_565 3_565 ? 
O7 Cu Te 40.0(3) . . ? 
O6 Cu Te 137.2(2) . . ? 
O8 Cu Te 40.3(3) . . ? 
O4 Cu Te 130.3(3) 3_565 . ? 
O5 Cu Te 101.3(2) 3_565 . ? 
O1 C O2 120.9(14) . . ? 
O1 C O3 121.0(14) . . ? 
O2 C O3 118.1(17) . . ? 
O1 C Pb3 64.7(8) . 3_455 ? 
O2 C Pb3 58.3(8) . 3_455 ? 
O3 C Pb3 163.9(10) . 3_455 ? 
O1 C Pb3 63.1(8) . . ? 
O2 C Pb3 173.7(12) . . ? 
O3 C Pb3 58.3(8) . . ? 
Pb3 C Pb3 126.8(7) 3_455 . ? 
O1 C Pb3 172.8(10) . 4_654 ? 
O2 C Pb3 64.8(9) . 4_654 ? 
O3 C Pb3 53.4(9) . 4_654 ? 
Pb3 C Pb3 119.2(5) 3_455 4_654 ? 
Pb3 C Pb3 111.7(5) . 4_654 ? 
O1 C Pb2 40.7(7) . 3_465 ? 
O2 C Pb2 102.2(9) . 3_465 ? 
O3 C Pb2 125.1(10) . 3_465 ? 
Pb3 C Pb2 69.7(3) 3_455 3_465 ? 
Pb3 C Pb2 77.7(4) . 3_465 ? 
Pb3 C Pb2 145.2(5) 4_654 3_465 ? 
O1 C Pb2 122.7(9) . 4_664 ? 
O2 C Pb2 44.7(7) . 4_664 ? 
O3 C Pb2 99.4(11) . 4_664 ? 
Pb3 C Pb2 87.9(3) 3_455 4_664 ? 
Pb3 C Pb2 129.3(5) . 4_664 ? 
Pb3 C Pb2 64.3(3) 4_654 4_664 ? 
Pb2 C Pb2 83.6(3) 3_465 4_664 ? 
O1 C Pb1 47.1(8) . 1_545 ? 
O2 C Pb1 116.2(9) . 1_545 ? 
O3 C Pb1 104.5(10) . 1_545 ? 
Pb3 C Pb1 67.6(4) 3_455 1_545 ? 
Pb3 C Pb1 70.1(4) . 1_545 ? 
Pb3 C Pb1 127.5(4) 4_654 1_545 ? 
Pb2 C Pb1 87.3(4) 3_465 1_545 ? 
Pb2 C Pb1 155.4(4) 4_664 1_545 ? 
O1 C Pb1 117.2(9) . 4_664 ? 
O2 C Pb1 107.9(11) . 4_664 ? 
O3 C Pb1 39.6(7) . 4_664 ? 
Pb3 C Pb1 154.6(5) 3_455 4_664 ? 
Pb3 C Pb1 65.9(3) . 4_664 ? 
Pb3 C Pb1 62.2(3) 4_654 4_664 ? 
Pb2 C Pb1 95.2(3) 3_465 4_664 ? 
Pb2 C Pb1 69.6(3) 4_664 4_664 ? 
Pb1 C Pb1 134.1(4) 1_545 4_664 ? 
O1 C Pb1 121.8(9) . 2_544 ? 
O2 C Pb1 40.1(7) . 2_544 ? 
O3 C Pb1 102.4(10) . 2_544 ? 
Pb3 C Pb1 64.3(2) 3_455 2_544 ? 
Pb3 C Pb1 143.5(4) . 2_544 ? 
Pb3 C Pb1 58.9(2) 4_654 2_544 ? 
Pb2 C Pb1 131.8(4) 3_465 2_544 ? 
Pb2 C Pb1 81.1(3) 4_664 2_544 ? 
Pb1 C Pb1 88.2(3) 1_545 2_544 ? 
Pb1 C Pb1 120.9(5) 4_664 2_544 ? 
C O1 Pb3 92.4(8) . . ? 
C O1 Pb3 90.7(9) . 3_455 ? 
Pb3 O1 Pb3 168.9(5) . 3_455 ? 
C O1 Pb2 122.7(9) . 3_465 ? 
Pb3 O1 Pb2 99.5(3) . 3_465 ? 
Pb3 O1 Pb2 87.7(3) 3_455 3_465 ? 
C O1 Pb1 115.8(9) . 1_545 ? 
Pb3 O1 Pb1 86.5(3) . 1_545 ? 
Pb3 O1 Pb1 82.6(3) 3_455 1_545 ? 
Pb2 O1 Pb1 120.7(4) 3_465 1_545 ? 
C O2 Pb3 96.1(10) . 3_455 ? 
C O2 Pb2 117.1(9) . 4_664 ? 
Pb3 O2 Pb2 116.6(4) 3_455 4_664 ? 
C O2 Pb3 93.5(10) . 4_654 ? 
Pb3 O2 Pb3 155.7(4) 3_455 4_654 ? 
Pb2 O2 Pb3 77.9(3) 4_664 4_654 ? 
C O2 Pb1 125.2(8) . 2_544 ? 
Pb3 O2 Pb1 83.8(3) 3_455 2_544 ? 
Pb2 O2 Pb1 111.2(3) 4_664 2_544 ? 
Pb3 O2 Pb1 72.5(2) 4_654 2_544 ? 
C O2 Pb2 59.9(8) . 3_465 ? 
Pb3 O2 Pb2 65.2(2) 3_455 3_465 ? 
Pb2 O2 Pb2 86.3(3) 4_664 3_465 ? 
Pb3 O2 Pb2 138.1(3) 4_654 3_465 ? 
Pb1 O2 Pb2 148.9(3) 2_544 3_465 ? 
C O3 Pb3 95.7(11) . . ? 
C O3 Pb3 105.3(10) . 4_654 ? 
Pb3 O3 Pb3 158.9(4) . 4_654 ? 
C O3 Pb1 125.1(9) . 4_664 ? 
Pb3 O3 Pb1 86.4(3) . 4_664 ? 
Pb3 O3 Pb1 80.6(3) 4_654 4_664 ? 
C O3 Pb2 142.4(9) . 2_644 ? 
Pb3 O3 Pb2 89.9(3) . 2_644 ? 
Pb3 O3 Pb2 74.2(2) 4_654 2_644 ? 
Pb1 O3 Pb2 92.3(2) 4_664 2_644 ? 
C O3 Pb2 62.3(9) . 4_664 ? 
Pb3 O3 Pb2 128.5(4) . 4_664 ? 
Pb3 O3 Pb2 63.3(2) 4_654 4_664 ? 
Pb1 O3 Pb2 73.9(2) 4_664 4_664 ? 
Pb2 O3 Pb2 136.8(3) 2_644 4_664 ? 
Te O4 Cu 107.0(4) . 3_465 ? 
Te O4 Pb1 95.5(4) . . ? 
Cu O4 Pb1 101.4(4) 3_465 . ? 
Te O4 Pb1 101.2(4) . 2_554 ? 
Cu O4 Pb1 90.6(4) 3_465 2_554 ? 
Pb1 O4 Pb1 155.5(3) . 2_554 ? 
Te O4 Pb3 166.1(5) . 3_465 ? 
Cu O4 Pb3 86.7(3) 3_465 3_465 ? 
Pb1 O4 Pb3 79.3(2) . 3_465 ? 
Pb1 O4 Pb3 80.2(2) 2_554 3_465 ? 
Te O4 Pb2 61.2(3) . 3_465 ? 
Cu O4 Pb2 59.5(2) 3_465 3_465 ? 
Pb1 O4 Pb2 70.7(2) . 3_465 ? 
Pb1 O4 Pb2 133.3(3) 2_554 3_465 ? 
Pb3 O4 Pb2 127.4(3) 3_465 3_465 ? 
Te O5 Cu 88.1(4) . 3_465 ? 
Te O5 Pb2 107.9(5) . 3_465 ? 
Cu O5 Pb2 89.1(4) 3_465 3_465 ? 
Te O5 Pb2 99.7(4) . 4_664 ? 
Cu O5 Pb2 111.7(4) 3_465 4_664 ? 
Pb2 O5 Pb2 146.0(4) 3_465 4_664 ? 
Te O5 Cu 47.9(3) . . ? 
Cu O5 Cu 114.5(3) 3_465 . ? 
Pb2 O5 Cu 69.4(2) 3_465 . ? 
Pb2 O5 Cu 120.1(4) 4_664 . ? 
Te O6 Cu 129.5(4) 4_665 . ? 
Te O6 Pb2 105.3(4) 4_665 . ? 
Cu O6 Pb2 109.5(4) . . ? 
Te O6 Pb1 104.5(4) 4_665 3_565 ? 
Cu O6 Pb1 100.7(4) . 3_565 ? 
Pb2 O6 Pb1 104.9(3) . 3_565 ? 
Te O6 Cu 54.8(2) 4_665 2_655 ? 
Cu O6 Cu 162.2(4) . 2_655 ? 
Pb2 O6 Cu 82.8(3) . 2_655 ? 
Pb1 O6 Cu 62.92(18) 3_565 2_655 ? 
Te O6 Pb1 75.0(2) 4_665 . ? 
Cu O6 Pb1 73.5(2) . . ? 
Pb2 O6 Pb1 83.9(2) . . ? 
Pb1 O6 Pb1 170.9(3) 3_565 . ? 
Cu O6 Pb1 121.7(3) 2_655 . ? 
Te O7 Cu 99.8(4) . . ? 
Te O7 Pb1 144.4(4) . 4_664 ? 
Cu O7 Pb1 114.9(4) . 4_664 ? 
Te O7 Cu 68.1(2) . 4_664 ? 
Cu O7 Cu 145.3(4) . 4_664 ? 
Pb1 O7 Cu 78.5(2) 4_664 4_664 ? 
Te O7 Pb2 91.9(3) . 2_654 ? 
Cu O7 Pb2 88.3(3) . 2_654 ? 
Pb1 O7 Pb2 81.9(2) 4_664 2_654 ? 
Cu O7 Pb2 60.93(14) 4_664 2_654 ? 
Te O7 Pb2 62.5(2) . 4_664 ? 
Cu O7 Pb2 148.3(4) . 4_664 ? 
Pb1 O7 Pb2 89.1(3) 4_664 4_664 ? 
Cu O7 Pb2 55.86(12) 4_664 4_664 ? 
Pb2 O7 Pb2 116.7(2) 2_654 4_664 ? 
Te O7 Pb3 129.6(4) . . ? 
Cu O7 Pb3 68.0(2) . . ? 
Pb1 O7 Pb3 74.2(2) 4_664 . ? 
Cu O7 Pb3 145.0(2) 4_664 . ? 
Pb2 O7 Pb3 133.9(2) 2_654 . ? 
Pb2 O7 Pb3 102.0(2) 4_664 . ? 
Te O7 Pb2 65.4(2) . 3_465 ? 
Cu O7 Pb2 71.1(3) . 3_465 ? 
Pb1 O7 Pb2 132.0(3) 4_664 3_465 ? 
Cu O7 Pb2 125.1(2) 4_664 3_465 ? 
Pb2 O7 Pb2 145.1(2) 2_654 3_465 ? 
Pb2 O7 Pb2 77.44(16) 4_664 3_465 ? 
Pb3 O7 Pb2 64.41(14) . 3_465 ? 
Te O8 Cu 99.2(4) . . ? 
Te O8 Pb1 110.4(4) . . ? 
Cu O8 Pb1 134.8(4) . . ? 
Te O8 Pb2 96.4(3) . 3_465 ? 
Cu O8 Pb2 103.7(4) . 3_465 ? 
Pb1 O8 Pb2 106.0(3) . 3_465 ? 
Te O8 Cu 58.6(2) . 3_465 ? 
Cu O8 Cu 151.6(4) . 3_465 ? 
Pb1 O8 Cu 73.1(2) . 3_465 ? 
Pb2 O8 Cu 65.36(17) 3_465 3_465 ? 
Te OH9 Pb2 134.0(5) . 2_654 ? 
Te OH9 O3 135.9(4) . 1_565 ? 
Pb2 OH9 O3 89.6(3) 2_654 1_565 ? 
Te OH9 Cu 63.4(3) . . ? 
Pb2 OH9 Cu 89.8(3) 2_654 . ? 
O3 OH9 Cu 136.1(4) 1_565 . ? 
Te OH9 Cu 78.4(3) . 4_664 ? 
Pb2 OH9 Cu 78.3(2) 2_654 4_664 ? 
O3 OH9 Cu 111.1(4) 1_565 4_664 ? 
Cu OH9 Cu 111.8(3) . 4_664 ? 
Te OH9 Pb1 69.7(2) . . ? 
Pb2 OH9 Pb1 137.3(3) 2_654 . ? 
O3 OH9 Pb1 82.0(3) 1_565 . ? 
Cu OH9 Pb1 69.32(17) . . ? 
Cu OH9 Pb1 143.5(3) 4_664 . ? 
Te OH9 Pb3 122.3(4) . 4_664 ? 
Pb2 OH9 Pb3 78.5(2) 2_654 4_664 ? 
O3 OH9 Pb3 49.4(3) 1_565 4_664 ? 
Cu OH9 Pb3 167.5(3) . 4_664 ? 
Cu OH9 Pb3 61.67(16) 4_664 4_664 ? 
Pb1 OH9 Pb3 122.6(3) . 4_664 ? 
Te OH9 Pb3 131.4(3) . 1_565 ? 
Pb2 OH9 Pb3 85.8(2) 2_654 1_565 ? 
O3 OH9 Pb3 39.2(3) 1_565 1_565 ? 
Cu OH9 Pb3 97.0(2) . 1_565 ? 
Cu OH9 Pb3 146.8(3) 4_664 1_565 ? 
Pb1 OH9 Pb3 61.73(15) . 1_565 ? 
Pb3 OH9 Pb3 86.8(2) 4_664 1_565 ? 
Te OH9 Pb1 66.4(2) . 2_554 ? 
Pb2 OH9 Pb1 128.8(3) 2_654 2_554 ? 
O3 OH9 Pb1 81.8(3) 1_565 2_554 ? 
Cu OH9 Pb1 129.7(3) . 2_554 ? 
Cu OH9 Pb1 58.85(15) 4_664 2_554 ? 
Pb1 OH9 Pb1 91.46(18) . 2_554 ? 
Pb3 OH9 Pb1 57.80(13) 4_664 2_554 ? 
Pb3 OH9 Pb1 114.4(2) 1_565 2_554 ? 
Pb3 OH10 Pb1 113.2(4) 1_565 . ? 
Pb3 OH10 Pb2 108.2(3) 1_565 . ? 
Pb1 OH10 Pb2 125.0(4) . . ? 
Pb3 OH10 O5 112.4(4) 1_565 3_565 ? 
Pb1 OH10 O5 128.8(4) . 3_565 ? 
Pb2 OH10 O5 57.0(3) . 3_565 ? 
Pb3 OH10 Cu 156.0(4) 1_565 . ? 
Pb1 OH10 Cu 82.7(3) . . ? 
Pb2 OH10 Cu 72.8(3) . . ? 
O5 OH10 Cu 47.0(3) 3_565 . ? 
 
_diffrn_measured_fraction_theta_max    0.998 
_diffrn_reflns_theta_full              27.45 
_diffrn_measured_fraction_theta_full   0.998 
_refine_diff_density_max    2.688 
_refine_diff_density_min   -1.487 
_refine_diff_density_rms    0.422 
