 
data_c2c
 
_audit_creation_method            SHELXL-97
_chemical_name_systematic
;
 ?
;
_chemical_name_common             ?
_chemical_melting_point           ?
_chemical_formula_moiety          ?
_chemical_formula_sum
 'As1.06 Cl3 O12.23 Pb10.67 Si0.27'
_chemical_formula_weight          2598.79
 
loop_
 _atom_type_symbol
 _atom_type_description
 _atom_type_scat_dispersion_real
 _atom_type_scat_dispersion_imag
 _atom_type_scat_source
 'O'  'O'   0.0106   0.0060
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'As'  'As'   0.0499   2.0058
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Cl'  'Cl'   0.1484   0.1585
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Pb'  'Pb'  -3.3944  10.1111
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Si'  'Si'   0.0817   0.0704
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 
_symmetry_cell_setting            ?
_symmetry_space_group_name_H-M    ?
 
loop_
 _symmetry_equiv_pos_as_xyz
 'x, y, z'
 '-x, y, -z+1/2'
 'x+1/2, y+1/2, z'
 '-x+1/2, y+1/2, -z+1/2'
 '-x, -y, -z'
 'x, -y, z-1/2'
 '-x+1/2, -y+1/2, -z'
 'x+1/2, -y+1/2, z-1/2'
 
_cell_length_a                    23.139(4)
_cell_length_b                    22.684(4)
_cell_length_c                    12.389(2)
_cell_angle_alpha                 90.00
_cell_angle_beta                  102.090(3)
_cell_angle_gamma                 90.00
_cell_volume                      6358.8(18)
_cell_formula_units_Z             12
_cell_measurement_temperature     296(2)
_cell_measurement_reflns_used     ?
_cell_measurement_theta_min       ?
_cell_measurement_theta_max       ?
 
_exptl_crystal_description        ?
_exptl_crystal_colour             ?
_exptl_crystal_size_max           ?
_exptl_crystal_size_mid           ?
_exptl_crystal_size_min           ?
_exptl_crystal_density_meas       ?
_exptl_crystal_density_diffrn     8.144
_exptl_crystal_density_method     'not measured'
_exptl_crystal_F_000              12746
_exptl_absorpt_coefficient_mu     86.456
_exptl_absorpt_correction_type    ?
_exptl_absorpt_correction_T_min   ?
_exptl_absorpt_correction_T_max   ?
_exptl_absorpt_process_details    ?
 
_exptl_special_details
;
 ?
;
 
_diffrn_ambient_temperature       296(2)
_diffrn_radiation_wavelength      0.71073
_diffrn_radiation_type            MoK\a
_diffrn_radiation_source          'fine-focus sealed tube'
_diffrn_radiation_monochromator   graphite
_diffrn_measurement_device_type   ?
_diffrn_measurement_method        ?
_diffrn_detector_area_resol_mean  ?
_diffrn_standards_number          ?
_diffrn_standards_interval_count  ?
_diffrn_standards_interval_time   ?
_diffrn_standards_decay_%         ?
_diffrn_reflns_number             56375
_diffrn_reflns_av_R_equivalents   0.0888
_diffrn_reflns_av_sigmaI/netI     0.0934
_diffrn_reflns_limit_h_min        -38
_diffrn_reflns_limit_h_max        33
_diffrn_reflns_limit_k_min        -37
_diffrn_reflns_limit_k_max        37
_diffrn_reflns_limit_l_min        -20
_diffrn_reflns_limit_l_max        20
_diffrn_reflns_theta_min          1.27
_diffrn_reflns_theta_max          36.15
_reflns_number_total              14483
_reflns_number_gt                 6931
_reflns_threshold_expression      >2sigma(I)
 
_computing_data_collection        ?
_computing_cell_refinement        ?
_computing_data_reduction         ?
_computing_structure_solution     ?
_computing_structure_refinement   'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics     ?
_computing_publication_material   ?
 
_refine_special_details
;
 Refinement of F^2^ against ALL reflections.  The weighted R-factor wR and
 goodness of fit S are based on F^2^, conventional R-factors R are based
 on F, with F set to zero for negative F^2^. The threshold expression of
 F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is
 not relevant to the choice of reflections for refinement.  R-factors based
 on F^2^ are statistically about twice as large as those based on F, and R-
 factors based on ALL data will be even larger.
;
 
_refine_ls_structure_factor_coef  Fsqd
_refine_ls_matrix_type            full
_refine_ls_weighting_scheme       calc
_refine_ls_weighting_details
 'calc w=1/[\s^2^(Fo^2^)+(0.0389P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_atom_sites_solution_primary      direct
_atom_sites_solution_secondary    difmap
_atom_sites_solution_hydrogens    geom
_refine_ls_hydrogen_treatment     mixed
_refine_ls_extinction_method      SHELXL
_refine_ls_extinction_coef        0.0000022(5)
_refine_ls_extinction_expression
 'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^'
_refine_ls_number_reflns          14483
_refine_ls_number_parameters      288
_refine_ls_number_restraints      0
_refine_ls_R_factor_all           0.1475
_refine_ls_R_factor_gt            0.0535
_refine_ls_wR_factor_ref          0.1388
_refine_ls_wR_factor_gt           0.1080
_refine_ls_goodness_of_fit_ref    1.002
_refine_ls_restrained_S_all       1.002
_refine_ls_shift/su_max           0.001
_refine_ls_shift/su_mean          0.000
 
loop_
 _atom_site_label
 _atom_site_type_symbol
 _atom_site_fract_x
 _atom_site_fract_y
 _atom_site_fract_z
 _atom_site_U_iso_or_equiv
 _atom_site_adp_type
 _atom_site_occupancy
 _atom_site_symmetry_multiplicity
 _atom_site_calc_flag
 _atom_site_refinement_flags
 _atom_site_disorder_assembly
 _atom_site_disorder_group
Pb1 Pb 0.02370(3) 0.33013(3) 0.11179(5) 0.01240(13) Uani 1 1 d . . .
Pb2 Pb -0.13847(3) 0.33113(2) -0.05572(5) 0.00938(10) Uani 1 1 d . . .
Pb3 Pb 0.24274(3) 0.16730(3) 0.00179(5) 0.01195(13) Uani 1 1 d . . .
Pb4 Pb -0.03666(3) 0.55670(3) 0.37405(5) 0.01179(12) Uani 1 1 d . . .
Pb5 Pb -0.30232(3) 0.33470(3) -0.22005(5) 0.01283(13) Uani 1 1 d . . .
Pb6 Pb 0.08073(2) 0.16427(2) -0.17277(5) 0.00920(12) Uani 1 1 d . . .
Pb7 Pb -0.19191(3) 0.66864(3) -0.28106(5) 0.01232(13) Uani 1 1 d . . .
Pb8 Pb -0.07902(3) 0.44391(3) 0.15108(5) 0.01180(13) Uani 1 1 d . . .
Pb9 Pb -0.19752(3) 0.44554(3) -0.26142(5) 0.01285(13) Uani 1 1 d . . .
Pb10 Pb -0.02290(3) 0.04875(3) -0.11756(6) 0.01329(12) Uani 1 1 d . . .
Pb11 Pb 0.03095(3) 0.16428(3) 0.11131(5) 0.01614(14) Uani 1 1 d . . .
Pb12 Pb -0.23979(3) 0.55461(3) -0.48495(5) 0.01140(12) Uani 1 1 d . . .
Pb13 Pb -0.08201(3) 0.67123(3) 0.17201(5) 0.01177(12) Uani 1 1 d . . .
Pb14 Pb 0.18340(3) 0.05181(3) -0.23282(5) 0.01399(13) Uani 1 1 d . . .
Pb15 Pb 0.13716(3) 0.05425(3) 0.03687(5) 0.01445(13) Uani 1 1 d . . .
Pb16 Pb 0.14468(3) 0.16517(3) -0.43715(5) 0.01309(12) Uani 1 1 d . . .
As1 As 0.09489(10) -0.06941(11) -0.15611(18) 0.0129(6) Uani 0.596(10) 1 d P . .
Si1 Si 0.09489(10) -0.06941(11) -0.15611(18) 0.0129(6) Uani 0.404(10) 1 d P . .
As2 As -0.13500(8) 0.56799(8) -0.05413(16) 0.0174(5) Uani 0.988(6) 1 d P . .
Cl1 Cl -0.2500 0.2500 0.0000 0.0207(14) Uani 1 2 d S . .
Cl2 Cl 0.14014(19) 0.2363(2) 0.0553(4) 0.0204(8) Uani 1 1 d . . .
Cl3 Cl -0.02706(19) 0.24850(18) -0.1112(4) 0.0215(10) Uani 1 1 d . . .
Cl4 Cl -0.07823(18) 0.25894(19) 0.1645(3) 0.0192(9) Uani 1 1 d . . .
Cl5 Cl -0.30200(17) 0.75128(19) -0.2273(4) 0.0200(10) Uani 1 1 d . . .
O1 O 0.0926(6) 0.0011(6) -0.1634(10) 0.030(3) Uiso 1 1 d . . .
O2 O 0.0413(5) -0.0931(6) -0.0975(11) 0.031(3) Uiso 1 1 d . . .
O3 O -0.4013(5) 0.3997(5) -0.2770(9) 0.016(2) Uiso 1 1 d . . .
O4 O -0.3410(5) 0.4083(6) -0.0730(10) 0.024(3) Uiso 1 1 d . . .
O5 O -0.0749(9) 0.5950(9) 0.0400(16) 0.077(6) Uiso 1 1 d . . .
O6 O -0.1331(5) 0.4952(6) -0.0590(10) 0.027(3) Uiso 1 1 d . . .
O7 O -0.1185(9) 0.5952(11) -0.1698(18) 0.099(8) Uiso 1 1 d . . .
O8A O -0.1839(14) 0.5906(15) 0.015(3) 0.071(12) Uiso 0.58(3) 1 d P . .
O8B O -0.2059(16) 0.5928(17) -0.115(3) 0.048(13) Uiso 0.42(3) 1 d P . .
O9 O 0.2278(5) 0.1153(5) -0.3526(9) 0.008(3) Uiso 0.85(3) 1 d P . .
O10 O -0.0489(4) 0.3895(5) 0.0160(8) 0.014(2) Uiso 1 1 d . . .
O11 O -0.2255(4) 0.3907(5) -0.1289(8) 0.010(2) Uiso 1 1 d . . .
O12 O 0.0560(4) 0.1105(5) -0.0214(8) 0.012(2) Uiso 1 1 d . . .
O13 O 0.0000 0.1031(6) -0.2500 0.006(3) Uiso 1 2 d S . .
O14 O -0.1587(4) 0.3887(5) 0.0934(9) 0.014(2) Uiso 1 1 d . . .
O15 O 0.1695(4) 0.1091(5) -0.0956(8) 0.011(2) Uiso 1 1 d . . .
O16 O 0.2221(5) 0.1126(5) 0.1404(9) 0.018(3) Uiso 1 1 d . . .
O17 O -0.1172(4) 0.3897(5) -0.2119(9) 0.015(2) Uiso 1 1 d . . .
O18 O 0.0000 0.3853(7) 0.2500 0.013(3) Uiso 1 2 d S . .
O19 O 0.1077(4) 0.1034(5) -0.3268(8) 0.012(2) Uiso 1 1 d . . .
O20 O 0.0000 0.6202(7) 0.2500 0.015(3) Uiso 1 2 d S . .
 
loop_
 _atom_site_aniso_label
 _atom_site_aniso_U_11
 _atom_site_aniso_U_22
 _atom_site_aniso_U_33
 _atom_site_aniso_U_23
 _atom_site_aniso_U_13
 _atom_site_aniso_U_12
Pb1 0.0127(3) 0.0114(3) 0.0122(3) -0.0007(2) 0.0004(2) 0.0030(2)
Pb2 0.0116(2) 0.0066(2) 0.0097(2) -0.0005(2) 0.00158(17) -0.0008(2)
Pb3 0.0126(3) 0.0103(3) 0.0117(3) 0.0010(2) -0.0002(2) -0.0027(2)
Pb4 0.0157(3) 0.0076(3) 0.0121(2) -0.0009(2) 0.0032(2) 0.0037(2)
Pb5 0.0158(3) 0.0104(3) 0.0106(3) 0.0016(2) -0.0010(2) -0.0036(2)
Pb6 0.0099(2) 0.0057(2) 0.0111(3) 0.0008(2) 0.00000(19) -0.0001(2)
Pb7 0.0125(3) 0.0115(3) 0.0125(3) -0.0048(2) 0.0016(2) -0.0015(2)
Pb8 0.0131(3) 0.0062(3) 0.0154(3) -0.0033(2) 0.0014(2) -0.0008(2)
Pb9 0.0136(3) 0.0076(3) 0.0175(3) 0.0046(2) 0.0035(2) 0.0017(2)
Pb10 0.0133(3) 0.0091(2) 0.0171(3) 0.0060(2) 0.0025(2) -0.0008(2)
Pb11 0.0170(3) 0.0166(3) 0.0149(3) -0.0063(3) 0.0034(2) 0.0028(3)
Pb12 0.0153(3) 0.0069(3) 0.0114(2) 0.0020(2) 0.0016(2) -0.0016(2)
Pb13 0.0133(3) 0.0097(3) 0.0125(3) 0.0035(2) 0.0030(2) 0.0019(2)
Pb14 0.0170(3) 0.0115(3) 0.0126(3) -0.0014(2) 0.0012(2) 0.0061(2)
Pb15 0.0137(3) 0.0092(3) 0.0205(3) 0.0069(2) 0.0036(2) 0.0025(2)
Pb16 0.0142(3) 0.0117(3) 0.0146(3) 0.0041(2) 0.0056(2) 0.0026(2)
As1 0.0111(11) 0.0172(12) 0.0104(10) 0.0015(8) 0.0024(7) -0.0016(9)
Si1 0.0111(11) 0.0172(12) 0.0104(10) 0.0015(8) 0.0024(7) -0.0016(9)
As2 0.0179(9) 0.0133(9) 0.0225(9) 0.0010(8) 0.0076(7) 0.0004(7)
Cl1 0.022(3) 0.024(4) 0.017(3) 0.003(2) 0.007(2) 0.004(2)
Cl2 0.0168(18) 0.027(2) 0.0163(17) -0.002(2) 0.0005(14) 0.0014(19)
Cl3 0.019(2) 0.028(3) 0.018(2) -0.0065(19) 0.0047(17) -0.0028(19)
Cl4 0.021(2) 0.0171(19) 0.017(2) 0.0032(16) -0.0002(17) 0.0017(17)
Cl5 0.018(2) 0.027(3) 0.015(2) 0.0006(17) 0.0044(17) 0.0016(17)
 
_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
 
loop_
 _geom_bond_atom_site_label_1
 _geom_bond_atom_site_label_2
 _geom_bond_distance
 _geom_bond_site_symmetry_2
 _geom_bond_publ_flag
Pb1 O18 2.279(8) . ?
Pb1 O10 2.281(10) . ?
Pb1 O7 2.74(2) 5_565 ?
Pb1 O5 2.96(2) 5_565 ?
Pb1 Cl4 3.040(5) . ?
Pb1 Cl4 3.228(4) 2 ?
Pb1 Cl3 3.329(4) . ?
Pb1 Pb8 3.6101(10) . ?
Pb1 As2 3.641(2) 5_565 ?
Pb1 Pb11 3.7657(11) . ?
Pb1 Pb1 3.8086(14) 2 ?
Pb1 Pb2 3.8894(10) . ?
Pb2 O14 2.389(11) . ?
Pb2 O11 2.437(10) . ?
Pb2 O10 2.463(10) . ?
Pb2 O17 2.480(11) . ?
Pb2 Cl4 3.236(4) . ?
Pb2 Cl5 3.295(4) 4_444 ?
Pb2 Cl1 3.3570(7) . ?
Pb2 Cl3 3.373(5) . ?
Pb2 Pb8 3.6776(9) . ?
Pb2 Pb9 3.6930(9) . ?
Pb2 Pb4 3.6933(10) 6_565 ?
Pb2 Pb12 3.7207(10) 6_566 ?
Pb3 O16 2.250(12) . ?
Pb3 O15 2.284(10) . ?
Pb3 O8A 2.41(3) 3_545 ?
Pb3 O8B 2.66(4) 3_545 ?
Pb3 Cl2 3.030(5) . ?
Pb3 Cl5 3.390(4) 5_565 ?
Pb3 Cl5 3.395(4) 3_545 ?
Pb3 Pb15 3.6301(10) . ?
Pb3 Pb3 3.7679(14) 7 ?
Pb3 Pb5 3.8041(11) 8_556 ?
Pb3 Pb6 3.9166(9) . ?
Pb3 Pb9 3.9205(10) 8_556 ?
Pb4 O10 2.207(11) 6_566 ?
Pb4 O17 2.292(10) 6_566 ?
Pb4 O20 2.388(9) . ?
Pb4 O5 2.721(19) 2 ?
Pb4 O6 2.798(13) 6_566 ?
Pb4 Pb13 3.6077(9) . ?
Pb4 Pb2 3.6933(10) 6_566 ?
Pb4 Pb8 3.7421(10) . ?
Pb4 Pb9 3.7495(10) 6_566 ?
Pb4 Pb8 3.7617(11) 6_566 ?
Pb4 Pb8 3.7624(9) 2 ?
Pb4 Pb4 3.8093(14) 2 ?
Pb5 O16 2.269(12) 8_455 ?
Pb5 O11 2.283(10) . ?
Pb5 O3 2.691(10) . ?
Pb5 O4 2.756(13) . ?
Pb5 Cl5 3.239(4) 4_444 ?
Pb5 Cl2 3.250(4) 8_455 ?
Pb5 Cl1 3.3476(7) . ?
Pb5 Si1 3.436(2) 3_455 ?
Pb5 As1 3.436(2) 3_455 ?
Pb5 Pb9 3.6035(10) . ?
Pb5 Pb7 3.7693(12) 4_444 ?
Pb5 Pb3 3.8041(11) 8_455 ?
Pb6 O13 2.363(8) . ?
Pb6 O12 2.404(10) . ?
Pb6 O15 2.425(10) . ?
Pb6 O19 2.536(10) . ?
Pb6 Cl2 3.304(5) . ?
Pb6 Cl3 3.311(4) 2_554 ?
Pb6 Cl3 3.354(5) . ?
Pb6 Pb15 3.6412(9) . ?
Pb6 Pb14 3.6667(10) . ?
Pb6 Pb10 3.7109(10) . ?
Pb6 Pb13 3.7318(10) 5_565 ?
Pb6 Pb10 3.7346(9) 2_554 ?
Pb7 O9 2.239(11) 3_455 ?
Pb7 O14 2.281(11) 6_565 ?
Pb7 O7 2.56(2) . ?
Pb7 O8B 2.75(4) . ?
Pb7 Cl4 3.289(4) 6_565 ?
Pb7 Cl1 3.3232(7) 4_454 ?
Pb7 Cl5 3.341(4) . ?
Pb7 Pb12 3.6231(10) . ?
Pb7 As2 3.647(2) . ?
Pb7 Pb5 3.7693(12) 4_454 ?
Pb7 Pb2 3.8562(11) 6_565 ?
Pb7 Pb8 3.8688(10) 6_565 ?
Pb8 O14 2.220(10) . ?
Pb8 O10 2.303(11) . ?
Pb8 O18 2.382(8) . ?
Pb8 O7 2.72(2) 6_566 ?
Pb8 O6 2.886(12) . ?
Pb8 Pb12 3.7490(10) 6_566 ?
Pb8 Pb4 3.7617(11) 6_565 ?
Pb8 Pb4 3.7624(9) 2 ?
Pb8 Pb7 3.8688(10) 6_566 ?
Pb9 O17 2.227(10) . ?
Pb9 O11 2.259(11) . ?
Pb9 O16 2.393(11) 8_455 ?
Pb9 O6 2.866(12) . ?
Pb9 O8A 2.96(3) 6_565 ?
Pb9 Pb12 3.6895(10) . ?
Pb9 Pb14 3.7334(10) 3_455 ?
Pb9 Pb4 3.7495(10) 6_565 ?
Pb9 Pb12 3.7540(11) 6_566 ?
Pb9 Pb3 3.9205(10) 8_455 ?
Pb10 O13 2.204(7) . ?
Pb10 O19 2.302(10) 2_554 ?
Pb10 O12 2.410(10) . ?
Pb10 O2 2.961(13) 5 ?
Pb10 O1 3.044(13) . ?
Pb10 O1 3.049(12) 2_554 ?
Pb10 Pb10 3.6343(13) 5 ?
Pb10 Pb10 3.6537(15) 2_554 ?
Pb10 Pb6 3.7346(9) 2_554 ?
Pb10 Pb14 3.7880(10) 2_554 ?
Pb10 Pb15 3.7982(10) . ?
Pb11 O12 2.220(11) . ?
Pb11 O2 2.306(13) 5 ?
Pb11 O3 2.359(10) 8_556 ?
Pb11 Cl2 3.205(5) . ?
Pb11 Cl3 3.392(5) . ?
Pb11 Cl4 3.482(4) . ?
Pb11 Si1 3.652(2) 6_556 ?
Pb11 As1 3.652(2) 6_556 ?
Pb11 Pb15 3.7509(10) . ?
Pb12 O11 2.253(10) 6_565 ?
Pb12 O14 2.313(10) 6_565 ?
Pb12 O9 2.380(12) 3_455 ?
Pb12 O4 2.513(11) 6_565 ?
Pb12 O6 3.026(13) 6_565 ?
Pb12 Pb2 3.7207(10) 6_565 ?
Pb12 Pb8 3.7490(10) 6_565 ?
Pb12 Pb9 3.7540(11) 6_565 ?
Pb12 Pb16 3.8013(10) 3_455 ?
Pb12 Pb15 3.8210(10) 8_455 ?
Pb13 O20 2.260(8) . ?
Pb13 O17 2.265(11) 6_566 ?
Pb13 O5 2.41(2) . ?
Pb13 Cl3 3.273(5) 6_566 ?
Pb13 Cl3 3.324(5) 5_565 ?
Pb13 Cl5 3.396(4) 7_465 ?
Pb13 As2 3.660(2) . ?
Pb13 Pb6 3.7318(10) 5_565 ?
Pb13 Pb2 3.8646(11) 6_566 ?
Pb13 Pb13 3.8816(13) 2 ?
Pb13 Pb4 3.9078(10) 2 ?
Pb14 O15 2.215(10) . ?
Pb14 O19 2.223(10) . ?
Pb14 O9 2.444(12) . ?
Pb14 O1 2.690(13) . ?
Pb14 O8B 2.83(4) 3_545 ?
Pb14 Pb16 3.5880(10) . ?
Pb14 As1 3.671(2) . ?
Pb14 Pb15 3.7143(9) 6 ?
Pb14 Pb15 3.7161(11) . ?
Pb14 Pb9 3.7333(10) 3_545 ?
Pb14 Pb10 3.7880(10) 2_554 ?
Pb15 O12 2.260(10) . ?
Pb15 O15 2.306(11) . ?
Pb15 O16 2.491(11) . ?
Pb15 O1 2.757(12) . ?
Pb15 O3 2.839(11) 8_556 ?
Pb15 As1 3.683(2) . ?
Pb15 Pb14 3.7143(9) 6_556 ?
Pb16 O19 2.248(11) . ?
Pb16 O9 2.287(11) . ?
Pb16 O4 2.440(12) 8 ?
Pb16 Cl5 3.279(4) 3_545 ?
Pb16 Cl1 3.3231(7) 2_554 ?
Pb16 Cl3 3.468(5) 2_554 ?
Pb16 Si1 3.478(2) 6 ?
Pb16 As1 3.478(2) 6 ?
Pb16 Pb2 3.7677(11) 2_554 ?
Pb16 Pb12 3.8013(10) 3_545 ?
As1 O1 1.603(13) . ?
As1 O2 1.651(13) . ?
As1 O3 1.673(11) 3_545 ?
As1 O4 1.695(11) 3_545 ?
As1 Pb5 3.436(2) 3_545 ?
As1 Pb16 3.478(2) 6_556 ?
As1 Pb11 3.652(2) 6 ?
As2 O8A 1.64(3) . ?
As2 O6 1.654(13) . ?
As2 O7 1.68(2) . ?
As2 O5 1.728(19) . ?
As2 O8B 1.75(4) . ?
As2 Pb1 3.641(2) 5_565 ?
Cl1 Pb16 3.3231(7) 2_554 ?
Cl1 Pb16 3.3231(7) 8_456 ?
Cl1 Pb7 3.3232(7) 4_444 ?
Cl1 Pb7 3.3232(7) 6_566 ?
Cl1 Pb5 3.3476(7) 7_455 ?
Cl1 Pb2 3.3570(7) 7_455 ?
Cl2 Pb5 3.250(4) 8_556 ?
Cl3 Pb13 3.273(5) 6_565 ?
Cl3 Pb6 3.311(4) 2_554 ?
Cl3 Pb13 3.324(5) 5_565 ?
Cl3 Pb16 3.468(5) 2_554 ?
Cl4 Pb1 3.228(4) 2 ?
Cl4 Pb7 3.289(4) 6_566 ?
Cl5 Pb5 3.239(4) 4_454 ?
Cl5 Pb16 3.279(4) 3_455 ?
Cl5 Pb2 3.295(4) 4_454 ?
Cl5 Pb3 3.390(4) 5_565 ?
Cl5 Pb3 3.395(4) 3_455 ?
Cl5 Pb13 3.396(4) 7_465 ?
O1 Pb10 3.049(12) 2_554 ?
O2 Pb11 2.306(13) 5 ?
O2 Pb10 2.961(13) 5 ?
O3 Si1 1.673(11) 3_455 ?
O3 As1 1.673(11) 3_455 ?
O3 Pb11 2.359(10) 8_455 ?
O3 Pb15 2.839(11) 8_455 ?
O4 Si1 1.695(11) 3_455 ?
O4 As1 1.695(11) 3_455 ?
O4 Pb16 2.440(12) 8_456 ?
O4 Pb12 2.513(11) 6_566 ?
O5 Pb4 2.721(19) 2 ?
O5 Pb1 2.96(2) 5_565 ?
O6 Pb4 2.798(13) 6_565 ?
O6 Pb12 3.026(13) 6_566 ?
O7 Pb8 2.72(2) 6_565 ?
O7 Pb1 2.74(2) 5_565 ?
O8A O8B 1.59(5) . ?
O8A Pb3 2.41(3) 3_455 ?
O8A Pb9 2.96(3) 6_566 ?
O8B Pb3 2.66(4) 3_455 ?
O8B Pb14 2.83(4) 3_455 ?
O9 Pb7 2.239(11) 3_545 ?
O9 Pb12 2.380(12) 3_545 ?
O10 Pb4 2.207(11) 6_565 ?
O11 Pb12 2.253(10) 6_566 ?
O13 Pb10 2.204(7) 2_554 ?
O13 Pb6 2.363(8) 2_554 ?
O14 Pb7 2.281(11) 6_566 ?
O14 Pb12 2.313(10) 6_566 ?
O16 Pb5 2.269(12) 8_556 ?
O16 Pb9 2.393(11) 8_556 ?
O17 Pb13 2.265(11) 6_565 ?
O17 Pb4 2.292(10) 6_565 ?
O18 Pb1 2.279(8) 2 ?
O18 Pb8 2.382(8) 2 ?
O19 Pb10 2.302(10) 2_554 ?
O20 Pb13 2.260(8) 2 ?
O20 Pb4 2.388(9) 2 ?
 
loop_
 _geom_angle_atom_site_label_1
 _geom_angle_atom_site_label_2
 _geom_angle_atom_site_label_3
 _geom_angle
 _geom_angle_site_symmetry_1
 _geom_angle_site_symmetry_3
 _geom_angle_publ_flag
O18 Pb1 O10 78.5(3) . . ?
O18 Pb1 O7 76.7(5) . 5_565 ?
O10 Pb1 O7 103.5(5) . 5_565 ?
O18 Pb1 O5 110.7(5) . 5_565 ?
O10 Pb1 O5 71.3(5) . 5_565 ?
O7 Pb1 O5 53.7(6) 5_565 5_565 ?
O18 Pb1 Cl4 79.1(3) . . ?
O10 Pb1 Cl4 84.6(3) . . ?
O7 Pb1 Cl4 152.2(5) 5_565 . ?
O5 Pb1 Cl4 150.8(4) 5_565 . ?
O18 Pb1 Cl4 75.0(3) . 2 ?
O10 Pb1 Cl4 148.7(3) . 2 ?
O7 Pb1 Cl4 86.4(5) 5_565 2 ?
O5 Pb1 Cl4 134.1(4) 5_565 2 ?
Cl4 Pb1 Cl4 74.41(13) . 2 ?
O18 Pb1 Cl3 146.15(11) . . ?
O10 Pb1 Cl3 78.6(3) . . ?
O7 Pb1 Cl3 133.2(5) 5_565 . ?
O5 Pb1 Cl3 84.9(4) 5_565 . ?
Cl4 Pb1 Cl3 74.22(12) . . ?
Cl4 Pb1 Cl3 116.17(11) 2 . ?
O18 Pb1 Pb8 40.28(18) . . ?
O10 Pb1 Pb8 38.3(3) . . ?
O7 Pb1 Pb8 92.1(5) 5_565 . ?
O5 Pb1 Pb8 92.2(4) 5_565 . ?
Cl4 Pb1 Pb8 77.79(8) . . ?
Cl4 Pb1 Pb8 113.07(8) 2 . ?
Cl3 Pb1 Pb8 112.44(8) . . ?
O18 Pb1 As2 95.2(3) . 5_565 ?
O10 Pb1 As2 89.8(3) . 5_565 ?
O7 Pb1 As2 25.9(5) 5_565 5_565 ?
O5 Pb1 As2 28.0(4) 5_565 5_565 ?
Cl4 Pb1 As2 172.68(9) . 5_565 ?
Cl4 Pb1 As2 108.71(8) 2 5_565 ?
Cl3 Pb1 As2 109.35(9) . 5_565 ?
Pb8 Pb1 As2 94.90(4) . 5_565 ?
O18 Pb1 Pb11 124.6(3) . . ?
O10 Pb1 Pb11 128.1(3) . . ?
O7 Pb1 Pb11 125.7(5) 5_565 . ?
O5 Pb1 Pb11 123.3(4) 5_565 . ?
Cl4 Pb1 Pb11 60.43(8) . . ?
Cl4 Pb1 Pb11 59.47(8) 2 . ?
Cl3 Pb1 Pb11 56.72(8) . . ?
Pb8 Pb1 Pb11 138.18(2) . . ?
As2 Pb1 Pb11 126.89(4) 5_565 . ?
O18 Pb1 Pb1 33.3(3) . 2 ?
O10 Pb1 Pb1 98.5(3) . 2 ?
O7 Pb1 Pb1 97.4(5) 5_565 2 ?
O5 Pb1 Pb1 143.2(4) 5_565 2 ?
Cl4 Pb1 Pb1 54.86(8) . 2 ?
Cl4 Pb1 Pb1 50.37(8) 2 2 ?
Cl3 Pb1 Pb1 128.93(8) . 2 ?
Pb8 Pb1 Pb1 63.705(17) . 2 ?
As2 Pb1 Pb1 121.68(3) 5_565 2 ?
Pb11 Pb1 Pb1 91.303(13) . 2 ?
O18 Pb1 Pb2 92.33(2) . . ?
O10 Pb1 Pb2 36.5(3) . . ?
O7 Pb1 Pb2 139.9(5) 5_565 . ?
O5 Pb1 Pb2 97.3(4) 5_565 . ?
Cl4 Pb1 Pb2 54.01(8) . . ?
Cl4 Pb1 Pb2 128.39(8) 2 . ?
Cl3 Pb1 Pb2 55.05(8) . . ?
Pb8 Pb1 Pb2 58.590(17) . . ?
As2 Pb1 Pb2 122.32(3) 5_565 . ?
Pb11 Pb1 Pb2 92.484(18) . . ?
Pb1 Pb1 Pb2 93.00(3) 2 . ?
O14 Pb2 O11 72.8(3) . . ?
O14 Pb2 O10 73.4(4) . . ?
O11 Pb2 O10 113.8(3) . . ?
O14 Pb2 O17 114.5(3) . . ?
O11 Pb2 O17 72.3(3) . . ?
O10 Pb2 O17 72.8(3) . . ?
O14 Pb2 Cl4 75.2(3) . . ?
O11 Pb2 Cl4 140.4(3) . . ?
O10 Pb2 Cl4 77.7(3) . . ?
O17 Pb2 Cl4 143.9(2) . . ?
O14 Pb2 Cl5 144.7(3) . 4_444 ?
O11 Pb2 Cl5 80.2(2) . 4_444 ?
O10 Pb2 Cl5 140.0(3) . 4_444 ?
O17 Pb2 Cl5 77.0(3) . 4_444 ?
Cl4 Pb2 Cl5 116.25(10) . 4_444 ?
O14 Pb2 Cl1 81.8(3) . . ?
O11 Pb2 Cl1 76.7(2) . . ?
O10 Pb2 Cl1 147.7(3) . . ?
O17 Pb2 Cl1 137.8(2) . . ?
Cl4 Pb2 Cl1 76.31(8) . . ?
Cl5 Pb2 Cl1 70.03(8) 4_444 . ?
O14 Pb2 Cl3 138.1(2) . . ?
O11 Pb2 Cl3 147.1(3) . . ?
O10 Pb2 Cl3 75.5(3) . . ?
O17 Pb2 Cl3 81.6(3) . . ?
Cl4 Pb2 Cl3 71.22(12) . . ?
Cl5 Pb2 Cl3 74.62(10) 4_444 . ?
Cl1 Pb2 Cl3 113.00(8) . . ?
O14 Pb2 Pb8 35.5(2) . . ?
O11 Pb2 Pb8 91.9(2) . . ?
O10 Pb2 Pb8 37.9(3) . . ?
O17 Pb2 Pb8 93.7(2) . . ?
Cl4 Pb2 Pb8 74.49(8) . . ?
Cl5 Pb2 Pb8 169.23(8) 4_444 . ?
Cl1 Pb2 Pb8 115.44(2) . . ?
Cl3 Pb2 Pb8 109.77(7) . . ?
O14 Pb2 Pb9 92.6(3) . . ?
O11 Pb2 Pb9 36.5(2) . . ?
O10 Pb2 Pb9 91.9(2) . . ?
O17 Pb2 Pb9 35.9(2) . . ?
Cl4 Pb2 Pb9 165.71(8) . . ?
Cl5 Pb2 Pb9 78.01(8) 4_444 . ?
Cl1 Pb2 Pb9 109.75(2) . . ?
Cl3 Pb2 Pb9 115.97(8) . . ?
Pb8 Pb2 Pb9 91.28(2) . . ?
O14 Pb2 Pb4 92.5(3) . 6_565 ?
O11 Pb2 Pb4 92.8(2) . 6_565 ?
O10 Pb2 Pb4 35.4(2) . 6_565 ?
O17 Pb2 Pb4 37.5(2) . 6_565 ?
Cl4 Pb2 Pb4 111.33(8) . 6_565 ?
Cl5 Pb2 Pb4 111.40(8) 4_444 6_565 ?
Cl1 Pb2 Pb4 169.09(2) . 6_565 ?
Cl3 Pb2 Pb4 77.42(8) . 6_565 ?
Pb8 Pb2 Pb4 61.373(19) . 6_565 ?
Pb9 Pb2 Pb4 61.012(18) . 6_565 ?
O14 Pb2 Pb12 37.0(2) . 6_566 ?
O11 Pb2 Pb12 35.8(2) . 6_566 ?
O10 Pb2 Pb12 93.7(3) . 6_566 ?
O17 Pb2 Pb12 92.8(3) . 6_566 ?
Cl4 Pb2 Pb12 109.59(8) . 6_566 ?
Cl5 Pb2 Pb12 113.51(7) 4_444 6_566 ?
Cl1 Pb2 Pb12 77.52(2) . 6_566 ?
Cl3 Pb2 Pb12 168.95(7) . 6_566 ?
Pb8 Pb2 Pb12 60.889(18) . 6_566 ?
Pb9 Pb2 Pb12 60.841(19) . 6_566 ?
Pb4 Pb2 Pb12 92.30(2) 6_565 6_566 ?
O16 Pb3 O15 80.3(4) . . ?
O16 Pb3 O8A 78.9(9) . 3_545 ?
O15 Pb3 O8A 93.0(8) . 3_545 ?
O16 Pb3 O8B 104.8(9) . 3_545 ?
O15 Pb3 O8B 73.3(8) . 3_545 ?
O8A Pb3 O8B 36.1(10) 3_545 3_545 ?
O16 Pb3 Cl2 79.5(3) . . ?
O15 Pb3 Cl2 83.5(3) . . ?
O8A Pb3 Cl2 158.4(8) 3_545 . ?
O8B Pb3 Cl2 155.0(8) 3_545 . ?
O16 Pb3 Cl5 77.6(3) . 5_565 ?
O15 Pb3 Cl5 151.4(3) . 5_565 ?
O8A Pb3 Cl5 100.3(8) 3_545 5_565 ?
O8B Pb3 Cl5 130.1(8) 3_545 5_565 ?
Cl2 Pb3 Cl5 74.85(11) . 5_565 ?
O16 Pb3 Cl5 150.6(3) . 3_545 ?
O15 Pb3 Cl5 79.6(3) . 3_545 ?
O8A Pb3 Cl5 123.4(8) 3_545 3_545 ?
O8B Pb3 Cl5 89.7(8) 3_545 3_545 ?
Cl2 Pb3 Cl5 77.13(12) . 3_545 ?
Cl5 Pb3 Cl5 112.53(8) 5_565 3_545 ?
O16 Pb3 Pb15 42.5(3) . . ?
O15 Pb3 Pb15 37.9(3) . . ?
O8A Pb3 Pb15 87.9(8) 3_545 . ?
O8B Pb3 Pb15 90.3(8) 3_545 . ?
Cl2 Pb3 Pb15 76.17(9) . . ?
Cl5 Pb3 Pb15 116.90(8) 5_565 . ?
Cl5 Pb3 Pb15 113.67(7) 3_545 . ?
O16 Pb3 Pb3 126.3(3) . 7 ?
O15 Pb3 Pb3 128.9(3) . 7 ?
O8A Pb3 Pb3 131.0(8) 3_545 7 ?
O8B Pb3 Pb3 125.1(8) 3_545 7 ?
Cl2 Pb3 Pb3 64.16(9) . 7 ?
Cl5 Pb3 Pb3 56.33(7) 5_565 7 ?
Cl5 Pb3 Pb3 56.21(7) 3_545 7 ?
Pb15 Pb3 Pb3 140.24(3) . 7 ?
O16 Pb3 Pb5 32.8(3) . 8_556 ?
O15 Pb3 Pb5 99.1(3) . 8_556 ?
O8A Pb3 Pb5 104.5(8) 3_545 8_556 ?
O8B Pb3 Pb5 136.3(8) 3_545 8_556 ?
Cl2 Pb3 Pb5 55.40(9) . 8_556 ?
Cl5 Pb3 Pb5 53.15(8) 5_565 8_556 ?
Cl5 Pb3 Pb5 132.12(8) 3_545 8_556 ?
Pb15 Pb3 Pb5 64.157(18) . 8_556 ?
Pb3 Pb3 Pb5 93.70(2) 7 8_556 ?
O16 Pb3 Pb6 94.6(3) . . ?
O15 Pb3 Pb6 34.9(3) . . ?
O8A Pb3 Pb6 127.2(8) 3_545 . ?
O8B Pb3 Pb6 100.0(8) 3_545 . ?
Cl2 Pb3 Pb6 55.02(8) . . ?
Cl5 Pb3 Pb6 129.78(7) 5_565 . ?
Cl5 Pb3 Pb6 57.26(7) 3_545 . ?
Pb15 Pb3 Pb6 57.546(17) . . ?
Pb3 Pb3 Pb6 95.07(2) 7 . ?
Pb5 Pb3 Pb6 95.04(2) 8_556 . ?
O16 Pb3 Pb9 33.5(3) . 8_556 ?
O15 Pb3 Pb9 97.1(3) . 8_556 ?
O8A Pb3 Pb9 49.0(8) 3_545 8_556 ?
O8B Pb3 Pb9 82.2(8) 3_545 8_556 ?
Cl2 Pb3 Pb9 110.07(9) . 8_556 ?
Cl5 Pb3 Pb9 73.78(7) 5_565 8_556 ?
Cl5 Pb3 Pb9 171.86(8) 3_545 8_556 ?
Pb15 Pb3 Pb9 65.785(18) . 8_556 ?
Pb3 Pb3 Pb9 129.83(2) 7 8_556 ?
Pb5 Pb3 Pb9 55.590(18) 8_556 8_556 ?
Pb6 Pb3 Pb9 123.26(2) . 8_556 ?
O10 Pb4 O17 81.3(4) 6_566 6_566 ?
O10 Pb4 O20 107.5(4) 6_566 . ?
O17 Pb4 O20 75.2(3) 6_566 . ?
O10 Pb4 O5 77.3(5) 6_566 2 ?
O17 Pb4 O5 128.7(5) 6_566 2 ?
O20 Pb4 O5 67.9(4) . 2 ?
O10 Pb4 O6 75.7(4) 6_566 6_566 ?
O17 Pb4 O6 74.9(4) 6_566 6_566 ?
O20 Pb4 O6 149.0(3) . 6_566 ?
O5 Pb4 O6 140.2(5) 2 6_566 ?
O10 Pb4 Pb13 95.0(3) 6_566 . ?
O17 Pb4 Pb13 37.4(3) 6_566 . ?
O20 Pb4 Pb13 37.82(15) . . ?
O5 Pb4 Pb13 99.0(4) 2 . ?
O6 Pb4 Pb13 112.0(2) 6_566 . ?
O10 Pb4 Pb2 40.2(3) 6_566 6_566 ?
O17 Pb4 Pb2 41.2(3) 6_566 6_566 ?
O20 Pb4 Pb2 93.8(3) . 6_566 ?
O5 Pb4 Pb2 106.7(4) 2 6_566 ?
O6 Pb4 Pb2 68.4(3) 6_566 6_566 ?
Pb13 Pb4 Pb2 63.906(19) . 6_566 ?
O10 Pb4 Pb8 155.4(3) 6_566 . ?
O17 Pb4 Pb8 87.6(3) 6_566 . ?
O20 Pb4 Pb8 90.6(3) . . ?
O5 Pb4 Pb8 126.0(4) 2 . ?
O6 Pb4 Pb8 80.2(3) 6_566 . ?
Pb13 Pb4 Pb8 89.25(2) . . ?
Pb2 Pb4 Pb8 124.30(2) 6_566 . ?
O10 Pb4 Pb9 94.8(3) 6_566 6_566 ?
O17 Pb4 Pb9 33.4(3) 6_566 6_566 ?
O20 Pb4 Pb9 99.98(4) . 6_566 ?
O5 Pb4 Pb9 162.0(4) 2 6_566 ?
O6 Pb4 Pb9 49.3(2) 6_566 6_566 ?
Pb13 Pb4 Pb9 65.286(18) . 6_566 ?
Pb2 Pb4 Pb9 59.490(18) 6_566 6_566 ?
Pb8 Pb4 Pb9 65.059(18) . 6_566 ?
O10 Pb4 Pb8 34.3(3) 6_566 6_566 ?
O17 Pb4 Pb8 94.8(3) 6_566 6_566 ?
O20 Pb4 Pb8 141.7(3) . 6_566 ?
O5 Pb4 Pb8 93.0(4) 2 6_566 ?
O6 Pb4 Pb8 49.6(3) 6_566 6_566 ?
Pb13 Pb4 Pb8 122.83(2) . 6_566 ?
Pb2 Pb4 Pb8 59.108(17) 6_566 6_566 ?
Pb8 Pb4 Pb8 126.37(2) . 6_566 ?
Pb9 Pb4 Pb8 89.11(2) 6_566 6_566 ?
O10 Pb4 Pb8 130.9(3) 6_566 2 ?
O17 Pb4 Pb8 147.7(3) 6_566 2 ?
O20 Pb4 Pb8 90.1(3) . 2 ?
O5 Pb4 Pb8 67.4(4) 2 2 ?
O6 Pb4 Pb8 111.4(3) 6_566 2 ?
Pb13 Pb4 Pb8 122.74(2) . 2 ?
Pb2 Pb4 Pb8 171.09(2) 6_566 2 ?
Pb8 Pb4 Pb8 63.57(2) . 2 ?
Pb9 Pb4 Pb8 127.63(2) 6_566 2 ?
Pb8 Pb4 Pb8 113.506(19) 6_566 2 ?
O10 Pb4 Pb4 142.7(3) 6_566 2 ?
O17 Pb4 Pb4 94.7(3) 6_566 2 ?
O20 Pb4 Pb4 37.1(3) . 2 ?
O5 Pb4 Pb4 76.7(4) 2 2 ?
O6 Pb4 Pb4 139.2(3) 6_566 2 ?
Pb13 Pb4 Pb4 63.520(18) . 2 ?
Pb2 Pb4 Pb4 127.155(18) 6_566 2 ?
Pb8 Pb4 Pb4 59.759(18) . 2 ?
Pb9 Pb4 Pb4 101.94(3) 6_566 2 ?
Pb8 Pb4 Pb4 168.95(3) 6_566 2 ?
Pb8 Pb4 Pb4 59.233(16) 2 2 ?
O16 Pb5 O11 77.9(4) 8_455 . ?
O16 Pb5 O3 81.1(4) 8_455 . ?
O11 Pb5 O3 110.9(3) . . ?
O16 Pb5 O4 110.6(4) 8_455 . ?
O11 Pb5 O4 70.3(4) . . ?
O3 Pb5 O4 57.6(3) . . ?
O16 Pb5 Cl5 80.8(3) 8_455 4_444 ?
O11 Pb5 Cl5 83.6(3) . 4_444 ?
O3 Pb5 Cl5 153.7(2) . 4_444 ?
O4 Pb5 Cl5 147.8(2) . 4_444 ?
O16 Pb5 Cl2 74.4(3) 8_455 8_455 ?
O11 Pb5 Cl2 146.8(3) . 8_455 ?
O3 Pb5 Cl2 82.7(2) . 8_455 ?
O4 Pb5 Cl2 137.3(2) . 8_455 ?
Cl5 Pb5 Cl2 74.15(10) 4_444 8_455 ?
O16 Pb5 Cl1 144.9(3) 8_455 . ?
O11 Pb5 Cl1 78.8(3) . . ?
O3 Pb5 Cl1 132.1(2) . . ?
O4 Pb5 Cl1 85.5(2) . . ?
Cl5 Pb5 Cl1 70.80(8) 4_444 . ?
Cl2 Pb5 Cl1 115.25(8) 8_455 . ?
O16 Pb5 Si1 97.9(3) 8_455 3_455 ?
O11 Pb5 Si1 92.2(3) . 3_455 ?
O3 Pb5 Si1 28.5(2) . 3_455 ?
O4 Pb5 Si1 29.2(2) . 3_455 ?
Cl5 Pb5 Si1 175.79(8) 4_444 3_455 ?
Cl2 Pb5 Si1 109.39(9) 8_455 3_455 ?
Cl1 Pb5 Si1 108.99(4) . 3_455 ?
O16 Pb5 As1 97.9(3) 8_455 3_455 ?
O11 Pb5 As1 92.2(3) . 3_455 ?
O3 Pb5 As1 28.5(2) . 3_455 ?
O4 Pb5 As1 29.2(2) . 3_455 ?
Cl5 Pb5 As1 175.79(8) 4_444 3_455 ?
Cl2 Pb5 As1 109.39(9) 8_455 3_455 ?
Cl1 Pb5 As1 108.99(4) . 3_455 ?
Si1 Pb5 As1 0.00(10) 3_455 3_455 ?
O16 Pb5 Pb9 40.7(3) 8_455 . ?
O11 Pb5 Pb9 37.3(3) . . ?
O3 Pb5 Pb9 98.2(2) . . ?
O4 Pb5 Pb9 89.6(3) . . ?
Cl5 Pb5 Pb9 80.03(8) 4_444 . ?
Cl2 Pb5 Pb9 113.02(9) 8_455 . ?
Cl1 Pb5 Pb9 112.141(19) . . ?
Si1 Pb5 Pb9 96.32(4) 3_455 . ?
As1 Pb5 Pb9 96.32(4) 3_455 . ?
O16 Pb5 Pb7 123.0(3) 8_455 4_444 ?
O11 Pb5 Pb7 125.4(3) . 4_444 ?
O3 Pb5 Pb7 121.3(2) . 4_444 ?
O4 Pb5 Pb7 125.9(3) . 4_444 ?
Cl5 Pb5 Pb7 56.32(8) 4_444 4_444 ?
Cl2 Pb5 Pb7 59.96(8) 8_455 4_444 ?
Cl1 Pb5 Pb7 55.289(14) . 4_444 ?
Si1 Pb5 Pb7 127.23(4) 3_455 4_444 ?
As1 Pb5 Pb7 127.23(4) 3_455 4_444 ?
Pb9 Pb5 Pb7 136.32(2) . 4_444 ?
O16 Pb5 Pb3 32.5(3) 8_455 8_455 ?
O11 Pb5 Pb3 97.0(3) . 8_455 ?
O3 Pb5 Pb3 98.6(2) . 8_455 ?
O4 Pb5 Pb3 142.6(3) . 8_455 ?
Cl5 Pb5 Pb3 56.86(8) 4_444 8_455 ?
Cl2 Pb5 Pb3 50.13(9) 8_455 8_455 ?
Cl1 Pb5 Pb3 127.58(2) . 8_455 ?
Si1 Pb5 Pb3 123.42(4) 3_455 8_455 ?
As1 Pb5 Pb3 123.42(4) 3_455 8_455 ?
Pb9 Pb5 Pb3 63.841(19) . 8_455 ?
Pb7 Pb5 Pb3 90.46(2) 4_444 8_455 ?
O13 Pb6 O12 73.8(3) . . ?
O13 Pb6 O15 112.9(3) . . ?
O12 Pb6 O15 75.6(3) . . ?
O13 Pb6 O19 71.0(2) . . ?
O12 Pb6 O19 116.6(3) . . ?
O15 Pb6 O19 72.2(3) . . ?
O13 Pb6 Cl2 142.08(9) . . ?
O12 Pb6 Cl2 73.0(3) . . ?
O15 Pb6 Cl2 75.6(3) . . ?
O19 Pb6 Cl2 142.0(2) . . ?
O13 Pb6 Cl3 83.2(2) . 2_554 ?
O12 Pb6 Cl3 144.4(2) . 2_554 ?
O15 Pb6 Cl3 139.5(3) . 2_554 ?
O19 Pb6 Cl3 79.4(2) . 2_554 ?
Cl2 Pb6 Cl3 115.10(11) . 2_554 ?
O13 Pb6 Cl3 82.2(2) . . ?
O12 Pb6 Cl3 78.6(3) . . ?
O15 Pb6 Cl3 144.5(3) . . ?
O19 Pb6 Cl3 142.4(2) . . ?
Cl2 Pb6 Cl3 73.73(11) . . ?
Cl3 Pb6 Cl3 71.58(15) 2_554 . ?
O13 Pb6 Pb15 91.2(2) . . ?
O12 Pb6 Pb15 37.3(2) . . ?
O15 Pb6 Pb15 38.5(3) . . ?
O19 Pb6 Pb15 93.2(2) . . ?
Cl2 Pb6 Pb15 72.91(8) . . ?
Cl3 Pb6 Pb15 171.82(8) 2_554 . ?
Cl3 Pb6 Pb15 113.64(8) . . ?
O13 Pb6 Pb14 90.0(2) . . ?
O12 Pb6 Pb14 94.3(3) . . ?
O15 Pb6 Pb14 35.8(2) . . ?
O19 Pb6 Pb14 36.6(2) . . ?
Cl2 Pb6 Pb14 110.26(8) . . ?
Cl3 Pb6 Pb14 112.76(9) 2_554 . ?
Cl3 Pb6 Pb14 170.64(8) . . ?
Pb15 Pb6 Pb14 61.126(19) . . ?
O13 Pb6 Pb10 34.24(13) . . ?
O12 Pb6 Pb10 39.6(2) . . ?
O15 Pb6 Pb10 95.1(2) . . ?
O19 Pb6 Pb10 91.4(2) . . ?
Cl2 Pb6 Pb10 111.15(9) . . ?
Cl3 Pb6 Pb10 114.14(8) 2_554 . ?
Cl3 Pb6 Pb10 79.65(8) . . ?
Pb15 Pb6 Pb10 62.202(19) . . ?
Pb14 Pb6 Pb10 90.99(2) . . ?
O13 Pb6 Pb13 126.4(3) . 5_565 ?
O12 Pb6 Pb13 120.6(3) . 5_565 ?
O15 Pb6 Pb13 120.6(2) . 5_565 ?
O19 Pb6 Pb13 122.9(2) . 5_565 ?
Cl2 Pb6 Pb13 60.11(8) . 5_565 ?
Cl3 Pb6 Pb13 55.00(8) 2_554 5_565 ?
Cl3 Pb6 Pb13 55.64(7) . 5_565 ?
Pb15 Pb6 Pb13 133.00(2) . 5_565 ?
Pb14 Pb6 Pb13 133.71(2) . 5_565 ?
Pb10 Pb6 Pb13 135.29(2) . 5_565 ?
O13 Pb6 Pb10 33.75(12) . 2_554 ?
O12 Pb6 Pb10 94.5(2) . 2_554 ?
O15 Pb6 Pb10 93.6(2) . 2_554 ?
O19 Pb6 Pb10 37.2(2) . 2_554 ?
Cl2 Pb6 Pb10 165.04(8) . 2_554 ?
Cl3 Pb6 Pb10 79.84(8) 2_554 2_554 ?
Cl3 Pb6 Pb10 112.50(7) . 2_554 ?
Pb15 Pb6 Pb10 92.18(2) . 2_554 ?
Pb14 Pb6 Pb10 61.559(19) . 2_554 ?
Pb10 Pb6 Pb10 58.78(2) . 2_554 ?
Pb13 Pb6 Pb10 134.82(2) 5_565 2_554 ?
O9 Pb7 O14 78.0(4) 3_455 6_565 ?
O9 Pb7 O7 105.3(6) 3_455 . ?
O14 Pb7 O7 73.5(6) 6_565 . ?
O9 Pb7 O8B 75.0(8) 3_455 . ?
O14 Pb7 O8B 105.2(9) 6_565 . ?
O7 Pb7 O8B 50.3(9) . . ?
O9 Pb7 Cl4 145.3(3) 3_455 6_565 ?
O14 Pb7 Cl4 75.4(3) 6_565 6_565 ?
O7 Pb7 Cl4 88.1(5) . 6_565 ?
O8B Pb7 Cl4 133.6(7) . 6_565 ?
O9 Pb7 Cl1 79.4(3) 3_455 4_454 ?
O14 Pb7 Cl1 84.1(3) 6_565 4_454 ?
O7 Pb7 Cl1 155.3(5) . 4_454 ?
O8B Pb7 Cl1 150.1(7) . 4_454 ?
Cl4 Pb7 Cl1 76.07(7) 6_565 4_454 ?
O9 Pb7 Cl5 77.1(3) 3_455 . ?
O14 Pb7 Cl5 146.7(3) 6_565 . ?
O7 Pb7 Cl5 134.8(5) . . ?
O8B Pb7 Cl5 89.3(8) . . ?
Cl4 Pb7 Cl5 115.90(11) 6_565 . ?
Cl1 Pb7 Cl5 69.89(8) 4_454 . ?
O9 Pb7 Pb12 39.8(3) 3_455 . ?
O14 Pb7 Pb12 38.2(3) 6_565 . ?
O7 Pb7 Pb12 89.0(5) . . ?
O8B Pb7 Pb12 90.5(8) . . ?
Cl4 Pb7 Pb12 110.76(8) 6_565 . ?
Cl1 Pb7 Pb12 79.34(2) 4_454 . ?
Cl5 Pb7 Pb12 113.89(7) . . ?
O9 Pb7 As2 95.9(3) 3_455 . ?
O14 Pb7 As2 92.8(3) 6_565 . ?
O7 Pb7 As2 24.2(5) . . ?
O8B Pb7 As2 27.4(7) . . ?
Cl4 Pb7 As2 107.20(8) 6_565 . ?
Cl1 Pb7 As2 174.84(4) 4_454 . ?
Cl5 Pb7 As2 111.40(8) . . ?
Pb12 Pb7 As2 95.68(4) . . ?
O9 Pb7 Pb5 120.9(3) 3_455 4_454 ?
O14 Pb7 Pb5 126.2(3) 6_565 4_454 ?
O7 Pb7 Pb5 131.8(5) . 4_454 ?
O8B Pb7 Pb5 127.7(8) . 4_454 ?
Cl4 Pb7 Pb5 62.10(8) 6_565 4_454 ?
Cl1 Pb7 Pb5 55.902(15) 4_454 4_454 ?
Cl5 Pb7 Pb5 53.80(8) . 4_454 ?
Pb12 Pb7 Pb5 135.24(2) . 4_454 ?
As2 Pb7 Pb5 129.06(4) . 4_454 ?
O9 Pb7 Pb2 92.6(3) 3_455 6_565 ?
O14 Pb7 Pb2 35.2(3) 6_565 6_565 ?
O7 Pb7 Pb2 100.2(5) . 6_565 ?
O8B Pb7 Pb2 140.4(8) . 6_565 ?
Cl4 Pb7 Pb2 53.14(8) 6_565 6_565 ?
Cl1 Pb7 Pb2 55.153(16) 4_454 6_565 ?
Cl5 Pb7 Pb2 125.03(8) . 6_565 ?
Pb12 Pb7 Pb2 59.568(18) . 6_565 ?
As2 Pb7 Pb2 123.40(4) . 6_565 ?
Pb5 Pb7 Pb2 91.146(19) 4_454 6_565 ?
O9 Pb7 Pb8 95.7(3) 3_455 6_565 ?
O14 Pb7 Pb8 30.3(2) 6_565 6_565 ?
O7 Pb7 Pb8 44.5(5) . 6_565 ?
O8B Pb7 Pb8 86.6(8) . 6_565 ?
Cl4 Pb7 Pb8 71.31(8) 6_565 6_565 ?
Cl1 Pb7 Pb8 111.42(2) 4_454 6_565 ?
Cl5 Pb7 Pb8 172.51(8) . 6_565 ?
Pb12 Pb7 Pb8 59.946(19) . 6_565 ?
As2 Pb7 Pb8 66.63(3) . 6_565 ?
Pb5 Pb7 Pb8 133.34(2) 4_454 6_565 ?
Pb2 Pb7 Pb8 56.858(16) 6_565 6_565 ?
O14 Pb8 O10 79.7(4) . . ?
O14 Pb8 O18 110.3(4) . . ?
O10 Pb8 O18 76.0(3) . . ?
O14 Pb8 O7 71.3(5) . 6_566 ?
O10 Pb8 O7 128.5(6) . 6_566 ?
O18 Pb8 O7 75.6(5) . 6_566 ?
O14 Pb8 O6 76.3(4) . . ?
O10 Pb8 O6 72.6(4) . . ?
O18 Pb8 O6 146.1(3) . . ?
O7 Pb8 O6 135.3(5) 6_566 . ?
O14 Pb8 Pb1 94.6(3) . . ?
O10 Pb8 Pb1 37.8(2) . . ?
O18 Pb8 Pb1 38.21(16) . . ?
O7 Pb8 Pb1 102.7(5) 6_566 . ?
O6 Pb8 Pb1 109.9(3) . . ?
O14 Pb8 Pb2 38.7(3) . . ?
O10 Pb8 Pb2 41.1(3) . . ?
O18 Pb8 Pb2 96.0(3) . . ?
O7 Pb8 Pb2 101.6(5) 6_566 . ?
O6 Pb8 Pb2 67.9(2) . . ?
Pb1 Pb8 Pb2 64.502(19) . . ?
O14 Pb8 Pb4 134.0(3) . . ?
O10 Pb8 Pb4 146.2(3) . . ?
O18 Pb8 Pb4 87.0(3) . . ?
O7 Pb8 Pb4 72.6(5) 6_566 . ?
O6 Pb8 Pb4 112.8(3) . . ?
Pb1 Pb8 Pb4 120.68(2) . . ?
Pb2 Pb8 Pb4 172.66(3) . . ?
O14 Pb8 Pb12 35.0(3) . 6_566 ?
O10 Pb8 Pb12 95.8(2) . 6_566 ?
O18 Pb8 Pb12 145.0(3) . 6_566 ?
O7 Pb8 Pb12 84.2(4) 6_566 6_566 ?
O6 Pb8 Pb12 52.3(2) . 6_566 ?
Pb1 Pb8 Pb12 124.41(2) . 6_566 ?
Pb2 Pb8 Pb12 60.123(17) . 6_566 ?
Pb4 Pb8 Pb12 114.05(2) . 6_566 ?
O14 Pb8 Pb4 93.6(3) . 6_565 ?
O10 Pb8 Pb4 32.7(3) . 6_565 ?
O18 Pb8 Pb4 98.56(4) . 6_565 ?
O7 Pb8 Pb4 160.0(5) 6_566 6_565 ?
O6 Pb8 Pb4 47.6(3) . 6_565 ?
Pb1 Pb8 Pb4 64.508(18) . 6_565 ?
Pb2 Pb8 Pb4 59.519(18) . 6_565 ?
Pb4 Pb8 Pb4 126.73(2) . 6_565 ?
Pb12 Pb8 Pb4 90.78(2) 6_566 6_565 ?
O14 Pb8 Pb4 156.1(3) . 2 ?
O10 Pb8 Pb4 88.6(3) . 2 ?
O18 Pb8 Pb4 86.5(3) . 2 ?
O7 Pb8 Pb4 131.0(5) 6_566 2 ?
O6 Pb8 Pb4 80.4(2) . 2 ?
Pb1 Pb8 Pb4 88.57(2) . 2 ?
Pb2 Pb8 Pb4 125.74(2) . 2 ?
Pb4 Pb8 Pb4 61.01(2) . 2 ?
Pb12 Pb8 Pb4 127.80(2) 6_566 2 ?
Pb4 Pb8 Pb4 66.494(19) 6_565 2 ?
O14 Pb8 Pb7 31.2(3) . 6_566 ?
O10 Pb8 Pb7 97.2(3) . 6_566 ?
O18 Pb8 Pb7 90.0(2) . 6_566 ?
O7 Pb8 Pb7 41.4(5) 6_566 6_566 ?
O6 Pb8 Pb7 106.1(2) . 6_566 ?
Pb1 Pb8 Pb7 92.93(2) . 6_566 ?
Pb2 Pb8 Pb7 61.398(18) . 6_566 ?
Pb4 Pb8 Pb7 112.03(2) . 6_566 ?
Pb12 Pb8 Pb7 56.771(18) 6_566 6_566 ?
Pb4 Pb8 Pb7 120.84(2) 6_565 6_566 ?
Pb4 Pb8 Pb7 172.35(2) 2 6_566 ?
O17 Pb9 O11 80.6(4) . . ?
O17 Pb9 O16 110.0(4) . 8_455 ?
O11 Pb9 O16 75.9(4) . 8_455 ?
O17 Pb9 O6 74.4(4) . . ?
O11 Pb9 O6 75.9(4) . . ?
O16 Pb9 O6 150.2(4) 8_455 . ?
O17 Pb9 O8A 81.6(7) . 6_565 ?
O11 Pb9 O8A 129.0(7) . 6_565 ?
O16 Pb9 O8A 66.2(7) 8_455 6_565 ?
O6 Pb9 O8A 142.0(7) . 6_565 ?
O17 Pb9 Pb5 96.4(3) . . ?
O11 Pb9 Pb5 37.7(2) . . ?
O16 Pb9 Pb5 38.1(3) 8_455 . ?
O6 Pb9 Pb5 113.1(3) . . ?
O8A Pb9 Pb5 98.4(6) 6_565 . ?
O17 Pb9 Pb12 131.5(3) . . ?
O11 Pb9 Pb12 147.5(2) . . ?
O16 Pb9 Pb12 86.1(3) 8_455 . ?
O6 Pb9 Pb12 113.6(3) . . ?
O8A Pb9 Pb12 63.1(6) 6_565 . ?
Pb5 Pb9 Pb12 119.61(2) . . ?
O17 Pb9 Pb2 40.8(3) . . ?
O11 Pb9 Pb2 39.9(2) . . ?
O16 Pb9 Pb2 95.7(3) 8_455 . ?
O6 Pb9 Pb2 67.8(3) . . ?
O8A Pb9 Pb2 110.7(6) 6_565 . ?
Pb5 Pb9 Pb2 64.804(19) . . ?
Pb12 Pb9 Pb2 172.23(3) . . ?
O17 Pb9 Pb14 158.6(3) . 3_455 ?
O11 Pb9 Pb14 87.5(3) . 3_455 ?
O16 Pb9 Pb14 83.9(3) 8_455 3_455 ?
O6 Pb9 Pb14 85.5(2) . 3_455 ?
O8A Pb9 Pb14 119.5(6) 6_565 3_455 ?
Pb5 Pb9 Pb14 84.55(2) . 3_455 ?
Pb12 Pb9 Pb14 63.47(2) . 3_455 ?
Pb2 Pb9 Pb14 124.19(2) . 3_455 ?
O17 Pb9 Pb4 34.5(3) . 6_565 ?
O11 Pb9 Pb4 94.3(2) . 6_565 ?
O16 Pb9 Pb4 144.4(3) 8_455 6_565 ?
O6 Pb9 Pb4 47.8(3) . 6_565 ?
O8A Pb9 Pb4 97.1(6) 6_565 6_565 ?
Pb5 Pb9 Pb4 124.16(2) . 6_565 ?
Pb12 Pb9 Pb4 115.30(2) . 6_565 ?
Pb2 Pb9 Pb4 59.498(17) . 6_565 ?
Pb14 Pb9 Pb4 130.50(3) 3_455 6_565 ?
O17 Pb9 Pb12 96.3(3) . 6_566 ?
O11 Pb9 Pb12 33.6(3) . 6_566 ?
O16 Pb9 Pb12 98.0(3) 8_455 6_566 ?
O6 Pb9 Pb12 52.3(3) . 6_566 ?
O8A Pb9 Pb12 161.8(6) 6_565 6_566 ?
Pb5 Pb9 Pb12 63.763(18) . 6_566 ?
Pb12 Pb9 Pb12 127.35(2) . 6_566 ?
Pb2 Pb9 Pb12 59.944(19) . 6_566 ?
Pb14 Pb9 Pb12 64.878(18) 3_455 6_566 ?
Pb4 Pb9 Pb12 90.89(2) 6_565 6_566 ?
O17 Pb9 Pb3 88.7(3) . 8_455 ?
O11 Pb9 Pb3 94.3(3) . 8_455 ?
O16 Pb9 Pb3 31.3(3) 8_455 8_455 ?
O6 Pb9 Pb3 161.5(2) . 8_455 ?
O8A Pb9 Pb3 37.9(6) 6_565 8_455 ?
Pb5 Pb9 Pb3 60.569(19) . 8_455 ?
Pb12 Pb9 Pb3 83.09(2) . 8_455 ?
Pb2 Pb9 Pb3 94.54(2) . 8_455 ?
Pb14 Pb9 Pb3 109.94(2) 3_455 8_455 ?
Pb4 Pb9 Pb3 119.18(2) 6_565 8_455 ?
Pb12 Pb9 Pb3 124.32(2) 6_566 8_455 ?
O13 Pb10 O19 78.4(3) . 2_554 ?
O13 Pb10 O12 76.5(3) . . ?
O19 Pb10 O12 110.2(3) 2_554 . ?
O13 Pb10 O2 125.6(4) . 5 ?
O19 Pb10 O2 79.2(4) 2_554 5 ?
O12 Pb10 O2 66.1(4) . 5 ?
O13 Pb10 O1 72.7(3) . . ?
O19 Pb10 O1 149.5(4) 2_554 . ?
O12 Pb10 O1 72.2(3) . . ?
O2 Pb10 O1 125.9(3) 5 . ?
O13 Pb10 O1 72.6(3) . 2_554 ?
O19 Pb10 O1 70.5(3) 2_554 2_554 ?
O12 Pb10 O1 148.3(4) . 2_554 ?
O2 Pb10 O1 140.5(3) 5 2_554 ?
O1 Pb10 O1 91.7(4) . 2_554 ?
O13 Pb10 Pb10 149.53(9) . 5 ?
O19 Pb10 Pb10 130.9(3) 2_554 5 ?
O12 Pb10 Pb10 83.9(2) . 5 ?
O2 Pb10 Pb10 63.8(3) 5 5 ?
O1 Pb10 Pb10 79.3(2) . 5 ?
O1 Pb10 Pb10 120.6(2) 2_554 5 ?
O13 Pb10 Pb10 34.0(3) . 2_554 ?
O19 Pb10 Pb10 96.9(3) 2_554 2_554 ?
O12 Pb10 Pb10 96.4(2) . 2_554 ?
O2 Pb10 Pb10 158.7(3) 5 2_554 ?
O1 Pb10 Pb10 53.2(2) . 2_554 ?
O1 Pb10 Pb10 53.1(3) 2_554 2_554 ?
Pb10 Pb10 Pb10 128.99(3) 5 2_554 ?
O13 Pb10 Pb6 37.10(15) . . ?
O19 Pb10 Pb6 96.2(3) 2_554 . ?
O12 Pb10 Pb6 39.5(2) . . ?
O2 Pb10 Pb6 98.4(3) 5 . ?
O1 Pb10 Pb6 65.8(2) . . ?
O1 Pb10 Pb6 109.1(3) 2_554 . ?
Pb10 Pb10 Pb6 119.09(3) 5 . ?
Pb10 Pb10 Pb6 60.936(17) 2_554 . ?
O13 Pb10 Pb6 36.56(15) . 2_554 ?
O19 Pb10 Pb6 41.8(3) 2_554 2_554 ?
O12 Pb10 Pb6 93.4(2) . 2_554 ?
O2 Pb10 Pb6 106.8(3) 5 2_554 ?
O1 Pb10 Pb6 108.7(2) . 2_554 ?
O1 Pb10 Pb6 65.4(2) 2_554 2_554 ?
Pb10 Pb10 Pb6 170.53(3) 5 2_554 ?
Pb10 Pb10 Pb6 60.288(18) 2_554 2_554 ?
Pb6 Pb10 Pb6 61.81(2) . 2_554 ?
O13 Pb10 Pb14 89.39(2) . 2_554 ?
O19 Pb10 Pb14 32.5(3) 2_554 2_554 ?
O12 Pb10 Pb14 142.7(2) . 2_554 ?
O2 Pb10 Pb14 97.1(2) 5 2_554 ?
O1 Pb10 Pb14 136.4(2) . 2_554 ?
O1 Pb10 Pb14 44.7(2) 2_554 2_554 ?
Pb10 Pb10 Pb14 119.66(3) 5 2_554 ?
Pb10 Pb10 Pb14 89.98(3) 2_554 2_554 ?
Pb6 Pb10 Pb14 120.13(2) . 2_554 ?
Pb6 Pb10 Pb14 58.338(17) 2_554 2_554 ?
O13 Pb10 Pb15 89.74(3) . . ?
O19 Pb10 Pb15 144.4(3) 2_554 . ?
O12 Pb10 Pb15 34.3(2) . . ?
O2 Pb10 Pb15 81.1(2) 5 . ?
O1 Pb10 Pb15 45.9(2) . . ?
O1 Pb10 Pb15 137.6(3) 2_554 . ?
Pb10 Pb10 Pb15 61.723(19) 5 . ?
Pb10 Pb10 Pb15 90.96(3) 2_554 . ?
Pb6 Pb10 Pb15 57.999(17) . . ?
Pb6 Pb10 Pb15 119.79(2) 2_554 . ?
Pb14 Pb10 Pb15 176.93(3) 2_554 . ?
O12 Pb11 O2 81.9(4) . 5 ?
O12 Pb11 O3 81.5(4) . 8_556 ?
O2 Pb11 O3 89.7(4) 5 8_556 ?
O12 Pb11 Cl2 77.2(3) . . ?
O2 Pb11 Cl2 159.0(3) 5 . ?
O3 Pb11 Cl2 89.1(3) 8_556 . ?
O12 Pb11 Cl3 80.1(3) . . ?
O2 Pb11 Cl3 100.2(3) 5 . ?
O3 Pb11 Cl3 157.6(3) 8_556 . ?
Cl2 Pb11 Cl3 74.48(11) . . ?
O12 Pb11 Cl4 142.3(2) . . ?
O2 Pb11 Cl4 84.4(3) 5 . ?
O3 Pb11 Cl4 133.4(3) 8_556 . ?
Cl2 Pb11 Cl4 111.27(12) . . ?
Cl3 Pb11 Cl4 68.10(11) . . ?
O12 Pb11 Si1 97.8(3) . 6_556 ?
O2 Pb11 Si1 79.2(3) 5 6_556 ?
O3 Pb11 Si1 20.8(3) 8_556 6_556 ?
Cl2 Pb11 Si1 105.30(8) . 6_556 ?
Cl3 Pb11 Si1 177.83(9) . 6_556 ?
Cl4 Pb11 Si1 113.85(8) . 6_556 ?
O12 Pb11 As1 97.8(3) . 6_556 ?
O2 Pb11 As1 79.2(3) 5 6_556 ?
O3 Pb11 As1 20.8(3) 8_556 6_556 ?
Cl2 Pb11 As1 105.30(8) . 6_556 ?
Cl3 Pb11 As1 177.83(9) . 6_556 ?
Cl4 Pb11 As1 113.85(8) . 6_556 ?
Si1 Pb11 As1 0.00(8) 6_556 6_556 ?
O12 Pb11 Pb15 33.5(2) . . ?
O2 Pb11 Pb15 91.0(3) 5 . ?
O3 Pb11 Pb15 49.2(3) 8_556 . ?
Cl2 Pb11 Pb15 72.49(8) . . ?
Cl3 Pb11 Pb15 110.06(8) . . ?
Cl4 Pb11 Pb15 174.60(7) . . ?
Si1 Pb11 Pb15 67.91(4) 6_556 . ?
As1 Pb11 Pb15 67.91(4) 6_556 . ?
O12 Pb11 Pb1 124.7(3) . . ?
O2 Pb11 Pb1 131.9(3) 5 . ?
O3 Pb11 Pb1 129.6(3) 8_556 . ?
Cl2 Pb11 Pb1 61.87(8) . . ?
Cl3 Pb11 Pb1 55.14(7) . . ?
Cl4 Pb11 Pb1 49.41(7) . . ?
Si1 Pb11 Pb1 126.75(4) 6_556 . ?
As1 Pb11 Pb1 126.75(4) 6_556 . ?
Pb15 Pb11 Pb1 134.17(2) . . ?
O12 Pb11 Pb10 34.9(2) . . ?
O2 Pb11 Pb10 49.8(3) 5 . ?
O3 Pb11 Pb10 94.9(3) 8_556 . ?
Cl2 Pb11 Pb10 109.51(9) . . ?
Cl3 Pb11 Pb10 76.93(7) . . ?
Cl4 Pb11 Pb10 114.90(7) . . ?
Si1 Pb11 Pb10 101.19(4) 6_556 . ?
As1 Pb11 Pb10 101.19(4) 6_556 . ?
Pb15 Pb11 Pb10 59.758(19) . . ?
Pb1 Pb11 Pb10 132.06(2) . . ?
O12 Pb11 Pb6 33.3(3) . . ?
O2 Pb11 Pb6 106.1(3) 5 . ?
O3 Pb11 Pb6 104.0(3) 8_556 . ?
Cl2 Pb11 Pb6 54.07(8) . . ?
Cl3 Pb11 Pb6 53.96(8) . . ?
Cl4 Pb11 Pb6 122.03(7) . . ?
Si1 Pb11 Pb6 124.12(4) 6_556 . ?
As1 Pb11 Pb6 124.12(4) 6_556 . ?
Pb15 Pb11 Pb6 56.574(16) . . ?
Pb1 Pb11 Pb6 91.320(19) . . ?
Pb10 Pb11 Pb6 56.840(17) . . ?
O11 Pb12 O14 77.6(4) 6_565 6_565 ?
O11 Pb12 O9 110.3(4) 6_565 3_455 ?
O14 Pb12 O9 74.6(4) 6_565 3_455 ?
O11 Pb12 O4 75.6(4) 6_565 6_565 ?
O14 Pb12 O4 126.6(4) 6_565 6_565 ?
O9 Pb12 O4 72.9(4) 3_455 6_565 ?
O11 Pb12 O6 72.6(4) 6_565 6_565 ?
O14 Pb12 O6 72.1(4) 6_565 6_565 ?
O9 Pb12 O6 145.1(3) 3_455 6_565 ?
O4 Pb12 O6 137.6(4) 6_565 6_565 ?
O11 Pb12 Pb7 94.9(3) 6_565 . ?
O14 Pb12 Pb7 37.6(3) 6_565 . ?
O9 Pb12 Pb7 37.0(3) 3_455 . ?
O4 Pb12 Pb7 100.7(3) 6_565 . ?
O6 Pb12 Pb7 109.1(2) 6_565 . ?
O11 Pb12 Pb9 154.6(3) 6_565 . ?
O14 Pb12 Pb9 89.6(3) 6_565 . ?
O9 Pb12 Pb9 86.7(3) 3_455 . ?
O4 Pb12 Pb9 128.8(3) 6_565 . ?
O6 Pb12 Pb9 82.7(2) 6_565 . ?
Pb7 Pb12 Pb9 87.77(2) . . ?
O11 Pb12 Pb2 39.2(2) 6_565 6_565 ?
O14 Pb12 Pb2 38.4(3) 6_565 6_565 ?
O9 Pb12 Pb2 93.7(3) 3_455 6_565 ?
O4 Pb12 Pb2 103.9(3) 6_565 6_565 ?
O6 Pb12 Pb2 66.1(2) 6_565 6_565 ?
Pb7 Pb12 Pb2 63.333(19) . 6_565 ?
Pb9 Pb12 Pb2 124.26(2) . 6_565 ?
O11 Pb12 Pb8 93.1(2) 6_565 6_565 ?
O14 Pb12 Pb8 33.4(3) 6_565 6_565 ?
O9 Pb12 Pb8 96.4(3) 3_455 6_565 ?
O4 Pb12 Pb8 159.9(3) 6_565 6_565 ?
O6 Pb12 Pb8 49.0(2) 6_565 6_565 ?
Pb7 Pb12 Pb8 63.282(18) . 6_565 ?
Pb9 Pb12 Pb8 65.576(18) . 6_565 ?
Pb2 Pb12 Pb8 58.988(17) 6_565 6_565 ?
O11 Pb12 Pb9 33.8(3) 6_565 6_565 ?
O14 Pb12 Pb9 92.3(3) 6_565 6_565 ?
O9 Pb12 Pb9 144.0(3) 3_455 6_565 ?
O4 Pb12 Pb9 90.1(3) 6_565 6_565 ?
O6 Pb12 Pb9 48.6(2) 6_565 6_565 ?
Pb7 Pb12 Pb9 122.46(2) . 6_565 ?
Pb9 Pb12 Pb9 127.27(2) . 6_565 ?
Pb2 Pb12 Pb9 59.214(17) 6_565 6_565 ?
Pb8 Pb12 Pb9 89.23(2) 6_565 6_565 ?
O11 Pb12 Pb16 89.1(3) 6_565 3_455 ?
O14 Pb12 Pb16 95.9(3) 6_565 3_455 ?
O9 Pb12 Pb16 34.7(3) 3_455 3_455 ?
O4 Pb12 Pb16 39.2(3) 6_565 3_455 ?
O6 Pb12 Pb16 159.8(2) 6_565 3_455 ?
Pb7 Pb12 Pb16 62.789(19) . 3_455 ?
Pb9 Pb12 Pb16 114.20(2) . 3_455 ?
Pb2 Pb12 Pb16 94.33(2) 6_565 3_455 ?
Pb8 Pb12 Pb16 126.02(2) 6_565 3_455 ?
Pb9 Pb12 Pb16 117.96(2) 6_565 3_455 ?
O11 Pb12 Pb15 130.3(2) 6_565 8_455 ?
O14 Pb12 Pb15 151.7(3) 6_565 8_455 ?
O9 Pb12 Pb15 88.7(3) 3_455 8_455 ?
O4 Pb12 Pb15 66.8(3) 6_565 8_455 ?
O6 Pb12 Pb15 116.6(2) 6_565 8_455 ?
Pb7 Pb12 Pb15 122.39(2) . 8_455 ?
Pb9 Pb12 Pb15 66.286(19) . 8_455 ?
Pb2 Pb12 Pb15 169.26(2) 6_565 8_455 ?
Pb8 Pb12 Pb15 131.15(2) 6_565 8_455 ?
Pb9 Pb12 Pb15 113.85(2) 6_565 8_455 ?
Pb16 Pb12 Pb15 81.75(2) 3_455 8_455 ?
O20 Pb13 O17 78.3(3) . 6_566 ?
O20 Pb13 O5 75.6(5) . . ?
O17 Pb13 O5 94.5(6) 6_566 . ?
O20 Pb13 Cl3 77.7(3) . 6_566 ?
O17 Pb13 Cl3 87.0(3) 6_566 6_566 ?
O5 Pb13 Cl3 152.4(5) . 6_566 ?
O20 Pb13 Cl3 76.6(3) . 5_565 ?
O17 Pb13 Cl3 150.3(3) 6_566 5_565 ?
O5 Pb13 Cl3 94.4(5) . 5_565 ?
Cl3 Pb13 Cl3 72.43(15) 6_566 5_565 ?
O20 Pb13 Cl5 143.84(10) . 7_465 ?
O17 Pb13 Cl5 77.5(3) 6_566 7_465 ?
O5 Pb13 Cl5 132.6(5) . 7_465 ?
Cl3 Pb13 Cl5 74.58(10) 6_566 7_465 ?
Cl3 Pb13 Cl5 115.58(11) 5_565 7_465 ?
O20 Pb13 Pb4 40.4(2) . . ?
O17 Pb13 Pb4 37.9(3) 6_566 . ?
O5 Pb13 Pb4 84.4(5) . . ?
Cl3 Pb13 Pb4 79.91(8) 6_566 . ?
Cl3 Pb13 Pb4 115.30(8) 5_565 . ?
Cl5 Pb13 Pb4 111.11(8) 7_465 . ?
O20 Pb13 As2 96.7(3) . . ?
O17 Pb13 As2 89.3(3) 6_566 . ?
O5 Pb13 As2 23.2(5) . . ?
Cl3 Pb13 As2 173.82(8) 6_566 . ?
Cl3 Pb13 As2 109.00(9) 5_565 . ?
Cl5 Pb13 As2 109.47(8) 7_465 . ?
Pb4 Pb13 As2 94.16(4) . . ?
O20 Pb13 Pb6 120.4(3) . 5_565 ?
O17 Pb13 Pb6 127.7(3) 6_566 5_565 ?
O5 Pb13 Pb6 135.9(5) . 5_565 ?
Cl3 Pb13 Pb6 55.95(7) 6_566 5_565 ?
Cl3 Pb13 Pb6 56.41(8) 5_565 5_565 ?
Cl5 Pb13 Pb6 59.21(7) 7_465 5_565 ?
Pb4 Pb13 Pb6 135.83(2) . 5_565 ?
As2 Pb13 Pb6 130.01(3) . 5_565 ?
O20 Pb13 Pb2 91.54(2) . 6_566 ?
O17 Pb13 Pb2 37.4(3) 6_566 6_566 ?
O5 Pb13 Pb2 131.8(5) . 6_566 ?
Cl3 Pb13 Pb2 55.65(8) 6_566 6_566 ?
Cl3 Pb13 Pb2 128.09(8) 5_565 6_566 ?
Cl5 Pb13 Pb2 53.50(7) 7_465 6_566 ?
Pb4 Pb13 Pb2 59.124(18) . 6_566 ?
As2 Pb13 Pb2 122.62(4) . 6_566 ?
Pb6 Pb13 Pb2 90.894(18) 5_565 6_566 ?
O20 Pb13 Pb13 30.8(3) . 2 ?
O17 Pb13 Pb13 97.3(2) 6_566 2 ?
O5 Pb13 Pb13 98.0(5) . 2 ?
Cl3 Pb13 Pb13 54.57(8) 6_566 2 ?
Cl3 Pb13 Pb13 53.35(8) 5_565 2 ?
Cl5 Pb13 Pb13 129.14(7) 7_465 2 ?
Pb4 Pb13 Pb13 62.779(16) . 2 ?
As2 Pb13 Pb13 121.13(3) . 2 ?
Pb6 Pb13 Pb13 89.559(12) 5_565 2 ?
Pb2 Pb13 Pb13 92.26(2) 6_566 2 ?
O20 Pb13 Pb4 33.80(17) . 2 ?
O17 Pb13 Pb4 92.5(3) 6_566 2 ?
O5 Pb13 Pb4 43.4(4) . 2 ?
Cl3 Pb13 Pb4 109.00(8) 6_566 2 ?
Cl3 Pb13 Pb4 74.99(8) 5_565 2 ?
Cl5 Pb13 Pb4 169.35(8) 7_465 2 ?
Pb4 Pb13 Pb4 60.75(2) . 2 ?
As2 Pb13 Pb4 66.16(3) . 2 ?
Pb6 Pb13 Pb4 131.27(2) 5_565 2 ?
Pb2 Pb13 Pb4 119.65(2) 6_566 2 ?
Pb13 Pb13 Pb4 55.181(16) 2 2 ?
O15 Pb14 O19 82.4(4) . . ?
O15 Pb14 O9 105.5(4) . . ?
O19 Pb14 O9 75.9(4) . . ?
O15 Pb14 O1 75.9(4) . . ?
O19 Pb14 O1 79.0(4) . . ?
O9 Pb14 O1 154.4(4) . . ?
O15 Pb14 O8B 70.8(8) . 3_545 ?
O19 Pb14 O8B 128.8(8) . 3_545 ?
O9 Pb14 O8B 70.7(8) . 3_545 ?
O1 Pb14 O8B 131.3(8) . 3_545 ?
O15 Pb14 Pb16 93.8(3) . . ?
O19 Pb14 Pb16 36.9(3) . . ?
O9 Pb14 Pb16 39.1(3) . . ?
O1 Pb14 Pb16 115.8(3) . . ?
O8B Pb14 Pb16 101.2(8) 3_545 . ?
O15 Pb14 Pb6 39.9(2) . . ?
O19 Pb14 Pb6 42.8(3) . . ?
O9 Pb14 Pb6 94.9(3) . . ?
O1 Pb14 Pb6 69.5(3) . . ?
O8B Pb14 Pb6 102.8(8) 3_545 . ?
Pb16 Pb14 Pb6 64.402(19) . . ?
O15 Pb14 As1 93.6(3) . . ?
O19 Pb14 As1 96.3(3) . . ?
O9 Pb14 As1 158.0(3) . . ?
O1 Pb14 As1 23.3(3) . . ?
O8B Pb14 As1 127.4(8) 3_545 . ?
Pb16 Pb14 As1 130.48(4) . . ?
Pb6 Pb14 As1 92.77(4) . . ?
O15 Pb14 Pb15 154.8(2) . 6 ?
O19 Pb14 Pb15 82.5(3) . 6 ?
O9 Pb14 Pb15 90.3(3) . 6 ?
O1 Pb14 Pb15 81.4(3) . 6 ?
O8B Pb14 Pb15 133.9(8) 3_545 6 ?
Pb16 Pb14 Pb15 86.16(2) . 6 ?
Pb6 Pb14 Pb15 120.79(2) . 6 ?
As1 Pb14 Pb15 68.11(4) . 6 ?
O15 Pb14 Pb15 35.5(3) . . ?
O19 Pb14 Pb15 96.9(3) . . ?
O9 Pb14 Pb15 140.7(3) . . ?
O1 Pb14 Pb15 47.7(3) . . ?
O8B Pb14 Pb15 86.0(8) 3_545 . ?
Pb16 Pb14 Pb15 123.19(2) . . ?
Pb6 Pb14 Pb15 59.098(17) . . ?
As1 Pb14 Pb15 59.81(4) . . ?
Pb15 Pb14 Pb15 127.56(3) 6 . ?
O15 Pb14 Pb9 132.8(2) . 3_545 ?
O19 Pb14 Pb9 143.8(3) . 3_545 ?
O9 Pb14 Pb9 84.9(3) . 3_545 ?
O1 Pb14 Pb9 113.3(3) . 3_545 ?
O8B Pb14 Pb9 69.8(8) 3_545 3_545 ?
Pb16 Pb14 Pb9 118.42(2) . 3_545 ?
Pb6 Pb14 Pb9 172.26(2) . 3_545 ?
As1 Pb14 Pb9 90.22(4) . 3_545 ?
Pb15 Pb14 Pb9 66.95(2) 6 3_545 ?
Pb15 Pb14 Pb9 116.88(2) . 3_545 ?
O15 Pb14 Pb10 95.8(2) . 2_554 ?
O19 Pb14 Pb10 33.8(3) . 2_554 ?
O9 Pb14 Pb10 102.0(2) . 2_554 ?
O1 Pb14 Pb10 52.9(3) . 2_554 ?
O8B Pb14 Pb10 161.5(8) 3_545 2_554 ?
Pb16 Pb14 Pb10 66.016(19) . 2_554 ?
Pb6 Pb14 Pb10 60.103(18) . 2_554 ?
As1 Pb14 Pb10 64.53(4) . 2_554 ?
Pb15 Pb14 Pb10 61.125(17) 6 2_554 ?
Pb15 Pb14 Pb10 90.17(2) . 2_554 ?
Pb9 Pb14 Pb10 127.53(3) 3_545 2_554 ?
O12 Pb15 O15 80.8(4) . . ?
O12 Pb15 O16 112.2(4) . . ?
O15 Pb15 O16 75.0(4) . . ?
O12 Pb15 O1 80.2(4) . . ?
O15 Pb15 O1 73.2(4) . . ?
O16 Pb15 O1 143.3(4) . . ?
O12 Pb15 O3 70.8(3) . 8_556 ?
O15 Pb15 O3 125.7(3) . 8_556 ?
O16 Pb15 O3 74.6(3) . 8_556 ?
O1 Pb15 O3 140.3(3) . 8_556 ?
O12 Pb15 Pb3 95.6(3) . . ?
O15 Pb15 Pb3 37.5(2) . . ?
O16 Pb15 Pb3 37.6(3) . . ?
O1 Pb15 Pb3 109.6(3) . . ?
O3 Pb15 Pb3 99.8(2) 8_556 . ?
O12 Pb15 Pb6 40.1(3) . . ?
O15 Pb15 Pb6 40.9(2) . . ?
O16 Pb15 Pb6 97.5(3) . . ?
O1 Pb15 Pb6 69.3(3) . . ?
O3 Pb15 Pb6 101.6(2) 8_556 . ?
Pb3 Pb15 Pb6 65.182(18) . . ?
O12 Pb15 As1 97.6(3) . . ?
O15 Pb15 As1 91.7(3) . . ?
O16 Pb15 As1 144.4(3) . . ?
O1 Pb15 As1 23.7(3) . . ?
O3 Pb15 As1 136.2(2) 8_556 . ?
Pb3 Pb15 As1 123.66(4) . . ?
Pb6 Pb15 As1 92.99(4) . . ?
O12 Pb15 Pb14 134.2(3) . 6_556 ?
O15 Pb15 Pb14 144.3(2) . 6_556 ?
O16 Pb15 Pb14 83.1(3) . 6_556 ?
O1 Pb15 Pb14 113.7(3) . 6_556 ?
O3 Pb15 Pb14 72.7(2) 8_556 6_556 ?
Pb3 Pb15 Pb14 117.18(2) . 6_556 ?
Pb6 Pb15 Pb14 173.98(3) . 6_556 ?
As1 Pb15 Pb14 90.00(4) . 6_556 ?
O12 Pb15 Pb14 95.6(3) . . ?
O15 Pb15 Pb14 33.9(3) . . ?
O16 Pb15 Pb14 97.3(3) . . ?
O1 Pb15 Pb14 46.2(3) . . ?
O3 Pb15 Pb14 159.1(2) 8_556 . ?
Pb3 Pb15 Pb14 64.861(19) . . ?
Pb6 Pb15 Pb14 59.775(19) . . ?
As1 Pb15 Pb14 59.48(4) . . ?
Pb14 Pb15 Pb14 126.18(2) 6_556 . ?
O12 Pb15 Pb11 32.8(3) . . ?
O15 Pb15 Pb11 98.3(3) . . ?
O16 Pb15 Pb11 90.4(3) . . ?
O1 Pb15 Pb11 111.8(3) . . ?
O3 Pb15 Pb11 39.0(2) 8_556 . ?
Pb3 Pb15 Pb11 92.95(2) . . ?
Pb6 Pb15 Pb11 64.138(19) . . ?
As1 Pb15 Pb11 124.60(4) . . ?
Pb14 Pb15 Pb11 109.89(2) 6_556 . ?
Pb14 Pb15 Pb11 123.91(2) . . ?
O12 Pb15 Pb10 36.9(3) . . ?
O15 Pb15 Pb10 95.0(2) . . ?
O16 Pb15 Pb10 149.1(3) . . ?
O1 Pb15 Pb10 52.5(3) . . ?
O3 Pb15 Pb10 89.0(2) 8_556 . ?
Pb3 Pb15 Pb10 124.93(2) . . ?
Pb6 Pb15 Pb10 59.799(16) . . ?
As1 Pb15 Pb10 63.23(4) . . ?
Pb14 Pb15 Pb10 117.34(2) 6_556 . ?
Pb14 Pb15 Pb10 88.89(2) . . ?
Pb11 Pb15 Pb10 61.686(19) . . ?
O19 Pb16 O9 78.7(4) . . ?
O19 Pb16 O4 96.8(4) . 8 ?
O9 Pb16 O4 75.9(4) . 8 ?
O19 Pb16 Cl5 91.0(3) . 3_545 ?
O9 Pb16 Cl5 77.9(3) . 3_545 ?
O4 Pb16 Cl5 150.6(3) 8 3_545 ?
O19 Pb16 Cl1 153.5(2) . 2_554 ?
O9 Pb16 Cl1 78.8(3) . 2_554 ?
O4 Pb16 Cl1 91.3(3) 8 2_554 ?
Cl5 Pb16 Cl1 70.63(8) 3_545 2_554 ?
O19 Pb16 Cl3 79.7(3) . 2_554 ?
O9 Pb16 Cl3 143.6(3) . 2_554 ?
O4 Pb16 Cl3 135.8(3) 8 2_554 ?
Cl5 Pb16 Cl3 73.55(10) 3_545 2_554 ?
Cl1 Pb16 Cl3 111.44(7) 2_554 2_554 ?
O19 Pb16 Si1 88.8(3) . 6 ?
O9 Pb16 Si1 99.1(3) . 6 ?
O4 Pb16 Si1 26.6(3) 8 6 ?
Cl5 Pb16 Si1 176.98(8) 3_545 6 ?
Cl1 Pb16 Si1 108.56(5) 2_554 6 ?
Cl3 Pb16 Si1 109.36(8) 2_554 6 ?
O19 Pb16 As1 88.8(3) . 6 ?
O9 Pb16 As1 99.1(3) . 6 ?
O4 Pb16 As1 26.6(3) 8 6 ?
Cl5 Pb16 As1 176.98(8) 3_545 6 ?
Cl1 Pb16 As1 108.56(5) 2_554 6 ?
Cl3 Pb16 As1 109.36(8) 2_554 6 ?
Si1 Pb16 As1 0.00(5) 6 6 ?
O19 Pb16 Pb14 36.4(2) . . ?
O9 Pb16 Pb14 42.3(3) . . ?
O4 Pb16 Pb14 87.0(3) 8 . ?
Cl5 Pb16 Pb14 82.56(8) 3_545 . ?
Cl1 Pb16 Pb14 119.56(2) 2_554 . ?
Cl3 Pb16 Pb14 110.96(8) 2_554 . ?
Si1 Pb16 Pb14 95.49(4) 6 . ?
As1 Pb16 Pb14 95.49(4) 6 . ?
O19 Pb16 Pb2 128.3(3) . 2_554 ?
O9 Pb16 Pb2 121.9(3) . 2_554 ?
O4 Pb16 Pb2 132.6(3) 8 2_554 ?
Cl5 Pb16 Pb2 55.22(8) 3_545 2_554 ?
Cl1 Pb16 Pb2 56.093(15) 2_554 2_554 ?
Cl3 Pb16 Pb2 55.38(7) 2_554 2_554 ?
Si1 Pb16 Pb2 126.94(4) 6 2_554 ?
As1 Pb16 Pb2 126.94(4) 6 2_554 ?
Pb14 Pb16 Pb2 137.33(2) . 2_554 ?
O19 Pb16 Pb12 93.1(3) . 3_545 ?
O9 Pb16 Pb12 36.3(3) . 3_545 ?
O4 Pb16 Pb12 40.6(3) 8 3_545 ?
Cl5 Pb16 Pb12 110.88(7) 3_545 3_545 ?
Cl1 Pb16 Pb12 76.78(2) 2_554 3_545 ?
Cl3 Pb16 Pb12 171.75(8) 2_554 3_545 ?
Si1 Pb16 Pb12 66.13(4) 6 3_545 ?
As1 Pb16 Pb12 66.13(4) 6 3_545 ?
Pb14 Pb16 Pb12 63.724(19) . 3_545 ?
Pb2 Pb16 Pb12 132.86(2) 2_554 3_545 ?
O19 Pb16 Pb6 38.7(3) . . ?
O9 Pb16 Pb6 92.5(3) . . ?
O4 Pb16 Pb6 135.4(3) 8 . ?
Cl5 Pb16 Pb6 58.58(8) 3_545 . ?
Cl1 Pb16 Pb6 129.14(2) 2_554 . ?
Cl3 Pb16 Pb6 53.34(8) 2_554 . ?
Si1 Pb16 Pb6 122.30(5) 6 . ?
As1 Pb16 Pb6 122.30(5) 6 . ?
Pb14 Pb16 Pb6 58.787(18) . . ?
Pb2 Pb16 Pb6 90.325(19) 2_554 . ?
Pb12 Pb16 Pb6 122.34(2) 3_545 . ?
O1 As1 O2 109.2(7) . . ?
O1 As1 O3 112.1(6) . 3_545 ?
O2 As1 O3 116.3(6) . 3_545 ?
O1 As1 O4 110.2(6) . 3_545 ?
O2 As1 O4 106.1(6) . 3_545 ?
O3 As1 O4 102.5(6) 3_545 3_545 ?
O1 As1 Pb5 129.5(5) . 3_545 ?
O2 As1 Pb5 121.0(5) . 3_545 ?
O3 As1 Pb5 50.2(4) 3_545 3_545 ?
O4 As1 Pb5 52.6(4) 3_545 3_545 ?
O1 As1 Pb16 132.0(5) . 6_556 ?
O2 As1 Pb16 67.1(4) . 6_556 ?
O3 As1 Pb16 111.4(4) 3_545 6_556 ?
O4 As1 Pb16 40.1(4) 3_545 6_556 ?
Pb5 As1 Pb16 69.65(5) 3_545 6_556 ?
O1 As1 Pb11 122.7(4) . 6 ?
O2 As1 Pb11 86.5(5) . 6 ?
O3 As1 Pb11 30.1(4) 3_545 6 ?
O4 As1 Pb11 117.5(4) 3_545 6 ?
Pb5 As1 Pb11 68.32(5) 3_545 6 ?
Pb16 As1 Pb11 105.11(6) 6_556 6 ?
O1 As1 Pb14 41.5(5) . . ?
O2 As1 Pb14 150.2(5) . . ?
O3 As1 Pb14 86.9(4) 3_545 . ?
O4 As1 Pb14 85.2(4) 3_545 . ?
Pb5 As1 Pb14 87.93(5) 3_545 . ?
Pb16 As1 Pb14 123.93(6) 6_556 . ?
Pb11 As1 Pb14 113.14(6) 6 . ?
O1 As1 Pb15 43.7(4) . . ?
O2 As1 Pb15 94.8(5) . . ?
O3 As1 Pb15 147.6(4) 3_545 . ?
O4 As1 Pb15 75.7(4) 3_545 . ?
Pb5 As1 Pb15 121.96(6) 3_545 . ?
Pb16 As1 Pb15 88.27(5) 6_556 . ?
Pb11 As1 Pb15 165.87(7) 6 . ?
Pb14 As1 Pb15 60.71(4) . . ?
O8A As2 O6 111.0(13) . . ?
O8A As2 O7 129.7(14) . . ?
O6 As2 O7 108.9(10) . . ?
O8A As2 O5 94.6(13) . . ?
O6 As2 O5 110.8(8) . . ?
O7 As2 O5 98.7(10) . . ?
O8A As2 O8B 55.8(16) . . ?
O6 As2 O8B 109.6(13) . . ?
O7 As2 O8B 82.7(15) . . ?
O5 As2 O8B 136.5(14) . . ?
O8A As2 Pb1 119.9(12) . 5_565 ?
O6 As2 Pb1 127.0(5) . 5_565 ?
O7 As2 Pb1 45.7(7) . 5_565 ?
O5 As2 Pb1 53.5(7) . 5_565 ?
O8B As2 Pb1 110.4(13) . 5_565 ?
O8A As2 Pb7 91.8(11) . . ?
O6 As2 Pb7 127.2(4) . . ?
O7 As2 Pb7 38.8(8) . . ?
O5 As2 Pb7 114.1(7) . . ?
O8B As2 Pb7 46.5(13) . . ?
Pb1 As2 Pb7 66.88(4) 5_565 . ?
O8A As2 Pb13 63.6(11) . . ?
O6 As2 Pb13 131.3(4) . . ?
O7 As2 Pb13 108.6(8) . . ?
O5 As2 Pb13 33.2(7) . . ?
O8B As2 Pb13 104.9(13) . . ?
Pb1 As2 Pb13 66.84(3) 5_565 . ?
Pb7 As2 Pb13 101.45(5) . . ?
Pb16 Cl1 Pb16 180.000(13) 2_554 8_456 ?
Pb16 Cl1 Pb7 71.233(17) 2_554 4_444 ?
Pb16 Cl1 Pb7 108.767(17) 8_456 4_444 ?
Pb16 Cl1 Pb7 108.767(17) 2_554 6_566 ?
Pb16 Cl1 Pb7 71.233(17) 8_456 6_566 ?
Pb7 Cl1 Pb7 180.00(2) 4_444 6_566 ?
Pb16 Cl1 Pb5 72.579(18) 2_554 7_455 ?
Pb16 Cl1 Pb5 107.421(18) 8_456 7_455 ?
Pb7 Cl1 Pb5 111.19(2) 4_444 7_455 ?
Pb7 Cl1 Pb5 68.81(2) 6_566 7_455 ?
Pb16 Cl1 Pb5 107.421(18) 2_554 . ?
Pb16 Cl1 Pb5 72.579(18) 8_456 . ?
Pb7 Cl1 Pb5 68.81(2) 4_444 . ?
Pb7 Cl1 Pb5 111.19(2) 6_566 . ?
Pb5 Cl1 Pb5 180.00(2) 7_455 . ?
Pb16 Cl1 Pb2 68.666(19) 2_554 . ?
Pb16 Cl1 Pb2 111.334(19) 8_456 . ?
Pb7 Cl1 Pb2 109.487(17) 4_444 . ?
Pb7 Cl1 Pb2 70.513(18) 6_566 . ?
Pb5 Cl1 Pb2 108.638(17) 7_455 . ?
Pb5 Cl1 Pb2 71.362(17) . . ?
Pb16 Cl1 Pb2 111.334(19) 2_554 7_455 ?
Pb16 Cl1 Pb2 68.666(19) 8_456 7_455 ?
Pb7 Cl1 Pb2 70.513(17) 4_444 7_455 ?
Pb7 Cl1 Pb2 109.487(17) 6_566 7_455 ?
Pb5 Cl1 Pb2 71.362(17) 7_455 7_455 ?
Pb5 Cl1 Pb2 108.638(17) . 7_455 ?
Pb2 Cl1 Pb2 180.00(3) . 7_455 ?
Pb3 Cl2 Pb11 118.25(14) . . ?
Pb3 Cl2 Pb5 74.47(9) . 8_556 ?
Pb11 Cl2 Pb5 76.23(11) . 8_556 ?
Pb3 Cl2 Pb6 76.25(11) . . ?
Pb11 Cl2 Pb6 74.18(9) . . ?
Pb5 Cl2 Pb6 120.65(14) 8_556 . ?
Pb13 Cl3 Pb6 69.05(9) 6_565 2_554 ?
Pb13 Cl3 Pb13 72.08(10) 6_565 5_565 ?
Pb6 Cl3 Pb13 107.89(14) 2_554 5_565 ?
Pb13 Cl3 Pb1 112.36(12) 6_565 . ?
Pb6 Cl3 Pb1 177.70(17) 2_554 . ?
Pb13 Cl3 Pb1 74.38(9) 5_565 . ?
Pb13 Cl3 Pb6 108.06(14) 6_565 . ?
Pb6 Cl3 Pb6 70.02(9) 2_554 . ?
Pb13 Cl3 Pb6 67.95(9) 5_565 . ?
Pb1 Cl3 Pb6 110.83(12) . . ?
Pb13 Cl3 Pb2 71.09(9) 6_565 . ?
Pb6 Cl3 Pb2 108.19(12) 2_554 . ?
Pb13 Cl3 Pb2 113.01(12) 5_565 . ?
Pb1 Cl3 Pb2 70.95(9) . . ?
Pb6 Cl3 Pb2 178.22(14) . . ?
Pb13 Cl3 Pb11 179.23(17) 6_565 . ?
Pb6 Cl3 Pb11 110.46(12) 2_554 . ?
Pb13 Cl3 Pb11 107.62(12) 5_565 . ?
Pb1 Cl3 Pb11 68.15(9) . . ?
Pb6 Cl3 Pb11 71.18(9) . . ?
Pb2 Cl3 Pb11 109.66(14) . . ?
Pb13 Cl3 Pb16 105.13(11) 6_565 2_554 ?
Pb6 Cl3 Pb16 69.51(8) 2_554 2_554 ?
Pb13 Cl3 Pb16 176.88(15) 5_565 2_554 ?
Pb1 Cl3 Pb16 108.24(14) . 2_554 ?
Pb6 Cl3 Pb16 112.13(12) . 2_554 ?
Pb2 Cl3 Pb16 66.83(9) . 2_554 ?
Pb11 Cl3 Pb16 75.15(10) . 2_554 ?
Pb1 Cl4 Pb1 74.77(9) . 2 ?
Pb1 Cl4 Pb2 76.52(10) . . ?
Pb1 Cl4 Pb2 119.52(13) 2 . ?
Pb1 Cl4 Pb7 117.94(14) . 6_566 ?
Pb1 Cl4 Pb7 76.08(10) 2 6_566 ?
Pb2 Cl4 Pb7 72.45(8) . 6_566 ?
Pb1 Cl4 Pb11 70.16(9) . . ?
Pb1 Cl4 Pb11 107.60(11) 2 . ?
Pb2 Cl4 Pb11 110.74(13) . . ?
Pb7 Cl4 Pb11 171.89(15) 6_566 . ?
Pb5 Cl5 Pb16 111.14(13) 4_454 3_455 ?
Pb5 Cl5 Pb2 73.52(9) 4_454 4_454 ?
Pb16 Cl5 Pb2 69.94(9) 3_455 4_454 ?
Pb5 Cl5 Pb7 69.88(9) 4_454 . ?
Pb16 Cl5 Pb7 71.55(9) 3_455 . ?
Pb2 Cl5 Pb7 110.59(13) 4_454 . ?
Pb5 Cl5 Pb3 69.99(8) 4_454 5_565 ?
Pb16 Cl5 Pb3 176.38(14) 3_455 5_565 ?
Pb2 Cl5 Pb3 113.63(12) 4_454 5_565 ?
Pb7 Cl5 Pb3 106.04(11) . 5_565 ?
Pb5 Cl5 Pb3 112.74(11) 4_454 3_455 ?
Pb16 Cl5 Pb3 109.08(12) 3_455 3_455 ?
Pb2 Cl5 Pb3 173.15(15) 4_454 3_455 ?
Pb7 Cl5 Pb3 74.94(8) . 3_455 ?
Pb3 Cl5 Pb3 67.47(8) 5_565 3_455 ?
Pb5 Cl5 Pb13 113.08(12) 4_454 7_465 ?
Pb16 Cl5 Pb13 106.64(11) 3_455 7_465 ?
Pb2 Cl5 Pb13 70.55(8) 4_454 7_465 ?
Pb7 Cl5 Pb13 177.03(15) . 7_465 ?
Pb3 Cl5 Pb13 75.65(9) 5_565 7_465 ?
Pb3 Cl5 Pb13 103.73(12) 3_455 7_465 ?
As1 O1 Pb14 115.2(7) . . ?
As1 O1 Pb15 112.6(6) . . ?
Pb14 O1 Pb15 86.0(4) . . ?
As1 O1 Pb10 111.3(6) . . ?
Pb14 O1 Pb10 133.1(5) . . ?
Pb15 O1 Pb10 81.6(3) . . ?
As1 O1 Pb10 114.1(6) . 2_554 ?
Pb14 O1 Pb10 82.4(3) . 2_554 ?
Pb15 O1 Pb10 132.4(5) . 2_554 ?
Pb10 O1 Pb10 73.7(3) . 2_554 ?
As1 O2 Pb11 142.6(8) . 5 ?
As1 O2 Pb10 123.2(6) . 5 ?
Pb11 O2 Pb10 93.7(4) 5 5 ?
Si1 O3 As1 0.0(2) 3_455 3_455 ?
Si1 O3 Pb11 129.0(6) 3_455 8_455 ?
As1 O3 Pb11 129.0(6) 3_455 8_455 ?
Si1 O3 Pb5 101.3(4) 3_455 . ?
As1 O3 Pb5 101.3(4) 3_455 . ?
Pb11 O3 Pb5 104.0(4) 8_455 . ?
Si1 O3 Pb15 131.1(6) 3_455 8_455 ?
As1 O3 Pb15 131.1(6) 3_455 8_455 ?
Pb11 O3 Pb15 91.9(3) 8_455 8_455 ?
Pb5 O3 Pb15 91.2(3) . 8_455 ?
Si1 O4 As1 0.00(19) 3_455 3_455 ?
Si1 O4 Pb16 113.3(6) 3_455 8_456 ?
As1 O4 Pb16 113.3(6) 3_455 8_456 ?
Si1 O4 Pb12 141.4(7) 3_455 6_566 ?
As1 O4 Pb12 141.4(7) 3_455 6_566 ?
Pb16 O4 Pb12 100.2(4) 8_456 6_566 ?
Si1 O4 Pb5 98.2(5) 3_455 . ?
As1 O4 Pb5 98.2(5) 3_455 . ?
Pb16 O4 Pb5 98.7(4) 8_456 . ?
Pb12 O4 Pb5 95.0(4) 6_566 . ?
As2 O5 Pb13 123.6(10) . . ?
As2 O5 Pb4 135.5(10) . 2 ?
Pb13 O5 Pb4 99.1(6) . 2 ?
As2 O5 Pb1 98.4(8) . 5_565 ?
Pb13 O5 Pb1 96.5(7) . 5_565 ?
Pb4 O5 Pb1 87.6(6) 2 5_565 ?
As2 O6 Pb4 117.3(6) . 6_565 ?
As2 O6 Pb9 114.3(6) . . ?
Pb4 O6 Pb9 82.9(3) 6_565 . ?
As2 O6 Pb8 112.3(6) . . ?
Pb4 O6 Pb8 82.9(3) 6_565 . ?
Pb9 O6 Pb8 132.8(5) . . ?
As2 O6 Pb12 109.4(6) . 6_566 ?
Pb4 O6 Pb12 133.2(5) 6_565 6_566 ?
Pb9 O6 Pb12 79.1(3) . 6_566 ?
Pb8 O6 Pb12 78.7(3) . 6_566 ?
As2 O7 Pb7 117.1(11) . . ?
As2 O7 Pb8 138.8(13) . 6_565 ?
Pb7 O7 Pb8 94.1(7) . 6_565 ?
As2 O7 Pb1 108.4(10) . 5_565 ?
Pb7 O7 Pb1 98.2(8) . 5_565 ?
Pb8 O7 Pb1 91.6(7) 6_565 5_565 ?
O8B O8A As2 65.6(19) . . ?
O8B O8A Pb3 80.5(19) . 3_455 ?
As2 O8A Pb3 137.9(19) . 3_455 ?
O8B O8A Pb9 152(2) . 6_566 ?
As2 O8A Pb9 128.6(16) . 6_566 ?
Pb3 O8A Pb9 93.0(11) 3_455 6_566 ?
O8A O8B As2 58.7(17) . . ?
O8A O8B Pb3 63.4(18) . 3_455 ?
As2 O8B Pb3 117.2(18) . 3_455 ?
O8A O8B Pb7 136(2) . . ?
As2 O8B Pb7 106.1(17) . . ?
Pb3 O8B Pb7 98.4(12) 3_455 . ?
O8A O8B Pb14 125(2) . 3_455 ?
As2 O8B Pb14 142(2) . 3_455 ?
Pb3 O8B Pb14 91.7(11) 3_455 3_455 ?
Pb7 O8B Pb14 93.1(11) . 3_455 ?
Pb7 O9 Pb16 117.6(5) 3_545 . ?
Pb7 O9 Pb12 103.3(5) 3_545 3_545 ?
Pb16 O9 Pb12 109.1(4) . 3_545 ?
Pb7 O9 Pb14 119.9(5) 3_545 . ?
Pb16 O9 Pb14 98.6(4) . . ?
Pb12 O9 Pb14 108.1(4) 3_545 . ?
Pb4 O10 Pb1 122.5(5) 6_565 . ?
Pb4 O10 Pb8 113.0(5) 6_565 . ?
Pb1 O10 Pb8 103.9(4) . . ?
Pb4 O10 Pb2 104.4(4) 6_565 . ?
Pb1 O10 Pb2 110.1(5) . . ?
Pb8 O10 Pb2 100.9(4) . . ?
Pb12 O11 Pb9 112.6(4) 6_566 . ?
Pb12 O11 Pb5 118.0(4) 6_566 . ?
Pb9 O11 Pb5 105.0(4) . . ?
Pb12 O11 Pb2 105.0(4) 6_566 . ?
Pb9 O11 Pb2 103.6(4) . . ?
Pb5 O11 Pb2 111.9(4) . . ?
Pb11 O12 Pb15 113.7(4) . . ?
Pb11 O12 Pb6 116.2(5) . . ?
Pb15 O12 Pb6 102.6(4) . . ?
Pb11 O12 Pb10 113.4(4) . . ?
Pb15 O12 Pb10 108.8(4) . . ?
Pb6 O12 Pb10 100.9(3) . . ?
Pb10 O13 Pb10 112.0(6) 2_554 . ?
Pb10 O13 Pb6 109.69(3) 2_554 . ?
Pb10 O13 Pb6 108.66(3) . . ?
Pb10 O13 Pb6 108.66(3) 2_554 2_554 ?
Pb10 O13 Pb6 109.69(3) . 2_554 ?
Pb6 O13 Pb6 108.1(5) . 2_554 ?
Pb8 O14 Pb7 118.6(4) . 6_566 ?
Pb8 O14 Pb12 111.6(5) . 6_566 ?
Pb7 O14 Pb12 104.1(4) 6_566 6_566 ?
Pb8 O14 Pb2 105.8(4) . . ?
Pb7 O14 Pb2 111.3(4) 6_566 . ?
Pb12 O14 Pb2 104.6(4) 6_566 . ?
Pb14 O15 Pb3 122.3(5) . . ?
Pb14 O15 Pb15 110.6(4) . . ?
Pb3 O15 Pb15 104.5(4) . . ?
Pb14 O15 Pb6 104.3(4) . . ?
Pb3 O15 Pb6 112.5(4) . . ?
Pb15 O15 Pb6 100.6(4) . . ?
Pb3 O16 Pb5 114.7(5) . 8_556 ?
Pb3 O16 Pb9 115.2(5) . 8_556 ?
Pb5 O16 Pb9 101.2(4) 8_556 8_556 ?
Pb3 O16 Pb15 99.8(4) . . ?
Pb5 O16 Pb15 112.1(4) 8_556 . ?
Pb9 O16 Pb15 114.5(5) 8_556 . ?
Pb9 O17 Pb13 124.2(5) . 6_565 ?
Pb9 O17 Pb4 112.1(5) . 6_565 ?
Pb13 O17 Pb4 104.7(4) 6_565 6_565 ?
Pb9 O17 Pb2 103.2(4) . . ?
Pb13 O17 Pb2 109.0(4) 6_565 . ?
Pb4 O17 Pb2 101.3(4) 6_565 . ?
Pb1 O18 Pb1 113.4(6) . 2 ?
Pb1 O18 Pb8 114.43(3) . 2 ?
Pb1 O18 Pb8 101.51(3) 2 2 ?
Pb1 O18 Pb8 101.51(3) . . ?
Pb1 O18 Pb8 114.43(3) 2 . ?
Pb8 O18 Pb8 112.1(6) 2 . ?
Pb14 O19 Pb16 106.7(4) . . ?
Pb14 O19 Pb10 113.7(5) . 2_554 ?
Pb16 O19 Pb10 124.3(4) . 2_554 ?
Pb14 O19 Pb6 100.6(4) . . ?
Pb16 O19 Pb6 107.7(4) . . ?
Pb10 O19 Pb6 100.9(4) 2_554 . ?
Pb13 O20 Pb13 118.3(7) 2 . ?
Pb13 O20 Pb4 101.80(6) 2 2 ?
Pb13 O20 Pb4 114.42(7) . 2 ?
Pb13 O20 Pb4 114.42(7) 2 . ?
Pb13 O20 Pb4 101.80(6) . . ?
Pb4 O20 Pb4 105.8(6) 2 . ?
 
_diffrn_measured_fraction_theta_max    0.949
_diffrn_reflns_theta_full              36.15
_diffrn_measured_fraction_theta_full   0.949
_refine_diff_density_max    6.602
_refine_diff_density_min   -4.798
_refine_diff_density_rms    0.811
