data_menchettiite _audit_creation_method SHELXL-97 _chemical_name_systematic ; ? ; _chemical_name_common menchettiite _chemical_melting_point 'Ag4 As7.56 Mn6.42 Pb9.11 S48 Sb12.91' _chemical_formula_moiety 'Ag4 As7.56 Mn6.42 Pb9.11 S48 Sb12.91' _chemical_formula_sum 'Ag4 As7.56 Mn6.42 Pb9.11 S48 Sb12.91' _chemical_formula_weight 6349.90 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'Ag' 'Ag' -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'As' 'As' 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Mn' 'Mn' 0.3368 0.7283 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Pb' 'Pb' -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Sb' 'Sb' -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M 'P21/n' loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 19.233(2) _cell_length_b 12.663(3) _cell_length_c 8.476(2) _cell_angle_alpha 90.00 _cell_angle_beta 90.080(10) _cell_angle_gamma 90.00 _cell_volume 2064.2(8) _cell_formula_units_Z 1 _cell_measurement_temperature 298(2) _cell_measurement_reflns_used 134 _cell_measurement_theta_min 12.5 _cell_measurement_theta_max 24.4 _exptl_crystal_description block _exptl_crystal_colour black _exptl_crystal_size_max 0.09 _exptl_crystal_size_mid 0.08 _exptl_crystal_size_min 0.06 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 5.108 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 2770.9 _exptl_absorpt_coefficient_mu 28.744 _exptl_absorpt_correction_type 'multi-scan' _exptl_absorpt_correction_T_min 0.265 _exptl_absorpt_correction_T_max 0.402 _exptl_absorpt_process_details 'Abspack' _exptl_special_details ; ? ; _diffrn_ambient_temperature 298(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Oxford Xcalibur 3' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean ? _diffrn_standards_number 13 _diffrn_standards_interval_count 345 _diffrn_standards_interval_time ? _diffrn_standards_decay_% 0 _diffrn_reflns_number 7808 _diffrn_reflns_av_R_equivalents 0.0698 _diffrn_reflns_av_sigmaI/netI 0.1193 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_h_max 22 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_l_min -10 _diffrn_reflns_limit_l_max 9 _diffrn_reflns_theta_min 4.24 _diffrn_reflns_theta_max 25.00 _reflns_number_total 3591 _reflns_number_gt 2365 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'Crysalis (Oxford, 2006)' _computing_cell_refinement 'Crysalis (Oxford, 2006)' _computing_data_reduction 'Crysalis (Oxford, 2006)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 2008)' _computing_structure_refinement 'SHELXS-97 (Sheldrick, 2008)' _computing_molecular_graphics 'Xtaldraw (Downs & Hall-Wallace, 2003)' _computing_publication_material 'SHELXL-97 (Sheldrick, 2008)' _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0540P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens 'noref' _refine_ls_hydrogen_treatment 'noref' _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 3591 _refine_ls_number_parameters 205 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.1359 _refine_ls_R_factor_gt 0.0903 _refine_ls_wR_factor_ref 0.1958 _refine_ls_wR_factor_gt 0.1731 _refine_ls_goodness_of_fit_ref 1.097 _refine_ls_restrained_S_all 1.097 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group M1PB Pb 0.13728(19) 0.3542(4) 0.1313(7) 0.078(2) Uani 0.396(11) 1 d P . . M1MN Mn 0.13728(19) 0.3542(4) 0.1313(7) 0.078(2) Uani 0.604(11) 1 d P . . M2SB Sb 0.06047(16) 0.6271(3) 0.1220(6) 0.0346(12) Uani 0.43(3) 1 d P . . M2AS As 0.06047(16) 0.6271(3) 0.1220(6) 0.0346(12) Uani 0.57(3) 1 d P . . M3PB Pb 0.24271(13) 0.5750(2) 0.3818(3) 0.0723(12) Uani 0.65(2) 1 d P . . M3SB Sb 0.24271(13) 0.5750(2) 0.3818(3) 0.0723(12) Uani 0.35(2) 1 d P . . M4AG Ag 0.3593(2) 0.3320(4) 0.1296(8) 0.0775(14) Uani 1 1 d . . . M5PB Pb 0.45294(13) 0.6006(2) 0.1302(4) 0.0387(10) Uani 0.232(18) 1 d P . . M5SB Sb 0.45294(13) 0.6006(2) 0.1302(4) 0.0387(10) Uani 0.768(18) 1 d P . . M6SB Sb 0.11854(17) 0.3444(2) 0.6177(5) 0.0457(8) Uani 1 1 d . . . M7SB Sb 0.05354(15) 0.6435(3) 0.6442(5) 0.0459(14) Uani 0.68(3) 1 d P . . M7AS As 0.05354(15) 0.6435(3) 0.6442(5) 0.0459(14) Uani 0.32(3) 1 d P . . M8PB Pb 0.24490(8) 0.58654(13) 0.8809(2) 0.0394(5) Uani 1 1 d . . . M9MN Mn 0.3643(2) 0.3519(4) 0.6229(11) 0.0270(13) Uani 1 1 d . . . M10A As 0.43765(17) 0.6106(3) 0.6362(5) 0.0224(9) Uani 1 1 d . . . S1 S 0.1004(5) 0.5071(9) 0.3313(12) 0.036(3) Uani 1 1 d . . . S2 S -0.0065(5) 0.2378(9) 0.1565(14) 0.039(3) Uani 1 1 d . . . S3 S 0.2553(5) 0.4399(7) 0.1419(11) 0.035(2) Uani 1 1 d . . . S4 S 0.1630(5) 0.7261(7) 0.1021(12) 0.024(2) Uani 1 1 d . . . S5 S 0.3916(6) 0.5128(9) 0.4309(13) 0.042(3) Uani 1 1 d . . . S6 S 0.3440(5) 0.7213(8) 0.109(2) 0.048(3) Uani 1 1 d . . . S7 S 0.0927(5) 0.5105(8) 0.9138(15) 0.041(3) Uani 1 1 d . . . S8 S 0.4838(6) 0.2797(10) 0.0763(12) 0.044(3) Uani 1 1 d . . . S9 S 0.2370(4) 0.4284(7) 0.6191(15) 0.038(2) Uani 1 1 d . . . S10 S 0.1650(5) 0.7242(8) 0.638(2) 0.045(3) Uani 1 1 d . . . S11 S 0.4005(5) 0.4954(9) 0.8303(11) 0.032(3) Uani 1 1 d . . . S12 S 0.3429(5) 0.7300(8) 0.6581(11) 0.027(2) Uani 1 1 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 M1PB 0.059(3) 0.118(4) 0.056(3) 0.015(3) 0.013(3) 0.013(2) M1MN 0.059(3) 0.118(4) 0.056(3) 0.015(3) 0.013(3) 0.013(2) M2SB 0.035(2) 0.0255(18) 0.044(2) -0.008(2) 0.005(2) -0.0056(15) M2AS 0.035(2) 0.0255(18) 0.044(2) -0.008(2) 0.005(2) -0.0056(15) M3PB 0.0560(16) 0.097(2) 0.0640(17) 0.0179(19) 0.010(2) 0.0259(16) M3SB 0.0560(16) 0.097(2) 0.0640(17) 0.0179(19) 0.010(2) 0.0259(16) M4AG 0.074(3) 0.085(3) 0.074(3) 0.016(4) 0.024(3) 0.049(3) M5PB 0.0316(14) 0.0462(17) 0.0383(15) -0.0007(16) -0.0007(15) 0.0042(11) M5SB 0.0316(14) 0.0462(17) 0.0383(15) -0.0007(16) -0.0007(15) 0.0042(11) M6SB 0.0560(18) 0.0349(16) 0.0462(18) -0.002(2) 0.008(2) -0.0016(15) M7SB 0.0259(17) 0.054(2) 0.058(3) -0.023(2) 0.003(2) 0.0050(16) M7AS 0.0259(17) 0.054(2) 0.058(3) -0.023(2) 0.003(2) 0.0050(16) M8PB 0.0331(9) 0.0354(9) 0.0497(9) 0.0007(10) -0.0058(13) 0.0022(8) M9MN 0.024(3) 0.024(3) 0.033(3) 0.006(4) -0.001(4) -0.003(3) M10A 0.026(2) 0.0154(17) 0.026(2) 0.004(2) 0.002(2) 0.0003(15) S1 0.033(5) 0.043(6) 0.031(6) 0.016(5) 0.005(5) 0.005(5) S2 0.034(5) 0.033(6) 0.050(7) 0.006(6) 0.007(6) 0.006(5) S3 0.041(5) 0.030(5) 0.034(6) -0.002(5) -0.002(7) 0.011(5) S4 0.027(5) 0.025(5) 0.020(5) -0.005(5) 0.004(5) -0.004(4) S5 0.042(6) 0.018(5) 0.067(8) 0.003(5) 0.010(6) 0.000(5) S6 0.028(5) 0.032(6) 0.084(9) 0.005(8) -0.001(8) -0.009(5) S7 0.033(5) 0.016(5) 0.073(9) 0.003(6) 0.005(6) -0.005(5) S8 0.045(7) 0.053(8) 0.033(6) 0.007(5) -0.002(5) 0.016(6) S9 0.030(5) 0.022(5) 0.062(6) 0.008(6) 0.002(7) 0.005(4) S10 0.033(5) 0.023(5) 0.079(8) -0.019(8) 0.019(8) 0.008(5) S11 0.034(5) 0.032(6) 0.030(6) 0.003(5) -0.005(5) 0.008(5) S12 0.026(5) 0.035(6) 0.019(5) 0.007(4) -0.002(5) -0.003(5) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag M1PB S3 2.518(11) . ? M1PB S1 2.669(13) . ? M1PB S6 2.793(17) 2_545 ? M1PB S7 2.837(12) 1_554 ? M1PB S12 2.939(11) 2_545 ? M2SB S4 2.344(10) . ? M2SB S7 2.383(12) 1_554 ? M2SB S1 2.458(11) . ? M3PB S3 2.669(10) . ? M3PB S9 2.740(11) . ? M3PB S1 2.900(11) . ? M3PB S5 2.998(13) . ? M4AG S3 2.425(10) . ? M4AG S8 2.525(12) . ? M4AG S4 2.675(12) 2_545 ? M4AG S10 2.689(18) 2_545 ? M5PB S6 2.600(11) . ? M5PB S8 2.617(12) 3_665 ? M5PB S2 2.710(11) 2 ? M5PB S5 3.022(11) . ? M5PB S11 3.041(11) 1_554 ? M5PB S11 3.087(11) 3_666 ? M6SB S12 2.501(11) 2_546 ? M6SB S9 2.514(9) . ? M6SB S6 2.579(15) 2_545 ? M7SB S10 2.375(11) . ? M7SB S2 2.435(12) 3_566 ? M7SB S8 2.641(13) 2 ? M7SB S7 2.936(13) . ? M8PB S3 2.895(10) 1_556 ? M8PB S9 2.993(12) . ? M8PB S4 3.021(10) 1_556 ? M8PB S7 3.095(10) . ? M8PB S10 3.102(15) . ? M9MN S4 2.539(13) 2_545 ? M9MN S11 2.621(13) . ? M9MN S9 2.632(10) . ? M9MN S10 2.654(16) 2_546 ? M9MN S5 2.660(13) . ? M9MN S2 2.748(12) 4_666 ? M10A S5 2.311(12) . ? M10A S11 2.312(11) . ? M10A S12 2.376(10) . ? S2 M7AS 2.435(12) 3_566 ? S2 M7SB 2.435(12) 3_566 ? S2 M5PB 2.710(11) 2_545 ? S2 M5SB 2.710(11) 2_545 ? S2 M9MN 2.748(12) 4_565 ? S3 M8PB 2.895(10) 1_554 ? S4 M9MN 2.539(13) 2 ? S4 M4AG 2.675(12) 2 ? S4 M8PB 3.021(10) 1_554 ? S6 M6SB 2.579(15) 2 ? S6 M1PB 2.793(17) 2 ? S6 M1MN 2.793(17) 2 ? S7 M2AS 2.383(12) 1_556 ? S7 M2SB 2.383(12) 1_556 ? S7 M1MN 2.837(12) 1_556 ? S7 M1PB 2.837(12) 1_556 ? S8 M5SB 2.617(12) 3_665 ? S8 M5PB 2.617(12) 3_665 ? S8 M7AS 2.641(13) 2_545 ? S8 M7SB 2.641(13) 2_545 ? S10 M9MN 2.654(16) 2_556 ? S10 M4AG 2.689(18) 2 ? S11 M5PB 3.041(11) 1_556 ? S11 M5PB 3.087(11) 3_666 ? S12 M6SB 2.501(11) 2_556 ? S12 M1PB 2.939(11) 2 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag S3 M1PB S1 84.6(4) . . ? S3 M1PB S6 96.7(3) . 2_545 ? S1 M1PB S6 88.4(4) . 2_545 ? S3 M1PB S7 89.7(3) . 1_554 ? S1 M1PB S7 80.0(3) . 1_554 ? S6 M1PB S7 166.2(4) 2_545 1_554 ? S3 M1PB S12 98.2(3) . 2_545 ? S1 M1PB S12 162.3(3) . 2_545 ? S6 M1PB S12 108.6(3) 2_545 2_545 ? S7 M1PB S12 82.5(3) 1_554 2_545 ? S4 M2SB S7 93.3(4) . 1_554 ? S4 M2SB S1 96.9(4) . . ? S7 M2SB S1 94.0(3) 1_554 . ? S3 M3PB S9 97.4(3) . . ? S3 M3PB S1 77.5(3) . . ? S9 M3PB S1 82.4(3) . . ? S3 M3PB S5 81.3(3) . . ? S9 M3PB S5 76.1(3) . . ? S1 M3PB S5 147.5(3) . . ? S3 M4AG S8 159.7(4) . . ? S3 M4AG S4 96.5(3) . 2_545 ? S8 M4AG S4 100.0(3) . 2_545 ? S3 M4AG S10 100.3(4) . 2_545 ? S8 M4AG S10 83.1(4) . 2_545 ? S4 M4AG S10 115.8(3) 2_545 2_545 ? S6 M5PB S8 89.4(4) . 3_665 ? S6 M5PB S2 88.5(4) . 2 ? S8 M5PB S2 84.1(3) 3_665 2 ? S6 M5PB S5 87.6(4) . . ? S8 M5PB S5 163.7(4) 3_665 . ? S2 M5PB S5 79.8(3) 2 . ? S6 M5PB S11 86.2(4) . 1_554 ? S8 M5PB S11 81.3(3) 3_665 1_554 ? S2 M5PB S11 164.5(3) 2 1_554 ? S5 M5PB S11 114.5(3) . 1_554 ? S6 M5PB S11 167.1(3) . 3_666 ? S8 M5PB S11 82.9(3) 3_665 3_666 ? S2 M5PB S11 80.4(3) 2 3_666 ? S5 M5PB S11 97.0(3) . 3_666 ? S11 M5PB S11 102.7(2) 1_554 3_666 ? S12 M6SB S9 88.5(4) 2_546 . ? S12 M6SB S6 97.7(3) 2_546 2_545 ? S9 M6SB S6 90.3(3) . 2_545 ? S10 M7SB S2 94.9(4) . 3_566 ? S10 M7SB S8 87.1(4) . 2 ? S2 M7SB S8 89.3(3) 3_566 2 ? S10 M7SB S7 91.9(4) . . ? S2 M7SB S7 84.8(4) 3_566 . ? S8 M7SB S7 173.9(4) 2 . ? S3 M8PB S9 98.1(3) 1_556 . ? S3 M8PB S4 86.4(3) 1_556 1_556 ? S9 M8PB S4 145.7(2) . 1_556 ? S3 M8PB S7 78.2(3) 1_556 . ? S9 M8PB S7 79.1(3) . . ? S4 M8PB S7 68.4(3) 1_556 . ? S3 M8PB S10 154.3(3) 1_556 . ? S9 M8PB S10 81.9(3) . . ? S4 M8PB S10 79.9(3) 1_556 . ? S7 M8PB S10 76.5(3) . . ? S4 M9MN S11 173.1(5) 2_545 . ? S4 M9MN S9 91.7(4) 2_545 . ? S11 M9MN S9 90.0(4) . . ? S4 M9MN S10 98.4(3) 2_545 2_546 ? S11 M9MN S10 88.1(5) . 2_546 ? S9 M9MN S10 92.0(4) . 2_546 ? S4 M9MN S5 93.5(4) 2_545 . ? S11 M9MN S5 80.0(3) . . ? S9 M9MN S5 84.0(4) . . ? S10 M9MN S5 167.5(5) 2_546 . ? S4 M9MN S2 90.2(4) 2_545 4_666 ? S11 M9MN S2 88.7(4) . 4_666 ? S9 M9MN S2 173.9(5) . 4_666 ? S10 M9MN S2 82.0(4) 2_546 4_666 ? S5 M9MN S2 101.6(4) . 4_666 ? S5 M10A S11 94.5(4) . . ? S5 M10A S12 96.1(4) . . ? S11 M10A S12 96.2(4) . . ? M2SB S1 M1PB 94.2(4) . . ? M2SB S1 M3PB 102.5(4) . . ? M1PB S1 M3PB 93.3(3) . . ? M7AS S2 M7SB 0.00(19) 3_566 3_566 ? M7AS S2 M5PB 94.3(4) 3_566 2_545 ? M7SB S2 M5PB 94.3(4) 3_566 2_545 ? M7AS S2 M5SB 94.3(4) 3_566 2_545 ? M7SB S2 M5SB 94.3(4) 3_566 2_545 ? M5PB S2 M5SB 0.00(13) 2_545 2_545 ? M7AS S2 M9MN 89.5(4) 3_566 4_565 ? M7SB S2 M9MN 89.5(4) 3_566 4_565 ? M5PB S2 M9MN 98.4(4) 2_545 4_565 ? M5SB S2 M9MN 98.4(4) 2_545 4_565 ? M4AG S3 M1PB 120.0(4) . . ? M4AG S3 M3PB 118.0(4) . . ? M1PB S3 M3PB 102.7(3) . . ? M4AG S3 M8PB 112.7(4) . 1_554 ? M1PB S3 M8PB 100.8(3) . 1_554 ? M3PB S3 M8PB 99.5(3) . 1_554 ? M2SB S4 M9MN 102.5(4) . 2 ? M2SB S4 M4AG 94.1(3) . 2 ? M9MN S4 M4AG 106.9(4) 2 2 ? M2SB S4 M8PB 99.8(3) . 1_554 ? M9MN S4 M8PB 90.5(3) 2 1_554 ? M4AG S4 M8PB 154.9(4) 2 1_554 ? M10A S5 M9MN 91.5(4) . . ? M10A S5 M3PB 109.2(4) . . ? M9MN S5 M3PB 95.5(4) . . ? M10A S5 M5PB 106.7(4) . . ? M9MN S5 M5PB 151.1(5) . . ? M3PB S5 M5PB 99.2(3) . . ? M6SB S6 M5PB 100.4(4) 2 . ? M6SB S6 M1PB 100.8(4) 2 2 ? M5PB S6 M1PB 101.4(5) . 2 ? M6SB S6 M1MN 100.8(4) 2 2 ? M5PB S6 M1MN 101.4(5) . 2 ? M1PB S6 M1MN 0.0(2) 2 2 ? M2AS S7 M2SB 0.0(2) 1_556 1_556 ? M2AS S7 M1MN 91.7(4) 1_556 1_556 ? M2SB S7 M1MN 91.7(4) 1_556 1_556 ? M2AS S7 M1PB 91.7(4) 1_556 1_556 ? M2SB S7 M1PB 91.7(4) 1_556 1_556 ? M1MN S7 M1PB 0.00(14) 1_556 1_556 ? M2AS S7 M7SB 98.9(3) 1_556 . ? M2SB S7 M7SB 98.9(3) 1_556 . ? M1MN S7 M7SB 169.4(5) 1_556 . ? M1PB S7 M7SB 169.4(5) 1_556 . ? M2AS S7 M8PB 97.0(4) 1_556 . ? M2SB S7 M8PB 97.0(4) 1_556 . ? M1MN S7 M8PB 89.5(3) 1_556 . ? M1PB S7 M8PB 89.5(3) 1_556 . ? M7SB S7 M8PB 89.6(3) . . ? M4AG S8 M5SB 114.2(5) . 3_665 ? M4AG S8 M5PB 114.2(5) . 3_665 ? M5SB S8 M5PB 0.00(17) 3_665 3_665 ? M4AG S8 M7AS 92.3(4) . 2_545 ? M5SB S8 M7AS 91.8(3) 3_665 2_545 ? M5PB S8 M7AS 91.8(3) 3_665 2_545 ? M4AG S8 M7SB 92.3(4) . 2_545 ? M5SB S8 M7SB 91.8(3) 3_665 2_545 ? M5PB S8 M7SB 91.8(3) 3_665 2_545 ? M7AS S8 M7SB 0.0(2) 2_545 2_545 ? M6SB S9 M9MN 133.4(4) . . ? M6SB S9 M3PB 108.7(4) . . ? M9MN S9 M3PB 102.7(4) . . ? M6SB S9 M8PB 109.4(4) . . ? M9MN S9 M8PB 101.0(4) . . ? M3PB S9 M8PB 95.1(3) . . ? M7SB S10 M9MN 93.0(4) . 2_556 ? M7SB S10 M4AG 94.6(5) . 2 ? M9MN S10 M4AG 107.3(4) 2_556 2 ? M7SB S10 M8PB 101.0(5) . . ? M9MN S10 M8PB 86.7(5) 2_556 . ? M4AG S10 M8PB 158.5(4) 2 . ? M10A S11 M9MN 92.4(4) . . ? M10A S11 M5PB 102.5(4) . 1_556 ? M9MN S11 M5PB 162.1(5) . 1_556 ? M10A S11 M5PB 92.5(3) . 3_666 ? M9MN S11 M5PB 92.4(3) . 3_666 ? M5PB S11 M5PB 77.3(2) 1_556 3_666 ? M10A S12 M6SB 101.6(4) . 2_556 ? M10A S12 M1PB 100.1(3) . 2 ? M6SB S12 M1PB 106.6(4) 2_556 2 ? _diffrn_measured_fraction_theta_max 0.992 _diffrn_reflns_theta_full 25.00 _diffrn_measured_fraction_theta_full 0.992 _refine_diff_density_max 2.140 _refine_diff_density_min -2.036 _refine_diff_density_rms 0.453