data_EPIDIDYMITE_publ

_pd_block_id
  2008-07-07T21:33|EPIDIDYMITE|A|Overall

_audit_creation_method  "from EXP file using GSAS2CIF"
_audit_creation_date                   2008-07-07T21:33
_audit_author_name                     A
_audit_update_record
; 2008-07-07T21:33  Initial CIF as created by GSAS2CIF
;

#=============================================================================
# this information describes the project, paper etc. for the CIF             #
# Acta Cryst. Section C papers and editorial correspondence is generated     #
# from the information in this section                                       #
#                                                                            #
#   (from)   CIF submission form for Rietveld refinements (Acta Cryst. C)    #
#                                                 Version 14 December 1998   #
#=============================================================================
# 1. SUBMISSION DETAILS

_publ_contact_author_name            ?   # Name of author for correspondence
_publ_contact_author_address             # Address of author for correspondence
; ?
;
_publ_contact_author_email           ?
_publ_contact_author_fax             ?
_publ_contact_author_phone           ?

_publ_contact_letter
; ?
;

_publ_requested_journal              ?
_publ_requested_coeditor_name        ?
_publ_requested_category             ?   # Acta C: one of CI/CM/CO/FI/FM/FO

#==============================================================================

# 2. PROCESSING SUMMARY (IUCr Office Use Only)

_journal_data_validation_number      ?

_journal_date_recd_electronic        ?
_journal_date_to_coeditor            ?
_journal_date_from_coeditor          ?
_journal_date_accepted               ?
_journal_date_printers_first         ?
_journal_date_printers_final         ?
_journal_date_proofs_out             ?
_journal_date_proofs_in              ?
_journal_coeditor_name               ?
_journal_coeditor_code               ?
_journal_coeditor_notes
; ?
;
_journal_techeditor_code             ?
_journal_techeditor_notes
; ?
;
_journal_coden_ASTM                  ?
_journal_name_full                   ?
_journal_year                        ?
_journal_volume                      ?
_journal_issue                       ?
_journal_page_first                  ?
_journal_page_last                   ?
_journal_paper_category              ?
_journal_suppl_publ_number           ?
_journal_suppl_publ_pages            ?

#==============================================================================

# 3. TITLE AND AUTHOR LIST

_publ_section_title
; ?
;
_publ_section_title_footnote
; ?
;

# The loop structure below should contain the names and addresses of all
# authors, in the required order of publication. Repeat as necessary.

loop_
	_publ_author_name
        _publ_author_footnote
	_publ_author_address
 ?                                   #<--'Last name, first name'
; ?
;
; ?
;

#==============================================================================

# 4. TEXT

_publ_section_synopsis
;  ?
;
_publ_section_abstract
; ?
;
_publ_section_comment
; ?
;
_publ_section_exptl_prep      # Details of the preparation of the sample(s)
                              # should be given here.
; ?
;
_publ_section_exptl_refinement
; ?
;
_publ_section_references
; ?
;
_publ_section_figure_captions
; ?
;
_publ_section_acknowledgements
; ?
;

#=============================================================================
# 5. OVERALL REFINEMENT & COMPUTING DETAILS

_refine_special_details
; ?
;
_pd_proc_ls_special_details
; ?
;

# The following items are used to identify the programs used.
_computing_molecular_graphics     ?
_computing_publication_material   ?

_refine_ls_weighting_scheme       ?
_refine_ls_weighting_details      ?
_refine_ls_hydrogen_treatment     ?
_refine_ls_extinction_method      ?
_refine_ls_extinction_coef        ?
_refine_ls_number_constraints     ?

_refine_ls_restrained_S_all       ?
_refine_ls_restrained_S_obs       ?

#==============================================================================
# 6. SAMPLE PREPARATION DATA

# (In the unusual case where multiple samples are used in a single
#  Rietveld study, this information should be moved into the phase
#  blocks)

# The following three fields describe the preparation of the material.
# The cooling rate is in K/min.  The pressure at which the sample was
# prepared is in kPa.  The temperature of preparation is in K.

_pd_prep_cool_rate                ?
_pd_prep_pressure                 ?
_pd_prep_temperature              ?

_pd_char_colour                   ?       # use ICDD colour descriptions
data_EPIDIDYMITE_overall

_refine_ls_shift/su_max                0.02
_refine_ls_shift/su_mean               0.00
_computing_structure_refinement        GSAS
_refine_ls_number_parameters           151
_refine_ls_goodness_of_fit_all         1.58
_refine_ls_number_restraints           0

# Overall powder R-factors

_pd_proc_ls_prof_R_factor              0.0070
_pd_proc_ls_prof_wR_factor             0.0097
_refine_ls_matrix_type                 full

# pointers to the phase blocks
loop_   _pd_phase_block_id
      2008-07-07T21:33|EPIDIDYMITE_phase1|A||
# pointers to the diffraction patterns
loop_   _pd_block_diffractogram_id
      2008-07-07T21:33|EPIDIDYMITE_H_02|A|D20

# Information for phase 1
data_EPIDIDYMITE_phase_1

_pd_block_id
  2008-07-07T21:33|EPIDIDYMITE_phase1|A||

# Histograms for phase 1
loop_   _pd_block_diffractogram_id
  2008-07-07T21:33|EPIDIDYMITE_H_02|A|D20

#==============================================================================
# 7. CHEMICAL, STRUCTURAL AND CRYSTAL DATA

_pd_char_particle_morphology      ?

_chemical_name_systematic
; ?
;
_chemical_name_common             ?
_chemical_formula_moiety          ?
_chemical_formula_structural      ?
_chemical_formula_analytical      ?
_chemical_melting_point           ?
_chemical_compound_source         ?       # for minerals and
                                          # natural products
_symmetry_space_group_name_Hall   ?

_exptl_crystal_F_000               ?
_exptl_crystal_density_diffrn      ?
_exptl_crystal_density_meas        ?
_exptl_crystal_density_method      ?

_cell_measurement_temperature     ?

_cell_special_details
; ?
;

_geom_special_details             ?

# The following item identifies the program(s) used (if appropriate).
_computing_structure_solution     ?

#==============================================================================

# 8. Phase information from GSAS

_pd_phase_name                         Epididymite
_cell_length_a                         12.7330(5)
_cell_length_b                         13.5863(5)
_cell_length_c                         7.33729(34)
_cell_angle_alpha                      90.0
_cell_angle_beta                       90.0
_cell_angle_gamma                      90.0
_cell_volume                           1269.30(13)
_symmetry_cell_setting                 orthorhombic
_symmetry_space_group_name_H-M         "P n m a"
loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz
       1 +x,+y,+z 
       2 -x+1/2,+y+1/2,+z+1/2 
       3 +x,-y+1/2,+z 
       4 -x+1/2,-y,+z+1/2 
      -1 -x,-y,-z 
      -2 +x+1/2,-y+1/2,-z+1/2 
      -3 -x,+y+1/2,-z 
      -4 +x+1/2,+y,-z+1/2 

# ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS


loop_
      _atom_site_type_symbol
      _atom_site_label
      _atom_site_fract_x
      _atom_site_fract_y
      _atom_site_fract_z
      _atom_site_occupancy
      _atom_site_thermal_displace_type
      _atom_site_U_iso_or_equiv
      _atom_site_symmetry_multiplicity
Na
Na1     0.10222(4)   0.069642(30  0.50209(6)   1.0        Uani   0.0157        8
Be
Be1     0.49299(10) -0.00054(8)   0.34311(19)  1.0        Uani   0.00933       8
Si
Si1     0.159402(22  0.137299(20  0.02068(4)   1.0        Uani   0.00722       8
Si
Si2     0.343994(22  0.135627(20  0.73731(4)   1.0        Uani   0.00745       8
Si
Si3     0.329535(22  0.137264(19  0.31160(4)   1.0        Uani   0.00754       8
O 
O1      0.12113(8)   0.25        -0.00109(14)  1.0        Uani   0.01106       4
O 
O2      0.21386(5)   0.12363(5)   0.21914(10)  1.0        Uani   0.00945       8
O 
O3      0.06037(6)   0.06644(5)   0.00873(9)   1.0        Uani   0.00826       8
O 
O4      0.24113(5)   0.11154(5)   0.85974(10)  1.0        Uani   0.01093       8
O 
O5      0.43776(5)   0.06465(5)   0.79271(10)  1.0        Uani   0.00902       8
O 
O6      0.37806(7)   0.25         0.77137(14)  1.0        Uani   0.00988       4
O 
O7      0.30415(5)   0.12293(5)   0.52773(10)  1.0        Uani   0.0094        8
O 
O8      0.36900(7)   0.25         0.27543(14)  1.0        Uani   0.00997       4
O 
O9      0.41170(5)   0.06215(5)   0.22863(10)  1.0        Uani   0.0091        8
O 
O10     0.05559(8)   0.25         0.48603(16)  1.0        Uani   0.01626       4
H 
H1      0.5120(11)   0.25         0.1094(18)   1.0        Uiso   0.034(4)      4
H 
H2      0.5046(11)   0.25        -0.0776(20)   1.0        Uiso   0.040(4)      4


loop_ _atom_type_symbol
      _atom_type_number_in_cell
                   Na  8.0        
                   Be  8.0        
                   Si 24.0        
                   O_ 64.0        
                   H_  8.0        
 
# If you change Z, be sure to change all 3 of the following
_chemical_formula_sum                  "Be H Na O8 Si3"
_chemical_formula_weight               245.26
_cell_formula_units_Z                  8

# MOLECULAR GEOMETRY

loop_
      _geom_bond_atom_site_label_1
      _geom_bond_atom_site_label_2
      _geom_bond_distance
      _geom_bond_site_symmetry_1
      _geom_bond_site_symmetry_2
      _geom_bond_publ_flag
  Na1       Na1              3.2185(9)  .     -1_556  N
  Na1       Be1             2.9347(14)  .      4_555  N
  Na1       Be1             3.0428(14)  .     -4_455  N
  Na1       Si2              3.4671(5)  .      4_554  N
  Na1       Si3              3.3428(5)  .      1_555  N
  Na1       O2               2.6208(8)  .      1_555  N
  Na1       O5               2.4389(8)  .      4_554  N
  Na1       O5               2.5801(8)  .     -4_456  N
  Na1       O7               2.6778(8)  .      1_555  N
  Na1       O9               2.4496(8)  .      4_555  N
  Na1       O9               2.9600(9)  .     -4_455  N
  Na1       O10              2.5241(5)  .      1_555  N
  Na1       H1                2.827(7)  .     -2_455  N
  Na1       H2                2.803(7)  .     -2_455  N
  Be1       Na1             2.9347(14)  .      4_554  N
  Be1       Na1             3.0428(14)  .     -4_555  N
  Be1       Be1             2.3092(28)  .     -1_656  N
  Be1       Si2             2.8329(12)  .     -1_656  N
  Be1       Si3             2.8090(12)  .      1_555  N
  Be1       O3              1.6553(14)  .      4_555  N
  Be1       O3              1.6571(14)  .     -4_555  N
  Be1       O5              1.5904(14)  .     -1_656  N
  Be1       O9              1.5819(14)  .      1_555  N
  Si1       O1               1.6148(4)  .      1_555  N
  Si1       O2               1.6234(8)  .      1_555  N
  Si1       O3               1.5889(7)  .      1_555  N
  Si1       O4               1.6124(8)  .      1_554  N
  Si2       Na1              3.4671(5)  .      4_555  N
  Si2       Be1             2.8329(12)  .     -1_656  N
  Si2       O4               1.6216(7)  .      1_555  N
  Si2       O5               1.5876(7)  .      1_555  N
  Si2       O6               1.6326(4)  .      1_555  N
  Si2       O7               1.6285(8)  .      1_555  N
  Si3       Na1              3.3428(5)  .      1_555  N
  Si3       Be1             2.8090(12)  .      1_555  N
  Si3       O2               1.6322(7)  .      1_555  N
  Si3       O7               1.6300(8)  .      1_555  N
  Si3       O8               1.6337(4)  .      1_555  N
  Si3       O9               1.5832(7)  .      1_555  N
  O1        Si1              1.6148(4)  .      1_555  N
  O1        Si1              1.6148(4)  .      3_555  N
  O2        Na1              2.6208(8)  .      1_555  N
  O2        Si1              1.6234(8)  .      1_555  N
  O2        Si3              1.6322(7)  .      1_555  N
  O3        Be1             1.6553(14)  .      4_554  N
  O3        Be1             1.6571(14)  .     -4_455  N
  O3        Si1              1.5889(7)  .      1_555  N
  O4        Si1              1.6124(8)  .      1_556  N
  O4        Si2              1.6216(7)  .      1_555  N
  O5        Na1              2.4389(8)  .      4_555  N
  O5        Na1              2.5801(8)  .     -4_556  N
  O5        Be1             1.5904(14)  .     -1_656  N
  O5        Si2              1.5876(7)  .      1_555  N
  O6        Si2              1.6326(4)  .      1_555  N
  O6        Si2              1.6326(4)  .      3_555  N
  O6        H2               1.955(15)  .      1_556  N
  O7        Na1              2.6778(8)  .      1_555  N
  O7        Si2              1.6285(8)  .      1_555  N
  O7        Si3              1.6300(8)  .      1_555  N
  O8        Si3              1.6337(4)  .      1_555  N
  O8        Si3              1.6337(4)  .      3_555  N
  O9        Na1              2.4496(8)  .      4_554  N
  O9        Na1              2.9600(9)  .     -4_555  N
  O9        Be1             1.5819(14)  .      1_555  N
  O9        Si3              1.5832(7)  .      1_555  N
  O10       Na1              2.5241(5)  .      1_555  N
  O10       Na1              2.5241(5)  .      3_555  N
  O10       H1               0.894(14)  .     -2_455  N
  O10       H2               0.934(14)  .     -2_455  N
  H1        Na1               2.827(7)  .     -2_555  N
  H1        Na1               2.827(7)  .     -4_555  N
  H1        O10              0.894(14)  .     -2_555  N
  H1        H2               1.375(15)  .      1_555  N
  H2        Na1               2.803(7)  .     -2_555  N
  H2        Na1               2.803(7)  .     -4_555  N
  H2        O6               1.955(15)  .      1_554  N
  H2        O10              0.934(14)  .     -2_555  N
  H2        H1               1.375(15)  .      1_555  N

loop_
      _geom_angle_atom_site_label_1
      _geom_angle_atom_site_label_2
      _geom_angle_atom_site_label_3
      _geom_angle
      _geom_angle_site_symmetry_1
      _geom_angle_site_symmetry_2
      _geom_angle_site_symmetry_3
      _geom_angle_publ_flag
  Na1       Na1       Be1             59.061(27)     -1_556  .      4_555  N
  Na1       Na1       O2             126.562(27)     -1_556  .      1_555  N
  Na1       Na1       O5              52.071(22)     -1_556  .      4_554  N
  Na1       Na1       O5              48.211(19)     -1_556  .     -4_557  N
  Na1       Na1       O7             159.435(27)     -1_556  .      1_555  N
  Na1       Na1       O9              61.194(21)     -1_556  .      4_555  N
  Na1       Na1       O10            112.339(34)     -1_556  .      1_555  N
  Be1       Na1       O2             171.501(34)      4_555  .      1_555  N
  Be1       Na1       O5             102.210(33)      4_555  .      4_554  N
  Be1       Na1       O5              32.726(28)      4_555  .     -4_557  N
  Be1       Na1       O7             115.041(32)      4_555  .      1_555  N
  Be1       Na1       O9              32.616(26)      4_555  .      4_555  N
  Be1       Na1       O10              104.67(4)      4_555  .      1_555  N
  O2        Na1       O5              79.841(26)      1_555  .      4_554  N
  O2        Na1       O5             155.480(27)      1_555  .     -4_557  N
  O2        Na1       O7              57.263(23)      1_555  .      1_555  N
  O2        Na1       O9             141.385(28)      1_555  .      4_555  N
  O2        Na1       O10             79.565(32)      1_555  .      1_555  N
  O5        Na1       O5             100.282(27)      4_554  .     -4_557  N
  O5        Na1       O7             116.548(28)      4_554  .      1_555  N
  O5        Na1       O9              82.268(30)      4_554  .      4_555  N
  O5        Na1       O10              130.37(4)      4_554  .      1_555  N
  O5        Na1       O7             138.198(29)     -4_557  .      1_555  N
  O5        Na1       O9              61.712(23)     -4_557  .      4_555  N
  O5        Na1       O10             82.057(31)     -4_557  .      1_555  N
  O7        Na1       O9             102.676(26)      1_555  .      4_555  N
  O7        Na1       O10             88.090(31)      1_555  .      1_555  N
  O9        Na1       O10              136.41(4)      4_555  .      1_555  N
  Na1       Be1       O3               106.46(6)      4_554  .      4_555  N
  Na1       Be1       O3               161.61(7)      4_554  .     -4_656  N
  Na1       Be1       O5                61.29(5)      4_554  .     -1_656  N
  Na1       Be1       O9                56.58(5)      4_554  .      1_555  N
  O3        Be1       O3                91.60(8)      4_555  .     -4_656  N
  O3        Be1       O5               113.04(7)      4_555  .     -1_656  N
  O3        Be1       O9               114.36(8)      4_555  .      1_555  N
  O3        Be1       O5               115.14(8)     -4_656  .     -1_656  N
  O3        Be1       O9               113.04(7)     -4_656  .      1_555  N
  O5        Be1       O9               108.96(9)     -1_656  .      1_555  N
  O1        Si1       O2               109.03(4)      1_555  .      1_555  N
  O1        Si1       O3               109.24(5)      1_555  .      1_555  N
  O1        Si1       O4               109.15(5)      1_555  .      1_554  N
  O2        Si1       O3               108.61(4)      1_555  .      1_555  N
  O2        Si1       O4               110.88(4)      1_555  .      1_554  N
  O3        Si1       O4               109.89(4)      1_555  .      1_554  N
  O4        Si2       O5               110.06(4)      1_555  .      1_555  N
  O4        Si2       O6               108.78(5)      1_555  .      1_555  N
  O4        Si2       O7               104.48(4)      1_555  .      1_555  N
  O5        Si2       O6               109.82(4)      1_555  .      1_555  N
  O5        Si2       O7               114.31(4)      1_555  .      1_555  N
  O6        Si2       O7               109.16(5)      1_555  .      1_555  N
  O2        Si3       O7               102.23(4)      1_555  .      1_555  N
  O2        Si3       O8               108.45(4)      1_555  .      1_555  N
  O2        Si3       O9               111.30(4)      1_555  .      1_555  N
  O7        Si3       O8               109.33(5)      1_555  .      1_555  N
  O7        Si3       O9               115.35(4)      1_555  .      1_555  N
  O8        Si3       O9               109.79(4)      1_555  .      1_555  N
  Si1       O1        Si1              142.97(7)      1_555  .      3_555  N
  Na1       O2        Si1              120.72(4)      1_555  .      1_555  N
  Na1       O2        Si3              101.06(4)      1_555  .      1_555  N
  Si1       O2        Si3              138.18(5)      1_555  .      1_555  N
  Be1       O3        Be1               88.40(8)      4_554  .     -4_546  N
  Be1       O3        Si1              133.95(7)      4_554  .      1_555  N
  Be1       O3        Si1              135.02(7)     -4_455  .      1_555  N
  Si1       O4        Si2              152.03(5)      1_556  .      1_555  N
  Na1       O5        Na1             79.718(27)      4_555  .     -4_546  N
  Na1       O5        Be1               95.78(5)      4_555  .     -1_656  N
  Na1       O5        Si2              117.30(4)      4_555  .      1_555  N
  Na1       O5        Be1               85.99(5)     -4_647  .     -1_656  N
  Na1       O5        Si2              138.06(4)     -4_657  .      1_555  N
  Be1       O5        Si2              126.10(7)     -1_656  .      1_555  N
  Si2       O6        Si2              144.28(7)      1_555  .      3_555  N
  Na1       O7        Si2              113.21(4)      1_555  .      1_555  N
  Na1       O7        Si3             98.879(34)      1_555  .      1_555  N
  Si2       O7        Si3              147.59(5)      1_555  .      1_555  N
  Si3       O8        Si3              139.29(7)      1_555  .      3_555  N
  Na1       O9        Be1               90.81(5)      4_554  .      1_555  N
  Na1       O9        Si3              133.18(4)      4_554  .      1_555  N
  Be1       O9        Si3              125.11(7)      1_555  .      1_555  N
  Na1       O10       Na1              152.25(5)      1_555  .      3_555  N
  Na1       O10       H1              100.53(14)      1_555  .     -2_566  N
  Na1       O10       H2               97.47(19)      1_555  .     -2_566  N
  Na1       O10       H1              100.53(14)      3_555  .     -2_566  N
  Na1       O10       H2               97.47(19)      3_555  .     -2_566  N
  H1        O10       H2                97.6(11)     -2_566  .     -2_566  N
  O10       H1        H2                 42.3(8)     -2_666  .      1_555  N
  O10       H2        H1                 40.1(8)     -2_666  .      1_555  N
data_EPIDIDYMITE_s_01


_reflns_number_total                   11300
_reflns_limit_h_min                    -16
_reflns_limit_h_max                    16
_reflns_limit_k_min                    -16
_reflns_limit_k_max                    17
_reflns_limit_l_min                    -9
_reflns_limit_l_max                    9
_reflns_d_resolution_high              0.768
_reflns_d_resolution_low               6.793

# Powder diffraction data for histogram  2
data_EPIDIDYMITE_p_02

_pd_block_id
  2008-07-07T21:33|EPIDIDYMITE_H_02|A|D20
#==============================================================================
# 9. INSTRUMENT CHARACTERIZATION

_exptl_special_details
; ?
;

# if regions of the data are excluded, the reason(s) are supplied here:
_pd_proc_info_excluded_regions
; ?
;

# The following item is used to identify the equipment used to record
# the powder pattern when the diffractogram was measured at a laboratory
# other than the authors' home institution, e.g. when neutron or synchrotron
# radiation is used.

_pd_instr_location
; ?
;
_pd_calibration_special_details           # description of the method used
                                          # to calibrate the instrument
; ?
;

_diffrn_ambient_temperature       ?
_diffrn_source                    ?
_diffrn_source_target             ?
_diffrn_source_type               ?
_diffrn_measurement_device_type   ?
_diffrn_detector                  ?
_diffrn_detector_type             ?       # make or model of detector

_pd_meas_scan_method              ?       # options are 'step', 'cont',
                                          # 'tof', 'fixed' or
                                          # 'disp' (= dispersive)
_pd_meas_special_details
;  ?
;

# The following two items identify the program(s) used (if appropriate).
_computing_data_collection        ?
_computing_data_reduction         ?

# Describe any processing performed on the data, prior to refinement.
# For example: a manual Lp correction or a precomputed absorption correction
_pd_proc_info_data_reduction      ?

# The following item is used for angular dispersive measurements only.

_diffrn_radiation_monochromator   ?

# The following items are used to define the size of the instrument.
# Not all distances are appropriate for all instrument types.

_pd_instr_dist_src/mono           ?
_pd_instr_dist_mono/spec          ?
_pd_instr_dist_src/spec           ?
_pd_instr_dist_spec/anal          ?
_pd_instr_dist_anal/detc          ?
_pd_instr_dist_spec/detc          ?

# 10. Specimen size and mounting information

# The next three fields give the specimen dimensions in mm.  The equatorial
# plane contains the incident and diffracted beam.

_pd_spec_size_axial               ?       # perpendicular to
                                          # equatorial plane

_pd_spec_size_equat               ?       # parallel to
                                          # scattering vector
                                          # in transmission

_pd_spec_size_thick               ?       # parallel to
                                          # scattering vector
                                          # in reflection

_pd_spec_mounting                         # This field should be
                                          # used to give details of the
                                          # container.
; ?
;

_pd_spec_mount_mode               ?       # options are 'reflection'
                                          # or 'transmission'

_pd_spec_shape                    ?       # options are 'cylinder'
                                          # 'flat_sheet' or 'irregular'

# phase table
loop_     _pd_phase_id
          _pd_phase_block_id
          _pd_phase_mass_%
          _pd_proc_ls_profile_function
          _pd_proc_ls_peak_cutoff
  1  2008-07-07T21:33|EPIDIDYMITE_phase1|A||
          ?
;
 CW Profile function number 2 with  18 terms
 Profile coefficients for Simpson's rule integration of pseudovoigt function
 C.J. Howard (1982). J. Appl. Cryst.,15,615-620.
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 #1(GU)   =  248.943 #2(GV)   = -486.424 #3(GW)   =  374.117
 #4(LX)   =   16.895 #5(LY)   =    0.631 #6(trns) =    0.000
 #7(asym) =  -3.8238 #8(shft) =   0.0000 #9(GP)   =    0.000
 #10(stec)=     0.00 #11(ptec)=     0.00 #12(sfec)=     0.00
 #13(L11) =    0.000 #14(L22) =    0.000 #15(L33) =    0.000
 #16(L12) =    0.000 #17(L13) =    0.000 #18(L23) =    0.000
 Peak tails are ignored  where the intensity is below 0.0100 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
           0.01000

loop_ _atom_type_symbol
      _atom_type_scat_length_neutron
      _atom_type_scat_source
  Na   0.3630
  International_Tables_Vol_C
  Be   0.7790
  International_Tables_Vol_C
  Si   0.4149
  International_Tables_Vol_C
  O   0.5803
  International_Tables_Vol_C
  H  -0.3739
  International_Tables_Vol_C
_diffrn_radiation_probe                neutron
_diffrn_radiation_wavelength           1.8678
_pd_proc_ls_prof_R_factor              0.0070
_pd_proc_ls_prof_wR_factor             0.0097
_pd_proc_ls_prof_wR_expected           0.0038
_refine_ls_R_Fsqd_factor               0.08259

_pd_proc_ls_background_function
;   GSAS Background function number 2 with 11 terms.
 Cosine Fourier series
      1:    6665.83     2:    3148.25     3:   -1761.84     4:    1879.06    
      5:   -1599.16     6:    1079.55     7:   -679.860     8:    516.821    
      9:   -314.006    10:    114.436    11:   -39.2505    
;

_exptl_absorpt_process_details
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_exptl_absorpt_correction_T_min        1.00000
_exptl_absorpt_correction_T_max        1.00000
# Extinction correction
_gsas_exptl_extinct_corr_T_min         1.00000
_gsas_exptl_extinct_corr_T_max         1.00000
_pd_proc_info_datetime                 2008-07-07T21:33:30
_pd_calc_method                        "Rietveld Refinement"

#---- raw/calc data loop -----
_pd_meas_2theta_range_min              0.0
_pd_meas_2theta_range_max              157.2
_pd_meas_2theta_range_inc              0.1
_pd_proc_2theta_range_min              -0.2268
_pd_proc_2theta_range_max              156.9732
_pd_proc_2theta_range_inc              0.1

loop_
      _pd_meas_intensity_total
      _pd_proc_ls_weight
      _pd_proc_intensity_bkg_calc
      _pd_calc_intensity_total
   65777(89)    0.0        9010.    .
   61667(86)    0.0        9010.    .
   57556(83)    0.0        9010.    .
   53445(79)    0.0        9010.    .
   49336(76)    0.0        9010.    .
   45223(73)    0.0        9010.    .
   41114(70)    0.0        9010.    .
   37003(66)    0.0        9010.    .
   32891(63)    0.0        9010.    .
   28401(58)    0.0        9010.    .
   27740(58)    0.0        9010.    .
   33636(63)    0.0        9010.    .
   38257(68)    0.0        9010.    .
   32262(62)    0.0        9010.    .
   20302(49)    0.0        9010.    .
   10777(35)    0.0        9009.7   .
   6016(27)     0.0        9009.6   .
   4531(23)     0.0        9009.6   .
   3724(21)     0.0        9009.6   .
   3170(19)     0.0        9009.5   .
   2972(19)     0.0        9009.5   .
   2968(19)     0.0        9009.5   .
   2987(19)     0.0        9009.4   .
   2790(18)     0.0        9009.4   .
   2653(18)     0.0        9009.4   .
   2555(17)     0.0        9009.3   .
   2596(18)     0.0        9009.3   .
   2656(18)     0.0        9009.2   .
   2710(18)     0.0        9009.2   .
   2778(18)     0.0        9009.1   .
   2862(19)     0.0        9009.1   .
   2931(19)     0.0        9009.0   .
   3010(19)     0.0        9009.0   .
   3063(19)     0.0        9008.9   .
   3093(19)     0.0        9008.8   .
   3160(20)     0.0        9008.8   .
   3163(20)     0.0        9008.7   .
   3209(20)     0.0        9008.6   .
   3218(20)     0.0        9008.6   .
   3192(20)     0.0        9008.5   .
   3208(20)     0.0        9008.4   .
   3139(19)     0.0        9008.3   .
   3167(19)     0.0        9008.2   .
   3123(19)     0.0        9008.2   .
   3087(19)     0.0        9008.1   .
   3094(19)     0.0        9008.0   .
   3064(19)     0.0        9007.9   .
   3066(19)     0.0        9007.8   .
   3105(19)     0.0        9007.7   .
   3073(19)     0.0        9007.6   .
   3105(19)     0.0        9007.5   .
   3112(19)     0.0        9007.4   .
   3176(19)     0.0        9007.2   .
   3322(20)     0.0        9007.1   .
   3531(21)     0.0        9007.0   .
   3732(21)     0.0        9006.9   .
   3973(22)     0.0        9006.7   .
   4294(23)     0.0        9006.6   .
   4578(23)     0.0        9006.5   .
   4843(24)     0.0        9006.3   .
   5156(25)     0.0        9006.2   .
   5488(26)     0.0        9006.0   .
   5791(26)     0.0        9005.9   .
   6113(27)     0.0        9005.7   .
   6416(28)     0.0        9005.6   .
   6766(28)     0.0        9005.4   .
   7029(29)     0.0        9005.2   .
   7318(30)     0.0        9005.0   .
   7532(31)     0.0        9004.9   .
   7669(31)     0.0        9004.7   .
   7773(31)     0.0        9004.5   .
   7897(31)     0.0        9004.3   .
   7941(31)     0.0        9004.1   .
   7957(31)     0.0        9003.9   .
   8082(31)     0.0        9003.7   .
   8160(31)     0.0        9003.4   .
   8298(31)     0.0        9003.2   .
   8285(31)     0.0        9003.0   .
   8354(32)     0.0        9002.7   .
   8396(32)     0.0        9002.5   .
   8403(31)     0.0        9002.3   .
   8430(32)     0.0        9002.0   .
   8617(32)     0.0        9001.8   .
   8505(32)     0.0        9001.5   .
   8619(32)     0.0        9001.2   .
   8723(32)     0.0        9000.9   .
   8664(32)     0.0        9000.7   .
   8825(32)     0.0        9000.4   .
   8850(32)     0.0        9000.1   .
   8880(33)     0.0        8999.8   .
   8942(33)     0.0        8999.5   .
   8952(33)     0.0        8999.1   .
   9060(33)     0.0        8998.8   .
   9063(33)     0.0        8998.5   .
   9142(33)     0.0        8998.2   .
   9122(33)     0.0        8997.8   .
   9092(33)     0.0        8997.5   .
   9111(33)     0.0        8997.1   .
   9148(33)     0.0        8996.7   .
   9155(33)     0.0        8996.4   .
   9069(34)     0.0        8996.0   .
   9112(34)     0.0        8995.6   .
   9141(33)     0.0        8995.2   .
   9113(33)     0.0        8994.8   .
   9028(33)     0.0        8994.4   .
   9050(33)     0.0        8994.0   .
   9069(33)     0.0        8993.6   .
   8973(33)     0.0        8993.1   .
   9064(33)     0.0        8992.7   .
   9127(33)     0.0        8992.2   .
   9020(33)     0.0        8991.8   .
   9031(33)     0.0        8991.3   .
   9036(33)     0.0        8990.8   .
   8991(33)     0.0        8990.3   .
   9065(33)     0.0        8989.8   .
   9046(33)     0.0        8989.3   .
   9035(33)     0.0        8988.8   .
   9116(33)     0.0        8988.3   .
   9020(33)     0.0        8987.8   .
   9073(33)     0.0        8987.2   .
   9119(33)     0.0        8986.7   .
   9051(33)     0.000918   8986.1   8986.2
   9077(33)     0.000918   8985.6   8985.6
   8992(33)     0.000918   8985.0   8985.0
   9058(33)     0.000918   8984.4   8984.4
   8984(33)     0.000918   8983.8   8983.8
   9051(33)     0.000918   8983.2   8983.2
   9034(33)     0.000918   8982.6   8982.6
   9063(33)     0.000918   8982.0   8982.0
   8999(33)     0.000918   8981.4   8981.4
   9042(33)     0.000918   8980.7   8980.7
   8981(33)     0.000918   8980.1   8980.1
   8993(34)     0.000865   8979.4   8979.4
   9062(34)     0.000865   8978.8   8978.8
   9045(33)     0.000918   8978.1   8978.1
   9061(33)     0.000918   8977.4   8977.4
   9084(33)     0.000918   8976.7   8976.7
   9082(33)     0.000918   8976.0   8976.0
   9099(33)     0.000918   8975.3   8975.3
   9034(33)     0.000918   8974.5   8974.5
   9178(33)     0.000918   8973.8   8973.8
   9019(33)     0.000918   8973.0   8973.1
   9056(33)     0.000918   8972.3   8972.3
   9124(33)     0.000918   8971.5   8971.5
   9076(32)     0.000977   8970.7   8988.0
   9050(33)     0.000918   8969.9   8989.5
   9036(34)     0.000865   8969.1   8991.3
   9036(32)     0.000977   8968.3   8993.8
   9058(33)     0.000918   8967.5   8996.9
   8931(32)     0.000977   8966.7   9001.1
   8967(33)     0.000918   8965.8   9006.6
   8950(33)     0.000918   8965.0   9014.1
   8875(32)     0.000977   8964.1   9024.8
   8929(33)     0.000918   8963.3   9041.5
   9014(33)     0.000918   8962.4   9073.7
   9167(33)     0.000918   8961.5   9168.9
   9272(33)     0.000918   8960.6   9321.9
   9575(34)     0.000865   8959.7   9617.1
   9905(34)     0.000865   8958.7   10091.8
   10455(35)    0.000816   8957.8   10690.1
   10751(36)    0.000772   8957.    11204.
   10751(36)    0.000772   8956.    11331.
   10555(35)    0.000816   8954.9   10990.0
   10164(35)    0.000816   8954.0   10427.1
   9751(35)     0.000816   8953.0   9913.8
   9522(34)     0.000865   8952.0   9590.7
   9530(35)     0.000816   8951.0   9495.4
   9794(34)     0.000865   8949.9   9646.4
   10274(35)    0.000816   8948.9   10086.1
   11087(36)    0.000772   8948.    10831.
   11894(38)    0.000693   8947.    11756.
   12640(39)    0.000657   8946.    12496.
   12599(39)    0.000657   8945.    12579.
   12020(38)    0.000693   8944.    11939.
   11100(37)    0.000730   8942.    11003.
   10146(34)    0.000865   8941.4   10174.1
   9453(34)     0.000865   8940.3   9618.2
   9197(33)     0.000918   8939.1   9313.5
   9148(33)     0.000918   8938.0   9151.7
   9066(33)     0.000918   8936.9   9086.3
   8974(33)     0.000918   8935.7   9054.0
   9019(33)     0.000918   8934.5   9035.8
   8969(33)     0.000918   8933.4   9026.4
   9003(33)     0.000918   8932.2   9027.0
   9017(33)     0.000918   8931.0   9045.3
   9068(32)     0.000977   8929.8   9096.1
   9179(33)     0.000918   8928.6   9194.3
   9297(33)     0.000918   8927.3   9339.0
   9455(34)     0.000865   8926.1   9491.8
   9492(34)     0.000865   8924.8   9549.3
   9505(34)     0.000865   8923.6   9499.7
   9365(33)     0.000918   8922.3   9353.5
   9199(33)     0.000918   8921.0   9194.0
   9078(33)     0.000918   8919.8   9072.4
   8989(33)     0.000918   8918.5   8999.1
   8974(33)     0.000918   8917.2   8961.7
   8897(33)     0.000918   8915.8   8943.9
   8964(34)     0.000865   8914.5   8934.7
   8968(33)     0.000918   8913.2   8929.0
   8893(33)     0.000918   8911.8   8924.7
   8967(33)     0.000918   8910.5   8921.2
   8921(33)     0.000918   8909.1   8918.1
   8906(33)     0.000918   8907.8   8915.5
   8945(33)     0.000918   8906.4   8913.1
   8922(33)     0.000918   8905.0   8910.8
   8936(33)     0.000918   8903.6   8908.7
   8894(33)     0.000918   8902.2   8902.2
   8945(33)     0.000918   8900.8   8900.8
   8925(33)     0.000918   8899.3   8899.3
   8869(32)     0.000977   8897.9   8898.3
   8966(33)     0.000918   8896.5   8896.9
   9004(33)     0.000918   8895.0   8895.5
   8952(33)     0.000918   8893.6   8894.1
   8929(33)     0.000918   8892.1   8892.7
   8904(33)     0.000918   8890.6   8891.4
   8969(33)     0.000918   8889.1   8890.0
   8941(33)     0.000918   8887.6   8888.7
   8905(33)     0.000918   8886.1   8910.4
   8956(33)     0.000918   8884.6   8912.6
   8969(33)     0.000918   8883.1   8915.0
   8946(33)     0.000918   8881.6   8918.4
   8899(33)     0.000918   8880.1   8923.7
   8938(33)     0.000918   8878.5   8932.4
   8933(33)     0.000918   8877.0   8947.1
   8975(33)     0.000918   8875.4   8968.3
   8967(33)     0.000918   8873.9   8995.7
   9006(33)     0.000918   8872.3   9024.7
   8981(33)     0.000918   8870.7   9051.4
   8981(34)     0.000865   8869.2   9088.9
   9092(34)     0.000865   8867.6   9180.8
   9266(33)     0.000918   8866.0   9407.0
   9738(35)     0.000816   8864.4   9871.6
   10435(35)    0.000816   8862.8   10630.9
   11464(37)    0.000730   8861.    11570.
   12118(38)    0.000693   8860.    12302.
   12147(38)    0.000693   8858.    12318.
   11485(37)    0.000730   8856.    11612.
   10711(36)    0.000772   8855.    10679.
   9724(33)     0.000918   8853.0   9917.1
   9264(34)     0.000865   8851.4   9446.1
   9069(33)     0.000918   8849.7   9206.4
   9001(33)     0.000918   8848.1   9088.1
   8887(32)     0.000977   8846.4   9018.8
   8833(33)     0.000918   8844.7   8971.2
   8846(32)     0.000977   8843.1   8937.1
   8871(32)     0.000977   8841.4   8913.9
   8849(32)     0.000977   8839.7   8898.1
   8872(33)     0.000918   8838.0   8886.6
   8907(33)     0.000918   8836.3   8877.8
   8864(32)     0.000977   8834.6   8870.5
   8836(33)     0.000918   8832.9   8864.3
   8878(32)     0.000977   8831.2   8858.9
   8882(33)     0.000918   8829.5   8830.5
   8863(32)     0.000977   8827.8   8828.7
   8844(33)     0.000918   8826.1   8826.8
   8922(33)     0.000918   8824.4   8825.0
   8898(33)     0.000918   8822.7   8823.2
   8857(33)     0.000918   8821.0   8821.0
   8890(33)     0.000918   8819.2   8819.2
   8887(33)     0.000918   8817.5   8817.5
   8933(33)     0.000918   8815.8   8815.8
   8922(33)     0.000918   8814.0   8814.3
   8880(33)     0.000918   8812.3   8812.6
   8941(33)     0.000918   8810.6   8810.9
   8956(33)     0.000918   8808.8   8809.3
   8855(33)     0.000918   8807.1   8807.6
   8847(32)     0.000977   8805.3   8805.9
   8836(32)     0.000977   8803.6   8804.3
   8869(33)     0.000918   8801.8   8802.7
   8815(32)     0.000977   8800.1   8801.1
   8824(32)     0.000977   8798.3   8799.6
   8772(32)     0.000977   8796.6   8798.4
   8807(32)     0.000977   8794.8   8797.6
   8718(32)     0.000977   8793.1   8797.9
   8800(32)     0.000977   8791.3   8800.7
   8804(32)     0.000977   8789.5   8806.9
   8787(32)     0.000977   8787.8   8816.1
   8791(32)     0.000977   8786.0   8824.8
   8777(32)     0.000977   8784.3   8826.3
   8809(32)     0.000977   8782.5   8818.3
   8810(32)     0.000977   8780.8   8809.1
   8799(32)     0.000977   8779.0   8797.8
   8820(32)     0.000977   8777.2   8790.1
   8801(32)     0.000977   8775.5   8785.6
   8857(32)     0.000977   8773.7   8783.2
   8857(32)     0.000977   8772.0   8781.9
   8852(32)     0.000977   8770.2   8781.2
   8870(32)     0.000977   8768.4   8781.1
   8808(32)     0.000977   8766.7   8781.7
   8823(32)     0.000977   8764.9   8783.5
   8851(32)     0.000977   8763.2   8787.7
   8905(33)     0.000918   8761.4   8797.6
   8911(33)     0.000918   8759.7   8820.9
   8959(33)     0.000918   8757.9   8873.0
   9040(33)     0.000918   8756.2   8968.4
   9202(33)     0.000918   8754.4   9109.7
   9357(33)     0.000918   8752.7   9263.3
   9494(34)     0.000865   8750.9   9352.2
   9509(34)     0.000865   8749.2   9306.4
   9343(33)     0.000918   8747.4   9159.1
   9126(33)     0.000918   8745.7   9001.3
   9039(33)     0.000918   8744.0   8885.6
   8894(32)     0.000977   8742.2   8819.8
   8951(33)     0.000918   8740.5   8790.1
   8830(32)     0.000977   8738.8   8780.2
   8859(32)     0.000977   8737.0   8788.8
   8882(32)     0.000977   8735.3   8805.7
   8896(32)     0.000977   8733.6   8835.9
   8927(32)     0.000977   8731.9   8872.8
   8923(32)     0.000977   8730.2   8901.3
   8995(33)     0.000918   8728.5   8901.5
   8945(33)     0.000918   8726.7   8869.8
   8862(32)     0.000977   8725.0   8828.1
   8793(32)     0.000977   8723.3   8795.0
   8795(32)     0.000977   8721.6   8773.8
   8743(32)     0.000977   8719.9   8773.2
   8772(32)     0.000977   8718.3   8791.7
   8843(32)     0.000977   8716.6   8842.1
   8916(33)     0.000918   8714.9   8945.2
   9062(33)     0.000918   8713.2   9113.9
   9237(33)     0.000918   8711.5   9321.7
   9405(34)     0.000865   8709.9   9487.7
   9349(33)     0.000918   8708.2   9490.8
   9247(33)     0.000918   8706.5   9324.0
   9031(33)     0.000918   8704.9   9106.5
   8805(33)     0.000918   8703.2   8932.1
   8694(33)     0.000918   8701.6   8826.5
   8702(32)     0.000977   8699.9   8774.5
   8717(32)     0.000977   8698.3   8752.2
   8673(32)     0.000977   8696.7   8743.1
   8702(32)     0.000977   8695.0   8740.0
   8683(32)     0.000977   8693.4   8740.8
   8738(32)     0.000977   8691.8   8746.4
   8760(32)     0.000977   8690.2   8763.3
   8879(33)     0.000918   8688.6   8807.3
   8923(33)     0.000918   8686.9   8902.3
   9174(33)     0.000918   8685.3   9065.2
   9385(33)     0.000918   8683.8   9302.9
   9543(34)     0.000865   8682.2   9466.6
   9517(34)     0.000865   8680.6   9459.3
   9405(33)     0.000918   8679.0   9308.2
   9251(33)     0.000918   8677.4   9138.7
   9120(33)     0.000918   8675.8   9031.4
   9121(33)     0.000918   8674.3   8988.4
   9012(33)     0.000918   8672.7   8966.4
   9023(33)     0.000918   8671.2   8938.3
   8957(33)     0.000918   8669.6   8917.2
   8936(33)     0.000918   8668.1   8927.8
   9032(33)     0.000918   8666.5   9005.4
   9246(33)     0.000918   8665.0   9251.6
   9707(34)     0.000865   8663.5   9749.5
   10641(36)    0.000772   8662.    10648.
   11984(38)    0.000693   8660.    11888.
   13128(40)    0.000625   8659.    13015.
   13443(40)    0.000625   8657.    13235.
   12542(39)    0.000657   8656.    12343.
   11339(38)    0.000693   8654.    11079.
   10090(35)    0.000816   8653.0   10052.7
   9396(34)     0.000865   8651.5   9444.4
   9049(33)     0.000918   8650.0   9174.2
   8962(33)     0.000918   8648.5   9121.1
   8975(33)     0.000918   8647.1   9249.3
   9326(33)     0.000918   8645.6   9628.3
   10052(34)    0.000865   8644.1   10351.2
   11087(36)    0.000772   8643.    11336.
   12153(38)    0.000693   8641.    12194.
   12195(38)    0.000693   8640.    12283.
   11407(37)    0.000730   8638.    11508.
   10397(35)    0.000816   8637.0   10485.8
   9528(34)     0.000865   8635.5   9679.6
   9102(33)     0.000918   8634.1   9204.1
   8944(33)     0.000918   8632.7   8950.2
   8828(32)     0.000977   8631.3   8864.2
   8841(32)     0.000977   8629.9   8840.2
   8899(33)     0.000918   8628.5   8848.1
   8925(33)     0.000918   8627.1   8881.5
   9059(33)     0.000918   8625.7   8956.5
   8995(32)     0.000977   8624.3   9125.1
   9495(34)     0.000865   8623.0   9444.9
   10008(34)    0.000865   8621.6   9895.0
   10429(35)    0.000816   8620.2   10290.2
   10539(35)    0.000816   8618.9   10330.2
   10194(35)    0.000816   8617.5   9978.2
   9713(34)     0.000865   8616.2   9495.6
   9261(33)     0.000918   8614.8   9138.9
   9022(33)     0.000918   8613.5   8919.5
   8868(33)     0.000918   8612.1   8797.3
   8779(33)     0.000918   8610.8   8730.8
   8704(33)     0.000918   8609.5   8693.4
   8673(33)     0.000918   8608.1   8672.7
   8728(33)     0.000918   8606.8   8662.9
   8726(32)     0.000977   8605.5   8663.1
   8700(32)     0.000977   8604.2   8676.8
   8726(32)     0.000977   8602.9   8710.1
   8745(32)     0.000977   8601.6   8760.7
   8768(32)     0.000977   8600.3   8809.6
   8733(32)     0.000977   8599.0   8821.5
   8685(32)     0.000977   8597.7   8781.7
   8629(32)     0.000977   8596.4   8710.3
   8568(32)     0.000977   8595.1   8661.7
   8557(32)     0.000977   8593.8   8634.1
   8573(32)     0.000977   8592.6   8625.2
   8529(32)     0.000977   8591.3   8628.7
   8519(32)     0.000977   8590.0   8638.2
   8538(32)     0.000977   8588.7   8643.4
   8578(32)     0.000977   8587.5   8636.5
   8523(32)     0.000977   8586.2   8624.4
   8528(32)     0.000977   8584.9   8611.7
   8505(32)     0.000977   8583.7   8604.3
   8516(32)     0.000977   8582.4   8601.1
   8469(32)     0.000977   8581.2   8599.0
   8511(32)     0.000977   8579.9   8595.6
   8545(32)     0.000977   8578.7   8591.8
   8567(32)     0.000977   8577.4   8587.7
   8536(32)     0.000977   8576.2   8586.2
   8554(32)     0.000977   8574.9   8586.1
   8509(32)     0.000977   8573.7   8587.4
   8526(32)     0.000977   8572.4   8591.1
   8612(32)     0.000977   8571.2   8600.9
   8616(32)     0.000977   8570.0   8624.9
   8616(33)     0.000918   8568.7   8674.7
   8696(33)     0.000918   8567.5   8754.7
   8837(33)     0.000918   8566.3   8846.6
   8848(33)     0.000918   8565.0   8895.6
   8802(32)     0.000977   8563.8   8855.8
   8822(32)     0.000977   8562.6   8775.6
   8636(32)     0.000977   8561.3   8692.0
   8598(32)     0.000977   8560.1   8638.8
   8597(32)     0.000977   8558.9   8613.4
   8565(32)     0.000977   8557.6   8603.8
   8572(32)     0.000977   8556.4   8601.1
   8585(32)     0.000977   8555.2   8602.1
   8552(32)     0.000977   8553.9   8605.1
   8572(32)     0.000977   8552.7   8609.4
   8603(32)     0.000977   8551.5   8614.3
   8578(32)     0.000977   8550.2   8623.9
   8650(32)     0.000977   8549.0   8645.0
   8653(32)     0.000977   8547.7   8694.8
   8754(32)     0.000977   8546.5   8812.9
   8966(33)     0.000918   8545.3   9060.9
   9410(33)     0.000918   8544.0   9474.4
   9954(34)     0.000865   8542.8   9981.1
   10316(35)    0.000816   8541.5   10313.5
   10140(35)    0.000816   8540.3   10161.9
   9667(34)     0.000865   8539.0   9684.6
   9206(33)     0.000918   8537.8   9217.4
   8883(33)     0.000918   8536.5   8913.3
   8750(32)     0.000977   8535.2   8771.4
   8687(32)     0.000977   8534.0   8730.8
   8650(32)     0.000977   8532.7   8730.7
   8732(32)     0.000977   8531.4   8729.9
   8688(33)     0.000918   8530.2   8703.9
   8634(33)     0.000918   8528.9   8673.2
   8619(32)     0.000977   8527.6   8657.2
   8656(33)     0.000918   8526.3   8671.2
   8670(32)     0.000977   8525.0   8739.2
   8879(33)     0.000918   8523.7   8900.2
   9157(33)     0.000918   8522.5   9180.6
   9502(34)     0.000865   8521.2   9530.9
   9773(34)     0.000865   8519.8   9751.8
   9713(34)     0.000865   8518.5   9659.4
   9436(34)     0.000865   8517.2   9338.8
   9060(33)     0.000918   8515.9   9035.3
   8905(33)     0.000918   8514.6   8872.3
   8869(32)     0.000977   8513.2   8873.5
   9089(33)     0.000918   8511.9   9010.4
   9256(33)     0.000918   8510.5   9207.6
   9383(33)     0.000918   8509.2   9317.4
   9316(33)     0.000918   8507.8   9219.1
   9175(33)     0.000918   8506.5   8999.7
   8896(33)     0.000918   8505.1   8799.8
   8777(32)     0.000977   8503.7   8675.0
   8682(32)     0.000977   8502.3   8623.6
   8673(32)     0.000977   8501.0   8626.3
   8700(32)     0.000977   8499.6   8671.7
   8793(33)     0.000918   8498.2   8755.7
   8875(33)     0.000918   8496.7   8833.4
   8874(33)     0.000918   8495.3   8857.4
   8832(33)     0.000918   8493.9   8790.6
   8806(32)     0.000977   8492.5   8691.8
   8687(32)     0.000977   8491.0   8613.3
   8617(32)     0.000977   8489.6   8568.9
   8586(32)     0.000977   8488.1   8551.2
   8587(32)     0.000977   8486.6   8550.3
   8521(33)     0.000918   8485.1   8560.4
   8545(33)     0.000918   8483.7   8601.0
   8608(32)     0.000977   8482.2   8689.7
   8724(32)     0.000977   8480.7   8843.1
   8896(33)     0.000918   8479.1   9040.9
   9035(33)     0.000918   8477.6   9194.2
   9048(33)     0.000918   8476.1   9206.7
   8985(33)     0.000918   8474.5   9119.6
   8868(33)     0.000918   8473.0   9019.5
   8788(32)     0.000977   8471.4   8900.4
   8663(32)     0.000977   8469.8   8760.1
   8499(32)     0.000977   8468.3   8644.6
   8434(32)     0.000977   8466.7   8570.1
   8443(32)     0.000977   8465.1   8533.1
   8440(32)     0.000977   8463.4   8522.4
   8529(32)     0.000977   8461.8   8529.3
   8516(32)     0.000977   8460.2   8547.8
   8547(32)     0.000977   8458.5   8559.6
   8576(32)     0.000977   8456.9   8550.8
   8548(32)     0.000977   8455.2   8527.1
   8595(32)     0.000977   8453.5   8505.9
   8585(32)     0.000977   8451.8   8497.1
   8588(32)     0.000977   8450.1   8500.3
   8689(32)     0.0        8448.4   .
   8819(32)     0.0        8446.6   .
   9071(33)     0.0        8444.9   .
   9444(34)     0.0        8443.1   .
   9496(34)     0.0        8441.3   .
   9289(33)     0.0        8439.6   .
   9072(33)     0.0        8437.8   .
   8896(33)     0.0        8435.9   .
   8804(33)     0.0        8434.1   .
   8835(33)     0.000918   8432.3   8796.6
   8899(33)     0.000918   8430.4   8870.6
   9046(33)     0.000918   8428.6   8881.8
   9309(33)     0.000918   8426.7   8893.6
   9553(34)     0.000865   8424.8   9033.5
   9973(35)     0.000816   8422.9   9435.8
   10529(35)    0.000816   8421.0   10167.9
   11256(37)    0.000730   8419.    11097.
   11790(38)    0.000693   8417.    11672.
   11505(37)    0.000730   8415.    11365.
   10710(36)    0.000772   8413.    10480.
   9869(34)     0.000865   8411.2   9633.5
   9536(34)     0.0        8409.1   .
   9502(34)     0.0        8407.1   .
   9532(34)     0.0        8405.1   .
   9486(34)     0.0        8403.0   .
   9243(33)     0.0        8401.0   .
   8941(33)     0.0        8398.9   .
   8834(32)     0.0        8396.8   .
   8779(32)     0.000977   8394.7   8734.3
   8818(32)     0.000977   8392.5   8813.6
   9032(33)     0.000918   8390.4   9078.7
   9540(34)     0.000865   8388.2   9559.9
   10089(35)    0.000816   8386.1   10134.6
   10373(35)    0.000816   8383.9   10423.5
   10123(35)    0.000816   8381.7   10102.7
   9551(34)     0.000865   8379.5   9514.5
   9084(33)     0.000918   8377.2   9026.6
   8817(33)     0.000918   8375.0   8755.8
   8717(32)     0.000977   8372.7   8672.3
   8715(32)     0.000977   8370.4   8699.6
   8730(32)     0.000977   8368.1   8757.4
   8748(33)     0.000918   8365.8   8753.6
   8618(33)     0.000918   8363.4   8666.1
   8542(32)     0.000977   8361.1   8563.2
   8535(32)     0.000977   8358.7   8490.2
   8506(32)     0.000977   8356.3   8450.6
   8464(32)     0.000977   8353.9   8433.3
   8479(32)     0.000977   8351.5   8428.1
   8442(32)     0.000977   8349.1   8423.7
   8431(32)     0.000977   8346.6   8427.1
   8402(32)     0.000977   8344.2   8432.7
   8402(32)     0.000977   8341.7   8469.4
   8457(32)     0.000977   8339.2   8507.2
   8402(32)     0.000977   8336.7   8523.8
   8418(32)     0.000977   8334.1   8525.2
   8423(32)     0.000977   8331.6   8520.0
   8384(31)     0.001041   8329.0   8492.3
   8341(31)     0.001041   8326.4   8448.9
   8302(31)     0.001041   8323.8   8413.1
   8311(31)     0.001041   8321.2   8404.4
   8356(31)     0.001041   8318.6   8433.7
   8460(32)     0.000977   8315.9   8516.6
   8610(32)     0.000977   8313.2   8660.5
   8831(32)     0.000977   8310.5   8828.9
   8908(33)     0.000918   8307.8   8911.1
   8810(32)     0.000977   8305.1   8826.3
   8652(32)     0.000977   8302.4   8661.5
   8540(32)     0.000977   8299.6   8521.8
   8427(32)     0.000977   8296.8   8437.1
   8372(32)     0.000977   8294.0   8398.5
   8366(32)     0.000977   8291.2   8385.5
   8413(32)     0.000977   8288.4   8375.2
   8380(32)     0.000977   8285.6   8361.3
   8324(32)     0.000977   8282.7   8356.9
   8365(32)     0.000977   8279.8   8373.2
   8377(32)     0.000977   8276.9   8416.5
   8421(32)     0.000977   8274.0   8479.3
   8474(32)     0.000977   8271.1   8531.8
   8496(32)     0.000977   8268.1   8523.5
   8473(32)     0.000977   8265.2   8457.6
   8418(32)     0.000977   8262.2   8389.3
   8352(32)     0.000977   8259.2   8345.9
   8359(31)     0.001041   8256.2   8328.4
   8365(32)     0.000977   8253.2   8314.8
   8356(32)     0.000977   8250.1   8298.7
   8362(32)     0.000977   8247.0   8285.0
   8349(31)     0.001041   8244.0   8278.4
   8360(32)     0.000977   8240.9   8268.4
   8343(31)     0.001041   8237.7   8259.4
   8344(31)     0.001041   8234.6   8253.2
   8309(31)     0.001041   8231.5   8258.7
   8309(31)     0.001041   8228.3   8258.6
   8290(31)     0.001041   8225.1   8259.2
   8245(31)     0.001041   8221.9   8259.1
   8217(31)     0.001041   8218.7   8257.8
   8176(31)     0.001041   8215.5   8259.0
   8186(31)     0.001041   8212.2   8269.8
   8187(31)     0.001041   8209.0   8281.2
   8188(31)     0.001041   8205.7   8299.8
   8223(31)     0.001041   8202.4   8337.4
   8285(32)     0.000977   8199.1   8417.5
   8471(32)     0.000977   8195.7   8570.7
   8788(33)     0.000918   8192.4   8804.0
   9071(33)     0.000918   8189.0   9064.3
   9224(33)     0.000918   8185.7   9211.3
   9255(34)     0.000865   8182.3   9297.8
   9526(34)     0.000865   8178.9   9488.0
   9775(34)     0.000865   8175.4   9700.6
   9742(34)     0.000865   8172.0   9636.9
   9375(33)     0.000918   8168.5   9320.5
   9126(33)     0.000918   8165.1   9077.6
   9027(33)     0.000918   8161.6   9059.9
   9171(33)     0.000918   8158.1   9192.4
   9231(33)     0.000918   8154.6   9239.7
   9097(33)     0.000918   8151.0   9096.2
   8935(33)     0.000918   8147.5   8892.6
   8800(32)     0.000977   8143.9   8775.9
   8978(32)     0.000977   8140.4   8876.5
   9356(33)     0.000918   8136.8   9266.8
   10039(35)    0.000816   8133.2   9882.9
   10540(35)    0.000816   8129.6   10389.5
   10402(35)    0.000816   8125.9   10321.9
   9826(34)     0.000865   8122.3   9751.1
   9195(33)     0.000918   8118.6   9127.2
   8776(32)     0.000977   8115.0   8712.9
   8597(32)     0.000977   8111.3   8493.7
   8499(32)     0.000977   8107.6   8412.8
   8511(32)     0.000977   8103.9   8386.9
   8510(32)     0.000977   8100.1   8366.9
   8406(32)     0.000977   8096.4   8351.3
   8352(32)     0.000977   8092.6   8360.8
   8434(32)     0.000977   8088.9   8411.9
   8532(32)     0.000977   8085.1   8478.1
   8617(32)     0.000977   8081.3   8548.0
   8666(32)     0.000977   8077.5   8608.5
   8617(32)     0.000977   8073.7   8596.6
   8583(32)     0.000977   8069.8   8513.6
   8541(32)     0.000977   8066.0   8462.2
   8635(33)     0.000918   8062.1   8549.3
   8850(33)     0.000918   8058.3   8779.6
   9145(33)     0.000918   8054.4   9034.4
   9178(33)     0.000918   8050.5   9075.3
   8932(33)     0.000918   8046.6   8832.4
   8576(32)     0.000977   8042.7   8523.2
   8288(31)     0.001041   8038.8   8298.2
   8183(31)     0.001041   8034.9   8175.2
   8126(31)     0.001041   8030.9   8121.1
   7981(31)     0.001041   8027.0   8093.6
   7984(31)     0.001041   8023.0   8077.7
   7998(31)     0.001041   8019.0   8066.6
   7897(30)     0.001111   8015.0   8060.3
   7910(30)     0.001111   8011.0   8057.9
   7885(31)     0.001041   8007.0   8059.9
   7931(31)     0.001041   8003.0   8072.5
   7996(31)     0.001041   7999.0   8094.9
   8060(31)     0.001041   7994.9   8127.5
   8074(31)     0.001041   7990.9   8178.0
   8148(31)     0.001041   7986.9   8253.2
   8198(31)     0.001041   7982.8   8323.1
   8261(31)     0.001041   7978.7   8348.9
   8284(31)     0.001041   7974.6   8356.3
   8344(31)     0.001041   7970.5   8407.1
   8403(32)     0.000977   7966.5   8476.0
   8373(31)     0.001041   7962.4   8450.2
   8244(31)     0.001041   7958.2   8314.5
   8104(31)     0.001041   7954.1   8175.2
   7964(31)     0.001041   7950.0   8087.3
   7976(31)     0.001041   7945.9   8051.3
   7983(31)     0.001041   7941.7   8045.3
   8005(31)     0.001041   7937.6   8049.1
   7995(32)     0.000977   7933.4   8044.0
   8026(31)     0.001041   7929.3   8052.8
   8102(31)     0.001041   7925.1   8111.7
   8193(30)     0.001111   7920.9   8214.6
   8382(30)     0.001111   7916.7   8340.8
   8315(34)     0.000865   7912.5   8391.8
   8279(36)     0.000772   7908.    8306.
   8194(33)     0.000918   7904.2   8180.0
   8152(29)     0.001189   7900.0   8095.1
   8118(30)     0.001111   7895.7   8071.5
   8130(31)     0.001041   7891.5   8093.6
   8187(31)     0.001041   7887.3   8143.0
   8260(31)     0.001041   7883.1   8193.7
   8321(31)     0.001041   7878.9   8275.5
   8467(32)     0.000977   7874.6   8449.1
   8717(32)     0.000977   7870.4   8715.7
   8995(33)     0.000918   7866.2   8980.0
   9159(33)     0.000918   7861.9   9184.2
   9406(33)     0.000918   7857.7   9405.1
   9474(33)     0.000918   7853.4   9508.6
   9227(33)     0.000918   7849.2   9226.6
   8779(32)     0.000977   7844.9   8745.8
   8366(31)     0.001041   7840.7   8355.2
   8145(31)     0.001041   7836.4   8130.9
   8055(31)     0.001041   7832.2   8023.6
   7989(31)     0.001041   7827.9   7969.2
   7936(31)     0.001041   7823.7   7936.1
   7885(31)     0.001041   7819.4   7920.5
   7896(31)     0.001041   7815.1   7931.7
   7902(31)     0.001041   7810.9   7965.2
   7924(31)     0.001041   7806.6   8025.2
   7962(31)     0.001041   7802.3   8082.4
   7985(32)     0.000977   7798.1   8086.2
   7942(31)     0.001041   7793.8   8024.1
   7880(31)     0.001041   7789.5   7961.1
   7900(31)     0.001041   7785.3   7923.6
   7879(31)     0.001041   7781.0   7910.6
   7943(31)     0.001041   7776.7   7936.8
   7986(31)     0.001041   7772.5   7973.2
   7982(31)     0.001041   7768.2   7988.4
   7951(31)     0.001041   7764.0   7984.4
   7965(31)     0.001041   7759.7   8009.6
   8078(31)     0.001041   7755.4   8121.5
   8371(31)     0.001041   7751.2   8349.7
   8623(32)     0.000977   7746.9   8637.6
   8639(32)     0.000977   7742.7   8795.3
   8535(32)     0.000977   7738.4   8662.8
   8285(31)     0.001041   7734.2   8419.7
   8181(31)     0.001041   7730.0   8269.8
   8227(31)     0.001041   7725.7   8254.9
   8204(31)     0.001041   7721.5   8320.4
   8188(31)     0.001041   7717.3   8309.7
   8091(31)     0.001041   7713.0   8190.3
   7976(31)     0.001041   7708.8   8077.7
   7972(31)     0.001041   7704.6   8067.1
   8138(31)     0.001041   7700.4   8189.2
   8381(31)     0.001041   7696.2   8424.9
   8574(32)     0.000977   7692.0   8643.1
   8535(32)     0.000977   7687.8   8626.8
   8353(31)     0.001041   7683.6   8398.9
   8134(31)     0.001041   7679.4   8165.7
   7986(31)     0.001041   7675.2   8021.4
   7914(31)     0.001041   7671.1   7963.5
   7994(31)     0.001041   7666.9   8012.4
   8210(32)     0.000977   7662.7   8206.9
   8699(32)     0.000977   7658.6   8612.0
   9482(34)     0.000865   7654.4   9195.6
   10016(35)    0.000816   7650.3   9659.5
   9854(34)     0.000865   7646.2   9566.1
   9193(33)     0.000918   7642.1   9106.8
   8755(32)     0.000977   7637.9   8703.2
   8488(32)     0.000977   7633.8   8444.5
   8266(31)     0.001041   7629.8   8218.1
   8086(31)     0.001041   7625.7   8016.3
   7926(30)     0.001111   7621.6   7871.8
   7851(30)     0.001111   7617.5   7791.0
   7852(30)     0.0        7613.5   .
   8176(31)     0.0        7609.4   .
   8761(32)     0.0        7605.4   .
   9097(33)     0.0        7601.4   .
   8735(32)     0.0        7597.3   .
   8172(31)     0.0        7593.3   .
   7909(31)     0.0        7589.3   .
   7810(30)     0.0        7585.4   .
   7779(30)     0.001111   7581.4   7835.7
   7853(30)     0.001111   7577.4   7838.2
   7934(30)     0.001111   7573.5   7870.7
   8055(31)     0.001041   7569.5   7913.1
   8168(31)     0.001041   7565.6   7962.1
   8100(30)     0.001111   7561.7   7995.7
   7932(28)     0.001276   7557.8   7943.4
   7733(45)     0.000494   7554.    7825.
   7641(40)     0.000625   7550.    7717.
   7562(28)     0.001276   7546.2   7652.1
   7569(28)     0.001276   7542.4   7625.6
   7488(35)     0.0        7538.5   .
   7718(33)     0.0        7534.7   .
   8231(31)     0.0        7530.9   .
   8828(32)     0.0        7527.1   .
   8932(33)     0.0        7523.4   .
   8494(32)     0.0        7519.6   .
   7936(31)     0.0        7515.9   .
   7675(30)     0.0        7512.1   .
   7662(30)     0.001111   7508.4   7558.3
   7670(30)     0.001111   7504.7   7580.6
   7641(30)     0.001111   7501.1   7628.5
   7730(30)     0.001111   7497.4   7718.7
   7880(31)     0.001041   7493.8   7843.1
   7935(31)     0.001041   7490.1   7936.1
   7908(31)     0.001041   7486.5   7907.1
   7804(30)     0.001111   7482.9   7790.5
   7720(30)     0.001111   7479.3   7693.5
   7678(30)     0.001111   7475.8   7661.5
   7711(30)     0.001111   7472.3   7693.0
   7788(30)     0.001111   7468.7   7758.3
   7805(30)     0.001111   7465.2   7794.3
   7758(30)     0.001111   7461.7   7761.0
   7720(30)     0.001111   7458.3   7706.8
   7702(30)     0.001111   7454.8   7702.0
   7782(30)     0.001111   7451.4   7768.9
   7853(31)     0.001041   7448.0   7875.1
   7915(31)     0.001041   7444.6   7929.6
   7906(31)     0.001041   7441.2   7900.7
   7914(31)     0.001041   7437.9   7893.8
   8002(31)     0.001041   7434.6   7962.4
   8061(31)     0.001041   7431.3   8044.7
   8035(31)     0.001041   7428.0   8049.4
   7933(31)     0.001041   7424.7   7933.2
   7771(31)     0.001041   7421.5   7776.0
   7697(31)     0.001041   7418.3   7674.8
   7712(31)     0.001041   7415.1   7657.6
   7739(30)     0.001111   7411.9   7722.8
   7893(31)     0.001041   7408.7   7841.3
   8018(31)     0.001041   7405.6   7933.9
   7940(31)     0.001041   7402.5   7900.1
   7838(31)     0.001041   7399.4   7795.6
   7781(30)     0.001111   7396.3   7724.8
   7831(31)     0.001041   7393.3   7746.2
   7918(31)     0.001041   7390.2   7875.6
   8204(31)     0.001041   7387.3   8107.7
   8438(32)     0.000977   7384.3   8380.0
   8679(32)     0.000977   7381.3   8654.1
   8957(33)     0.000918   7378.4   8966.7
   9126(33)     0.000918   7375.5   9193.0
   9005(33)     0.000918   7372.6   9075.3
   8616(32)     0.000977   7369.8   8622.3
   8159(31)     0.001041   7366.9   8135.4
   7872(31)     0.001041   7364.1   7804.5
   7697(30)     0.001111   7361.3   7635.3
   7621(30)     0.001111   7358.6   7575.1
   7673(30)     0.001111   7355.9   7576.1
   7694(30)     0.001111   7353.2   7609.6
   7624(30)     0.001111   7350.5   7631.3
   7580(30)     0.001111   7347.8   7589.7
   7544(30)     0.001111   7345.2   7525.1
   7482(30)     0.001111   7342.6   7487.9
   7477(30)     0.001111   7340.0   7471.1
   7479(30)     0.001111   7337.5   7472.6
   7487(30)     0.001111   7335.0   7476.9
   7501(31)     0.001041   7332.5   7472.3
   7496(31)     0.001041   7330.0   7461.1
   7480(30)     0.001111   7327.6   7461.5
   7534(30)     0.001111   7325.1   7485.5
   7583(30)     0.001111   7322.8   7523.2
   7663(30)     0.001111   7320.4   7583.0
   7798(31)     0.001041   7318.1   7698.0
   8025(31)     0.001041   7315.8   7928.5
   8431(32)     0.000977   7313.5   8342.0
   8960(33)     0.000918   7311.2   8927.6
   9419(34)     0.000865   7309.0   9465.1
   9710(34)     0.000865   7306.8   9732.3
   9758(34)     0.000865   7304.7   9759.5
   9542(34)     0.000865   7302.5   9507.4
   9002(33)     0.000918   7300.4   8955.6
   8494(32)     0.000977   7298.3   8429.0
   8158(31)     0.001041   7296.3   8113.0
   7964(31)     0.001041   7294.3   7937.5
   7786(30)     0.001111   7292.3   7792.3
   7613(30)     0.001111   7290.3   7659.3
   7585(30)     0.001111   7288.4   7568.5
   7571(30)     0.001111   7286.5   7536.5
   7599(30)     0.001111   7284.6   7558.4
   7635(30)     0.001111   7282.8   7603.3
   7635(30)     0.001111   7281.0   7620.9
   7617(30)     0.001111   7279.2   7581.7
   7570(30)     0.001111   7277.4   7521.2
   7512(30)     0.001111   7275.7   7483.7
   7545(30)     0.001111   7274.0   7506.1
   7647(30)     0.001111   7272.3   7597.3
   7832(31)     0.001041   7270.7   7740.4
   7971(31)     0.001041   7269.1   7912.4
   8122(32)     0.000977   7267.5   8088.4
   8215(32)     0.000977   7266.0   8283.4
   8258(32)     0.000977   7264.5   8376.7
   8119(31)     0.001041   7263.0   8220.4
   7867(31)     0.001041   7261.6   7913.6
   7603(30)     0.001111   7260.1   7652.7
   7463(30)     0.001111   7258.8   7502.0
   7437(30)     0.001111   7257.4   7443.6
   7453(29)     0.001189   7256.1   7441.4
   7488(30)     0.001111   7254.8   7459.5
   7487(30)     0.001111   7253.5   7471.5
   7453(30)     0.001111   7252.3   7438.0
   7404(30)     0.001111   7251.1   7403.7
   7401(30)     0.001111   7249.9   7393.5
   7410(30)     0.001111   7248.8   7417.9
   7490(30)     0.001111   7247.7   7483.8
   7594(30)     0.001111   7246.6   7578.8
   7642(30)     0.001111   7245.5   7663.9
   7696(30)     0.001111   7244.5   7682.5
   7684(30)     0.001111   7243.5   7660.3
   7714(30)     0.001111   7242.6   7686.3
   7812(31)     0.001041   7241.7   7820.8
   7969(31)     0.001041   7240.8   8028.8
   8108(31)     0.001041   7239.9   8152.9
   8056(31)     0.001041   7239.1   8082.3
   7852(31)     0.001041   7238.3   7946.3
   7848(31)     0.001041   7237.5   7923.6
   8057(31)     0.001041   7236.8   8135.6
   8601(32)     0.000977   7236.1   8606.6
   9290(33)     0.000918   7235.4   9181.1
   9468(34)     0.000865   7234.8   9430.0
   9052(33)     0.000918   7234.2   9083.4
   8406(32)     0.000977   7233.6   8513.2
   7969(32)     0.000977   7233.1   8081.7
   7783(31)     0.001041   7232.6   7864.4
   7656(30)     0.001111   7232.1   7793.5
   7669(30)     0.001111   7231.6   7764.5
   7650(30)     0.001111   7231.2   7701.9
   7543(30)     0.001111   7230.8   7591.3
   7481(30)     0.001111   7230.5   7491.5
   7380(30)     0.001111   7230.1   7430.2
   7369(30)     0.001111   7229.8   7401.2
   7397(30)     0.001111   7229.6   7398.8
   7367(30)     0.001111   7229.3   7424.5
   7460(30)     0.001111   7229.1   7495.4
   7574(30)     0.001111   7229.0   7624.2
   7732(30)     0.001111   7228.8   7802.1
   7942(31)     0.001041   7228.7   7984.7
   7999(31)     0.001041   7228.6   8021.9
   7871(31)     0.001041   7228.6   7883.9
   7705(30)     0.001111   7228.5   7706.9
   7588(30)     0.001111   7228.5   7586.3
   7485(30)     0.001111   7228.6   7495.6
   7391(30)     0.001111   7228.6   7431.7
   7365(30)     0.001111   7228.7   7393.0
   7393(30)     0.001111   7228.9   7379.8
   7431(30)     0.001111   7229.0   7387.5
   7426(30)     0.001111   7229.2   7407.4
   7421(30)     0.001111   7229.4   7444.3
   7508(30)     0.001111   7229.7   7506.9
   7615(30)     0.001111   7229.9   7591.8
   7749(30)     0.001111   7230.2   7681.2
   7871(31)     0.001041   7230.6   7823.9
   8116(31)     0.001041   7230.9   8131.7
   8673(33)     0.000918   7231.3   8669.5
   9271(34)     0.000865   7231.7   9311.8
   9489(34)     0.000865   7232.2   9652.2
   9240(34)     0.000865   7232.6   9452.0
   8684(32)     0.000977   7233.1   8903.9
   8227(31)     0.001041   7233.6   8361.1
   7929(31)     0.001041   7234.2   8027.1
   7814(31)     0.001041   7234.8   7910.0
   7852(31)     0.001041   7235.4   7919.6
   7808(31)     0.001041   7236.0   7903.0
   7653(30)     0.001111   7236.7   7795.5
   7562(30)     0.001111   7237.4   7691.2
   7513(30)     0.001111   7238.1   7655.6
   7540(30)     0.001111   7238.8   7680.6
   7579(30)     0.001111   7239.6   7736.1
   7629(30)     0.001111   7240.4   7795.5
   7614(30)     0.001111   7241.2   7792.7
   7586(30)     0.001111   7242.0   7733.4
   7582(30)     0.001111   7242.9   7694.3
   7568(30)     0.001111   7243.8   7661.8
   7561(30)     0.001111   7244.7   7613.9
   7508(30)     0.001111   7245.6   7535.2
   7440(30)     0.001111   7246.6   7458.2
   7378(30)     0.001111   7247.6   7393.1
   7365(30)     0.001111   7248.6   7354.6
   7356(30)     0.001111   7249.6   7338.5
   7370(30)     0.001111   7250.7   7335.7
   7357(30)     0.001111   7251.7   7345.3
   7341(30)     0.001111   7252.8   7352.0
   7339(30)     0.001111   7254.0   7355.7
   7350(30)     0.001111   7255.1   7368.3
   7382(30)     0.001111   7256.3   7394.1
   7404(30)     0.001111   7257.5   7445.0
   7508(31)     0.001041   7258.7   7545.9
   7687(31)     0.001041   7259.9   7736.5
   7995(31)     0.001041   7261.2   8050.4
   8449(32)     0.000977   7262.4   8459.3
   8855(33)     0.000918   7263.7   8820.2
   8859(33)     0.000918   7265.0   8837.3
   8501(32)     0.000977   7266.4   8504.8
   8097(31)     0.001041   7267.7   8124.4
   7828(31)     0.001041   7269.1   7846.5
   7757(31)     0.0        7270.5   .
   7912(31)     0.0        7271.9   .
   8378(32)     0.0        7273.3   .
   8675(32)     0.0        7274.7   .
   8549(32)     0.0        7276.2   .
   8275(32)     0.0        7277.7   .
   8034(31)     0.0        7279.2   .
   7868(31)     0.0        7280.7   .
   7846(31)     0.001041   7282.2   7794.5
   7949(31)     0.001041   7283.8   7778.4
   8052(31)     0.001041   7285.3   7788.3
   8112(31)     0.001041   7286.9   7758.4
   8088(31)     0.001041   7288.5   7699.0
   8018(31)     0.001041   7290.1   7666.0
   7988(31)     0.001041   7291.7   7686.9
   7984(31)     0.001041   7293.3   7753.0
   8011(31)     0.001041   7295.0   7821.4
   8039(31)     0.001041   7296.6   7884.3
   8109(31)     0.001041   7298.3   7983.4
   8317(32)     0.0        7300.0   .
   8801(33)     0.0        7301.7   .
   9657(34)     0.0        7303.4   .
   10391(36)    0.0        7305.    .
   10290(36)    0.0        7307.    .
   9603(35)     0.0        7308.5   .
   8914(33)     0.0        7310.3   .
   8396(32)     0.0        7312.1   .
   8082(31)     0.0        7313.8   .
   7901(31)     0.0        7315.6   .
   7849(31)     0.001041   7317.4   7780.7
   7872(31)     0.001041   7319.2   7749.8
   7759(31)     0.001041   7321.0   7706.5
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   8851(33)     0.000918   7467.3   8883.1
   8928(33)     0.000918   7468.4   8971.8
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   7895(31)     0.001041   7475.6   7910.9
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   7792(31)     0.001041   7478.4   7889.5
   7855(31)     0.001041   7479.3   7908.7
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   7840(31)     0.001041   7482.6   7873.9
   7916(31)     0.001041   7483.4   7905.1
   7998(31)     0.001041   7484.2   7990.1
   8070(31)     0.001041   7484.9   8123.9
   8211(31)     0.001041   7485.6   8238.2
   8279(32)     0.000977   7486.3   8281.4
   8257(32)     0.000977   7486.9   8241.1
   8174(31)     0.001041   7487.6   8152.1
   8053(31)     0.001041   7488.2   8074.7
   8042(31)     0.001041   7488.8   8028.2
   8034(31)     0.001041   7489.3   7974.0
   7908(31)     0.001041   7489.9   7896.7
   7810(31)     0.001041   7490.4   7822.8
   7784(31)     0.001041   7490.9   7777.9
   7739(31)     0.001041   7491.3   7766.0
   7723(31)     0.001041   7491.8   7773.2
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   7637(31)     0.001041   7492.6   7755.0
   7639(31)     0.001041   7493.0   7726.2
   7682(31)     0.001041   7493.3   7699.7
   7626(31)     0.001041   7493.6   7676.9
   7638(31)     0.001041   7494.0   7674.2
   7678(31)     0.001041   7494.2   7688.2
   7677(31)     0.001041   7494.5   7719.4
   7742(31)     0.001041   7494.7   7756.7
   7745(31)     0.001041   7494.9   7779.8
   7724(31)     0.001041   7495.1   7771.4
   7717(31)     0.001041   7495.3   7751.5
   7712(31)     0.001041   7495.4   7755.4
   7776(31)     0.001041   7495.6   7799.1
   7871(31)     0.001041   7495.6   7891.5
   7991(31)     0.001041   7495.7   8011.1
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   8171(31)     0.001041   7495.8   8099.0
   8074(31)     0.001041   7495.8   8012.2
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   7806(31)     0.001041   7495.7   7873.2
   7840(31)     0.001041   7495.7   7887.0
   7931(31)     0.001041   7495.6   7971.5
   8082(31)     0.001041   7495.5   8120.4
   8279(32)     0.000977   7495.4   8322.7
   8505(32)     0.000977   7495.2   8546.2
   8691(32)     0.000977   7495.1   8735.6
   8769(33)     0.000918   7494.9   8824.2
   8804(33)     0.000918   7494.6   8810.5
   8704(33)     0.000918   7494.4   8691.2
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   8261(32)     0.000977   7493.9   8270.4
   8026(32)     0.000977   7493.6   8080.3
   7939(32)     0.000977   7493.3   7955.4
   7924(31)     0.001041   7492.9   7888.3
   7892(31)     0.001041   7492.6   7860.4
   7868(31)     0.001041   7492.2   7855.2
   7905(31)     0.001041   7491.8   7866.5
   7976(31)     0.001041   7491.4   7907.4
   8016(31)     0.001041   7491.0   7998.2
   8157(31)     0.001041   7490.5   8141.5
   8366(32)     0.000977   7490.1   8326.3
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   8579(32)     0.000977   7489.1   8550.2
   8536(32)     0.000977   7488.5   8477.1
   8435(32)     0.000977   7488.0   8362.2
   8314(32)     0.000977   7487.4   8280.8
   8235(32)     0.000977   7486.9   8248.0
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   8439(32)     0.000977   7483.8   8469.1
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   8478(32)     0.000977   7481.7   8493.8
   8314(32)     0.000977   7481.0   8289.3
   8130(31)     0.001041   7480.3   8075.4
   7982(31)     0.001041   7479.5   7904.8
   7847(31)     0.001041   7478.8   7800.5
   7776(31)     0.001041   7478.0   7739.3
   7774(31)     0.001041   7477.2   7711.8
   7749(31)     0.001041   7476.4   7698.9
   7710(31)     0.001041   7475.6   7690.6
   7745(31)     0.001041   7474.8   7685.0
   7757(31)     0.001041   7474.0   7686.6
   7725(31)     0.001041   7473.2   7696.9
   7721(31)     0.001041   7472.3   7738.9
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   7852(31)     0.001041   7470.6   7889.6
   7932(31)     0.001041   7469.7   7970.3
   7950(31)     0.001041   7468.8   8017.2
   7922(31)     0.001041   7467.9   8003.7
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   7786(31)     0.001041   7466.1   7847.0
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   7602(30)     0.001111   7464.3   7745.9
   7638(31)     0.0        7463.4   .
   7688(30)     0.0        7462.4   .
   7738(31)     0.0        7461.5   .
   7850(31)     0.0        7460.5   .
   8010(31)     0.0        7459.6   .
   8212(31)     0.0        7458.6   .
   8510(32)     0.0        7457.6   .
   8798(33)     0.0        7456.7   .
   8929(33)     0.0        7455.7   .
   8962(33)     0.0        7454.7   .
   8927(33)     0.0        7453.7   .
   8738(32)     0.0        7452.7   .
   8507(32)     0.0        7451.7   .
   8264(32)     0.0        7450.8   .
   8064(31)     0.0        7449.8   .
   7970(31)     0.0        7448.8   .
   7844(31)     0.0        7447.8   .
   7794(31)     0.0        7446.8   .
   7800(31)     0.001041   7445.8   7650.0
   7745(31)     0.001041   7444.8   7659.9
   7747(31)     0.001041   7443.8   7689.0
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   7808(31)     0.001041   7438.8   7724.5
   7795(31)     0.0        7437.8   .
   7881(31)     0.0        7436.8   .
   7947(31)     0.0        7435.9   .
   8063(31)     0.0        7434.9   .
   8116(31)     0.0        7433.9   .
   8060(31)     0.0        7432.9   .
   7968(31)     0.0        7432.0   .
   7797(31)     0.0        7431.0   .
   7667(31)     0.0        7430.1   .
   7601(30)     0.0        7429.1   .
   7556(30)     0.001111   7428.2   7562.7
   7532(30)     0.001111   7427.2   7572.1
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   7877(31)     0.001041   7400.5   7826.6
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   7730(31)     0.001041   7397.6   7708.6
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   7518(30)     0.001111   7395.0   7563.3
   7571(31)     0.001041   7394.6   7571.6
   7580(31)     0.001041   7394.1   7583.2
   7556(31)     0.001041   7393.6   7589.1
   7511(31)     0.001041   7393.2   7586.2
   7499(30)     0.001111   7392.7   7585.8
   7557(30)     0.001111   7392.3   7589.8
   7587(30)     0.001111   7391.9   7608.2
   7577(30)     0.001111   7391.5   7643.4
   7646(30)     0.001111   7391.1   7696.4
   7778(31)     0.001041   7390.7   7763.9
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   7649(30)     0.001111   7387.4   7599.3
   7564(30)     0.001111   7387.1   7547.7
   7521(30)     0.001111   7386.8   7512.9
   7565(30)     0.001111   7386.5   7490.1
   7542(30)     0.001111   7386.3   7476.8
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   7559(30)     0.001111   7384.5   7549.0
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   7762(31)     0.001041   7383.0   7737.7
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   7826(31)     0.001041   7380.0   7822.4
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   7594(31)     0.001041   7371.2   7608.7
   7572(31)     0.001041   7370.5   7600.3
   7587(31)     0.001041   7369.8   7581.7
   7543(30)     0.001111   7369.1   7558.3
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   7501(30)     0.001111   7367.5   7518.4
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   7488(30)     0.001111   7363.8   7526.1
   7529(30)     0.001111   7362.8   7546.7
   7548(30)     0.001111   7361.8   7568.9
   7554(30)     0.001111   7360.7   7595.2
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   7624(30)     0.001111   7358.4   7646.7
   7629(30)     0.001111   7357.2   7665.6
   7666(30)     0.001111   7355.9   7674.2
   7639(31)     0.001041   7354.6   7672.0
   7616(31)     0.001041   7353.2   7662.3
   7648(30)     0.001111   7351.8   7645.1
   7615(30)     0.001111   7350.4   7624.8
   7606(30)     0.001111   7348.8   7604.4
   7597(30)     0.001111   7347.2   7586.4
   7591(30)     0.001111   7345.6   7571.7
   7581(30)     0.001111   7343.9   7559.5
   7568(30)     0.001111   7342.1   7549.4
   7553(30)     0.001111   7340.3   7542.1
   7546(30)     0.001111   7338.4   7537.8
   7538(30)     0.001111   7336.5   7539.2
   7582(30)     0.001111   7334.5   7548.9
   7593(31)     0.001041   7332.4   7566.6
   7605(31)     0.001041   7330.2   7592.9
   7700(31)     0.001041   7328.0   7625.6
   7767(31)     0.001041   7325.7   7660.8
   7778(31)     0.001041   7323.3   7691.7
   7750(31)     0.001041   7320.9   7710.3
   7763(31)     0.001041   7318.4   7713.6
   7782(31)     0.001041   7315.8   7701.2
   7710(31)     0.001041   7313.1   7675.4
   7627(30)     0.001111   7310.3   7640.0
   7599(30)     0.001111   7307.5   7599.8
   7589(30)     0.001111   7304.5   7560.0
   7534(30)     0.001111   7301.5   7525.4
   7471(30)     0.001111   7298.4   7498.6
   7496(30)     0.001111   7295.2   7481.1
   7486(30)     0.001111   7291.9   7472.0
   7424(30)     0.001111   7288.5   7472.2
   7435(30)     0.001111   7285.0   7479.2
   7455(30)     0.001111   7281.4   7492.6
   7471(30)     0.001111   7277.7   7510.9
   7484(30)     0.001111   7273.9   7532.1
   7463(30)    .           .        .
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   1021(11)    .           .        .
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   851(10)     .           .        .
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   676(9)      .           .        .
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   356(7)      .           .        .
   335(6)      .           .        .
   340(7)      .           .        .
   340(6)      .           .        .
  100.0(20)    .           .        .
   0.0(10)     .           .        .
   0.0(10)     .           .        .
   0.0(10)     .           .        .
   0.0(10)     .           .        .
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   0.0(10)     .           .        .
   0.0(10)     .           .        .
   0.0(10)     .           .        .
   0.0(10)     .           .        .
   0.0(10)     .           .        .
_pd_meas_number_of_points              1573
_pd_proc_number_of_points              1573

_reflns_number_total                   651
_reflns_limit_h_min                    0
_reflns_limit_h_max                    12
_reflns_limit_k_min                    0
_reflns_limit_k_max                    13
_reflns_limit_l_min                    0
_reflns_limit_l_max                    7
_reflns_d_resolution_high              0.996
_reflns_d_resolution_low               6.793
#--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--#
